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Synlett 2001; 2001(1): 0105-0107
DOI: 10.1055/s-2001-9734
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Halodecarboxylation of α,β-Unsaturated Carboxylic Acids bearing Aryl and Styrenyl Group at β-Carbon with Oxone® and Sodium Halide

Ho-Woong You* , Kee-Jung Lee
  • *Department of Industrial Chemistry, Hanyang University, Seoul 133-791, South Korea; Fax +82-2-2298-4101; E-mail: leekj@email.hanyang.ac.kr
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Publication Date:
31 December 2001 (online)

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Reaction of α,β-unsaturated carboxylic acid bearing aryl and styrenyl group at β-carbon with Oxone® and sodium halide in aqueous acetonitrile afforded the corresponding haloalkenes.

halodecarboxylation - Hunsdiecker reaction - Oxone - sodium halide - α,β-unsaturated aromatic carboxylic acid