Synfacts

Ausgabe 08 · August 2023

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Ausgabe
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A133
SYNFORM ISSUE 2023/08 FREIER ZUGRIFF

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Synthesis of Natural Products
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0741
Synthesis of (–)-Retigeranic Acid A FREIER ZUGRIFF

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0742
Synthesis of (–)-Alloaristoteline

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0743
Synthesis of (+)-Aberrarone

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0744
Synthesis of (±)-Sculponin U

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0745
Synthesis of (±)-Daphnillonin B

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0746
Total Synthesis of (–)-Alstomutinine C

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0747
Total Synthesis of (±)-Khusimone FREIER ZUGRIFF

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Synthesis of Heterocycles
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0749
Alternative to Ozonolysis for the Oxidative Cleavage of Olefins FREIER ZUGRIFF

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0750
General, Scalable Synthesis of 3-Azabicyclo[3.1.1]heptanes

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0751
Synthesis and Reactivity of 4H-Dewar Pyridines as Rigid Bioisosteres for 4-Substituted Piperidines

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0752
Building Highly Substituted Furyl Boronates via Carbene Boryl Migratory Insertion

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0753
Synthesis of P-Heterocycles from Unsaturated Phosphonites with C(sp²)-Electrophiles

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0754
Palladium-Catalyzed Synthesis of Indoles from ortho-Nitrostyrene and Formic Acid

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0755
Computational Studies on the Reaction Pathways of 1,2-Azaborinine with Unsaturated Organic Compounds

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0756
Photocatalyzed Access to Protected Trifluoromethyl Ketones through C–C Bond Formation

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0757
Ironing-Out Photodecarboxylation: Cross-Nucleophile Coupling Mediated by Iron Salts

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0758
Efficient Ring Opening Kinetic Resolution of 2,3-Aziridinyl Alcohols with Dinuclear Zinc Complexes

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0759
Sustainable Syntheses of Pyridines and Quinolines

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0760
Radical Ring Expansion of Hemiketal Hydroperoxides to Macrolactones

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Synthesis of Materials and Unnatural Products
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0761
Topologically Chiral Nanohoops FREIER ZUGRIFF

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0762
Stereoselective Synthesis of Tetraarylethylene

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0763
Functionalizing High-Energy Density Cages

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0764
Isolable Arene-Fused 1,2-Diborete Biradicaloid

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0765
Facile Functionalization of Bicyclo[1.1.1]pentane

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0766
Direct C–H Borylation of Trityl Radical

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0767
Mechanical Chirality

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0768
Joining Inorganic Cages into Polymers

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0769
Sliding Pseudorotaxane Catalysts

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0770
Enantioselective Access to Carbohelicenes

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0771
[2+2+2]-Enabled Organic Covalent Cages

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0772
Three-State Photochromism

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Metals in Synthesis
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0773
The Catellani Reaction meets C–H Activation: Synthesis of 1,3-Disubstituted Planar Chiral Metallocenes FREIER ZUGRIFF

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0774
Unsymmetrical Ketone Synthesis via Selective Nickel-Catalyzed Reductive Carbonylation

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0775
Leveraging Strain-Release in Dearomative Photocycloadditions of Bicyclic Aza-Arenes FREIER ZUGRIFF

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0776
Asymmetric Synthesis of Unnatural Monoterpene-Linked Heterocycles

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0777
Novel Acyl Suzuki–Miyaura Coupling Between N-Hydroxybenzotriazole Esters and Boronic Acids

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0778
Cobalt-Catalyzed Cleavage of Tertiary Allylic Alcohols into Ketones

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0779
Benzopyrano[4,3-b]pyridine Synthesis via Copper-Catalyzed Oxidative Reaction

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0780
Turning Homoallylic Alcohols into Aliphatic Ketones under Nickel Catalysis

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0781
Alkynylative Lactonization of 2-Vinylbenzoates to 3-Substituted Isochroman-1-ones

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0782
Synthesis of Bicyclic α,β-Unsaturated γ-Lactams through an Intramolecular Reductive Pauson–Khand Reaction

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0783
Silanols as Carbon-Centered Radical Precursors: Photo-induced Cerium-Catalyzed C(sp³)–Si Bond Cleavage

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0784
Ru-Catalyzed Synthesis of Polysubstituted Arenes via a Directing Group Relay Strategy and C–H Functionalization

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0785
Synthesis of Arylated Allenyl Monofluorides via Copper-Catalyzed Defluoroarylation of gem-Difluoroallenes

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0786
Enantioselective Three-Component Sulfonylalkenylation of Styrenes to Access β-Chiral Sulfones

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0787
Access to Aryl and Vinyl Halides Enabled by Nickel-Catalyzed Halogenation of Thianthrenium Salts

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0788
Nickel- and Neodymium-Catalyzed Asymmetric Synthesis of Hantzsch Esters

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0789
Two-Step One-Carbon Homologation/Ring Expansion of Ketones

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0790
Palladium-Catalyzed Regio- and Enantioselective Remote Diacetylation of Internal Olefins

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0791
Synthesis of Bis-Heterocycles via Gold-Catalyzed Domino Cyclization Reactions

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0792
Co-Catalyzed Three-Component Synthesis of N-Pyrimidyl Indoles

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0793
Iridium-Catalyzed Synthesis of N–N Biaryl Atropisomers via Asymmetric C–H Activation with Acrylates

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0794
Rhodium-Catalyzed Stereoselective Synthesis of E-Dienyl Esters from Acetylene and Carboxylic Acids

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0795
Electrified: Electroreductive Cobalt-Catalyzed C(sp²)–Ge and C(sp³)–Ge Bond Formation

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0796
Synthesis of N–O-Linked Glycosides via Stereospecific Pd-Catalyzed Reaction

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0797
Pd/Visible Light-Promoted Head-to-Tail Hydroalkenylation of Alkenes

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0798
Pd-Catalyzed Synthesis of Bridged Polycyclic Lactams via Intermolecular Carbonylative Dearomatization

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0799
The Saegusa–Ito Oxidation of Silyl Enol Ethers to α,β-Unsaturated Carbonyl Compounds FREIER ZUGRIFF

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Polymer-Supported Synthesis
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0801
Oxidative Cleavage and Ammoxidation of C–S Bonds by Cobalt/N-Doped Carbon Catalyst FREIER ZUGRIFF

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0802
Photocatalytic Methylation of (Iso)quinoliniums with DMSO

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0803
Iminyl Radical-Mediated Reactions Using a Dimeric Cu-BINAP Complex Supported on Pillar-Layered MOF

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0804
Arylation of Elemental Sulfur Forming Diaryl Disulfides by a Single-Atom Copper Catalyst on Ceria

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0805
Suzuki–Miyaura Coupling Using Flow-Through Membrane Reactor

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0806
Transfer Hydrogenation of N-Heteroarenes with a COF-Anchored Rhodium Bipyridine Catalyst in Water

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0807
N-Formylation of Aliphatic Primary and Secondary Amines with CO₂/H₂ by Cu₂O/Cu Supported on Alumina

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0808
Photocatalytic Arylation of Quinoxalin-2(1H)-ones with Arylhydrazines by g-C₃N₄ and NaI

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0809
Regio- and Stereoselective Hydroboration of Enallenes by Palladium Nanoparticles Immobilized on Cellulose

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0810
Synthesis of Substituted Pyridines Using a Ni(II)−Picolyamine Complex Supported on SiO₂/Fe₃O₄

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0811
Gold Nanoparticles Supported on Ti or Zr Oxide for Deoxygenative Silylation of C(sp³)–O Bonds

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Organo- and Biocatalysis
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0813
Chiral-Phosphoric-Acid-Catalyzed Asymmetric Dearomatization of Indole Derivatives FREIER ZUGRIFF

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0814
CO₂ Reduction by a Membranous, Metal-Free, Triazine- and Imine-Containing Covalent Organic Framework

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0815
Enantioselective Nucleophilic Desymmetrization of Phosphonate Esters Using Bifunctional Superbases

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0816
Biocatalysis and Photocatalysis Joining Forces in a Stereoselective Method for Synthesis of Sulfones

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0817
Bifunctional Iminophosphorane Catalyst Enables Challenging Intramolecular Oxa-Michael Reactions

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0818
An Effcient Organocatalytic Chlor-Alkali Process

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0819
Photocatalytic Z to E Isomerisation of Fluorinated β-Borylacrylates

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0820
Imidodiphosphorimidates(IDPis) Permit Asymmetric Synthesis of cis-Tetrahydrocannabinoids

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0821
Engineered Photoenzyme Overrides Traditional Regioselectivities in the Alkylation of Indoles

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Innovative Drug Discovery and Development
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0823
Development of the Commercial Manufacturing Process for Nirmatrelvir in 17 Months FREIER ZUGRIFF

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0824
Selective Boronate Addition to Pyridiniums

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0825
Photoproximity Labeling of Proteins FREIER ZUGRIFF

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0826
Discovery of ACT-774312: A Potent and Selective CRTH2 Receptor Antagonist

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0827
Tenofovir Prodrug Synthesis Inspires Novel C–P Bond-Forming Method

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0828
Discovery of the First OX₁R-Selective Agonist: YNT-3708

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0829
RAFT Polymer−Antibody Conjugation of a Therapeutic Anti-EGFR Antibody to Increase Tumor Uptake In Vivo

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0830
Design and Synthesis of the First-in-Class MC4R Antagonist, PF-07258669 with [4,5]-Spirocyclic Core

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0831
A Modular Platform for Covalent, Photoswitchable Control over Enzyme Activity

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0832
One-Pot Preparation of Thioamide Peptides

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0833
Scalable Synthesis of KRAS G12C Inhibitor GDC-6036

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0834
Understanding the Impact of Impurities in Peptide Coupling Reagents

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0835
No Need to Feed: Complete Integration of Carbene-Transfer Chemistry into Biosynthesis

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Peptide Chemistry
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0837
Efficient Method for Cyclic Peptide Synthesis Mediated by Acylammonium Species FREIER ZUGRIFF

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0838
Ir-Catalyzed Functionalization of Alkyl Silane with Benzosultam

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0839
Organocatalyzed Synthesis of Cyclized Amino Acids with Cyanocoumarin

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0840
Copper-Catalyzed Synthesis of α,α-Disubstituted Amino Acid Derivatives

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0841
Enantio- and Diastereoselective Annulation to Form Fused Amino Acid Derivatives

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0842
Synthesis of anti-β-Amino Organoborons via Radical Hydroboration

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0843
AlMe₃-Mediated One-Pot Peptide Bond Formation of N- and C-Terminal Amino Acids

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0844
Diboronic Acid Anhydride-Catalyzed Synthesis of Serine or Threonine Containing 2,5-Diketopiperazines

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0845
Synthesis of Unnatural Amino Acids from in situ Generated Glycine Cation Equivalents FREIER ZUGRIFF

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0846
W-Catalyzed C(sp³)–H Alkylation of Valine

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Flow Chemistry
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0847
Photochemical [2+2] Cycloaddition between Alkynes and Maleimides Using Continuous Flow

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0848
Microwave-Assisted C–C Bond Formation to Access Fused-Ring Compounds

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