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Synlett 1999; 1999(6): 750-752
DOI: 10.1055/s-1999-2714
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Preparation of a Rigid Macrocycle with Two Exotopic Phenanthroline Binding Sites

Michael Schmittel* , Horst Ammon
  • *Institut für Organische Chemie der Universität Würzburg, Am Hubland, D-97074 Würzburg, Germany. New address: FB 8 (Chemie - Biologie), Organische Chemie I, Universität GH Siegen, Adolf Reichwein Str., D-57068 Siegen, Germany; Fax +49 2 71 7 40 32 70; E-mail: schmittel@chemie.uni-siegen.de
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Publication Date:
31 December 1999 (online)

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The preparation of the first rigid macrocyclic bisphenanthroline with exotopic binding sites is described using a series of Sonogashira coupling reactions.

phenanthroline - bisphenanthroline - macrocyclization - Sonogashira coupling