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Synlett 2001; 2001(12): 1953-1955
DOI: 10.1055/s-2001-18737
DOI: 10.1055/s-2001-18737
letter
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Efficient Synthesis of Pyrrolo[3,4-b]hexahydro-1H-1,5-benzodiazepine Derivatives
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Publication History
Publication Date:
04 December 2001 (online)
A variety of pyrrolo[3,4-b]hexahydro-1H-1,5-benzodiazepine derivatives have been prepared in a new one-pot reaction from thiophene-2,3-dione as well as pyrrolidinetrione derivatives and trans-(±)-1,2-diaminocyclohexane. The reactivity of 2,3-dicarbonyl fragment of thiophene-2,3-dione was exploited in the synthesis of fused quinoxaline systems.
1,5-benzodiazepine - condensation - fused heterocycles - rearrangements - quinoxaline