Synfacts

Ausgabe 10 · Oktober 2022

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A151
Zanda, Matteo: SYNFORM ISSUE 2022/10 FREIER ZUGRIFF

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Synthesis of Natural Products
z1057
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1057
Synthesis of (–)-Tetrodotoxin

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1058
Synthesis of (–)-Simplicissin

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1059
Total Synthesis of Indolizidine Alkaloid (±)-Bipolamine I FREIER ZUGRIFF

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1060
Total Synthesis of (+)-Alstonlarsine A

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1061
Synthesis of (+)-Darobactin A

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1062
Total Synthesis of (–)-Antroalbocin A

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1063
Total Synthesis of (–)-Salsolene Oxide FREIER ZUGRIFF

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Synthesis of Heterocycles
z1065
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1065
Copper-Catalyzed Isoxazole Synthesis

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PDF (93 kb)
1066
TEMPO-Mediated Convergent Synthesis of Benzoxazoles from Primary Amines and Cyclohexanones

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1067
Photoredox Cross-Coupling for Propellane-Curious Chemists FREIER ZUGRIFF

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1068
One-Pot Cascade Synthesis of 2‑Azafluorenones Mediated by Generation of Ammonia in situ

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1069
A Mild and Site-Selective Protocol for N1-Carboxylation of 2-Alkynylindoles

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PDF (105 kb)
1070
NHC-Alcohol Adduct-Mediated Photocatalytic Deoxygenation for the Synthesis of 6-Phenanthridine Derivatives

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1071
Carbonyl Compounds through Photochemical Olefin Cleavage

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1072
α-C–H Functionalization of Alcohols Delivers C⁶-Hydroxyalkylated Purines and Purine Nucleosides

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1073
Copper-Catalyzed Synthesis of Trifluoromethylated 4H-Pyrans

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1074
Manganese(III) Acetate-Promoted Mild Sulfonation of (Het)arenes

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1075
Facile Rearrangement of Oxetane-Carboxylic Acids to Lactones

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1076
Multicomponent Approach to Functionalized Isoquinolines

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1077
Synthesis of Pyrazoloimidazoquinazolinones and COVID-19 Protease Docking Studies

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1078
Synthesis of 7-[(Arylsulfanyl)methyl]dibenzo[b,d]azepines

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Synthesis of Materials and Unnatural Products
z1079
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1079
A Möbius Carbon Nanobelt Accomplished FREIER ZUGRIFF

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1080
γ-Graphyne via Alkyne Metathesis

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1081
Dibenzocarbazole from Decarboxylative Biscyclization

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1082
Syntheses of PAHs Embedded with Azulene Modules

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1083
Contorted PAHs via Cycloaddition to Cyclobutadienoids

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1084
Cascade Polymer Degradation on the Trigger

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1085
Quintuple [7]Helicene in One

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1086
Ring-Fusion and Polymerization of Aza-Heteroaromatics

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1087
B,N-Doped Emitters from Amine-Directed Borylation

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1088
[3]Rotaxanes Threaded by Polyyne via Dicobalt Complexes

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1089
Living Suzuki–Miyaura Catalyst-Transfer Polymerization

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Metals in Synthesis
z1091
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1091
Site-Selective Allylic C–H Amination of Alkenes Enabled by Formation of an Aminium Radical Cation FREIER ZUGRIFF

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1092
Dioxazolones as Masked Amides in the Copper-Promoted Reaction with Arylboronic Acids

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1093
Stereospecific Functionalization of Activated Alkylboronic Esters under Copper Catalysis FREIER ZUGRIFF

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PDF (138 kb)
1094
The Bigger the Better: ortho-Selective C–H Activation in Alkylarenes by Transient Benzylic C–H Activation

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1095
Rh(III)-Catalyzed Diastereoselective Amino Oxygenation/Amination of 1,3-Dienes

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1096
A Cyclopropane-Based Diphosphine Ligand Enables Regioselective Hydroboration of Internal Alkynes

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1097
Regiodivergent Access to 1,1- or 1,2-Disubstituted Alkenes via Cobalt-Catalyzed Hydroalkylation of Alkynes

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1098
Nickel-Catalyzed Cross-Electrophile Coupling of Heteroaryl Imines and Alkyl Halides

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1099
Switching Regioselectivity in the Mizoroki–Heck-Reaction by Cooperative Triple Catalysis

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1100
Nickel-Catalyzed Hydroalkylation of Trifluoromethylalkenes

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1101
Enantioconvergent Nickel-Catalyzed α-Alkylation of Racemic Reformatsky Reagents

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1102
Alkylation of Amines and Ammonia with Nitriles by Nickel-Catalyzed Hydrogenative Cross-Coupling

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1103
Three-Component Coupling of Aldimine Esters, 1,3-Butadiene and Alkyl Bromides under Dual Catalysis

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1104
Nickel-Catalyzed Enantioconvergent Cross-Electrophile Arylation and Vinylation of 1-Chloro-1-Alkanol Esters

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1105
Deoxygenative Cross-Coupling of Benzyl Alcohols and Boronic Acids Enabled by Transient Isourea Formation

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1106
Cu/Photoredox Dual-Catalytic Decarboxylative Sulfonylfluorination Reaction

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1107
Nickel Electrocatalytic Sulfinylation of Aryl Halides using SO₂

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1108
Deoxygenative Cross-Coupling Reactions of Phenols Enabled by Transient O-Phenyl-Uronium Formation

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1109
A Base-Free Protocol for the Rhodium-Catalyzed Benzylic Addition of Alkylarenes to Michael Acceptors

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1110
Nickel-Catalyzed Isomerization/Cross-Coupling Reaction of Epoxides and Aryl Triflates

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1111
C4 Alkylation of Pyridines Enabled by the Use of a Bulky Aluminum Lewis Acid and Nickel Catalysis

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1112
Asymmetric Benzylic C(sp³)–H Trifluoromethylation by Dual Organophotoredox and Copper Catalysis

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1113
Iron-Catalyzed Domino Cyclization of Methylene Cyclopropyl 1,6-Enynes

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1114
Stereoselective Rh(III)-Catalyzed Cyclopropanation of Sulfoxonium Ylides with β,γ-Unsaturated Keto Esters

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1115
Photo/Cobalt Dual Catalytic Enantioselective Hydroarylation of 1,6-Enynes

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1116
Enantioselective Conjugate Addition of Alkenyl Heteroarenes with Alkene Nucleophiles

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1117
The Enantioselective Tsuji Decarboxylative Allylic Alkylation FREIER ZUGRIFF

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1118
Arylalkenylation of Alkynes Catalyzed by Nickel

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Polymer-Supported Synthesis
z1119
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1119
Heck Reaction and Suzuki–Miyaura Cross-Coupling on a Humin-Like-Polymer-Immobilized Pd Catalyst

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1120
Palladium Nanoparticles Catalyze the Oxidative Methoxylation of 8-Methylquinolines with Methanol

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1121
Hydroamination of Arylacetylenes by Gold Nanoclusters Immobilized on Carbon FREIER ZUGRIFF

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1122
C–P Cross-Coupling of Terminal Alkynes with H-Phosphonates by a Copper Photocatalyst

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1123
Metal–Organic Layers Containing Ru Photosensitizers and Au Catalysts for Reactions of Aryldiazonium Salts

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1124
Click Reactions Promoted by a Nanomagnetic Manganese(II)–Schiff Base Complex

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1125
Photocatalytic C–N Coupling of Aryl Chlorides on a Copper Nanocluster

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1126
Markovnikov Hydroaminocarbonylation of Alkenes and Alkynes with a Soluble Heterogeneous Pd Catalyst

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1127
Visible-Light-Driven C–N Coupling Promoted by Nickel Single Atoms on Carbon Nitride

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1128
Synthesis of Thiazolidin-4-ones and Hexahydroquinolines on Fe₃O₄@Urea-Benzoic Acid

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1129
Dehydrogenative Condensation of N,N′-Disubstituted Ureas and 1,2-Diols on Pd/Al₂O₃

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Organo- and Biocatalysis
z1131
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1131
Brønsted Acid Catalysis Permits Electrophilic Halogenation of Electron-Deficient Arenes FREIER ZUGRIFF

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1132
Photocatalytic Decarboxylative Phosphorylation of α-Amino Esters of N-Hydroxyphthalimide

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1133
Acridine Radicals Permit Reductive Coupling of Aliphatic and Aromatic Carbonyls with Olefins

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1134
Organophotocatalytic Radical Difluoromethylation of Nonactivated Alkenes

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1135
Photoenzymatic Intramolecular Cyclization of α-Chloroamides with Allylsilanes

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1136
Organocatalytic Asymmetric Synthesis of Axially Chiral Cyclohexadienylidene Compounds

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1137
Engineered Cytochrome P450 Permits Scalable Oxidative Biaryl Coupling toward Arylomycins

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1138
Desymmetrization of meso-Cyclohexenediones through Dienamine Catalysis

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1139
Base-Promoted Reductive Coupling of (Trifluoromethyl)arenes

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Innovative Drug Discovery and Development
z1141
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1141
A β-Lactone for Covalent Inhibition of KRAS G12S FREIER ZUGRIFF

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1142
A Novel Covalent Target for Inhibiting Pancreatic Cancer Stem Cell Growth

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1143
Anticancer Dual Molecule Targeting Inhibition of Tubulin Polymerization and HDAC

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1144
Improved Solubility of Contezolid via an O-Acyl Phosphoramidate Prodrug

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1145
A Late-Stage Electrophilic Halogenation of Arenes with Electron-Withdrawing Substituents

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1146
Deep-Near-IR Bioimaging Using Silicon-Substituted Bis-Benzannulated Rhodamine Dyes

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1147
Synthesis of BLU-945, an EGFR Mutant Inhibitor for Treatment-Resistant Non-Small-Cell Lung Cancer

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1148
Improved Synthesis toward β-Lactam Antibiotics

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1149
General Synthesis of TF-DUBTACs

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1150
Thallusin – A Potent Chemical Mediator for Chemosynthetic Symbioses of Marine Organisms

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1151
Overcoming Drug Resistance with Mechanistic Understanding

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1152
Five-Step Synthesis of MDM2-p43 Inhibitor BI-0282

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1153
A Convergent Synthesis of (+)-Ikarugamycin FREIER ZUGRIFF

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1154
Enzyme Evolution as Key to Selective Bioconjugation

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Peptide Chemistry
z1155
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1155
Preparation of Dehydroamino Acids/Peptides and their Application FREIER ZUGRIFF

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1156
Palladium-Catalyzed Cyanomethylation of Amino Acids

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1157
Photoredox C(sp³)–H Bond Activation to Form Tetrasubstituted Amino Acids

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1158
Copper/Iridium-Catalyzed Cascade Reaction for the Synthesis of α-Deuterated α-Amino Acids

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PDF (100 kb)
1159
Asymmetric Mannich Reaction for the Synthesis of β-Amino Amides

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1160
Microwave-Assisted Aminocarbonylation of α-Amino Acid Esters

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1161
α,β-Diamino Acid Synthesis by a Mannich-Type Reaction of Azlactones and 2-Aminoacrylates

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1162
Iridium-Catalyzed Carbonyl Alkylative Amination Reaction under Blue LED Irradiation

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1163
(Diethylamino)sulfur Trifluoride (DAST) for Fmoc-Amino Acyl Fluoride Synthesis FREIER ZUGRIFF

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Flow Chemistry
z1165
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1165
Synthesis of Ketones via a Multiphoton Tandem Photoredox Protocol in Continuous Flow

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1166
Flow Synthesis of 1,4-Benzothiazines from (E)-β-Chlorovinyl Ketones and 2,2′-Sulfanyldianilines

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