Allylic Ethers as Educts for Aqueous Suzuki-Miyaura
Couplings

T. Nishikata; B. H. Lipshutz

doi:10.1055/s-0029-1218174

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Synfacts 2009(12): 1391-1391
DOI: 10.1055/s-0029-1218174

Metal-Mediated Synthesis

Allylic Ethers as Educts for Aqueous Suzuki-Miyaura Couplings

Contributor(s): Paul Knochel, Andreas J. Wagner
T. Nishikata, B. H. Lipshutz*
University of California, Santa Barbara, USA

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Publikationsverlauf

Publikationsdatum:
20. November 2009 (online)

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Significance

The first palladium-catalyzed Suzuki-Miyaura cross-coupling of functionalized allylic ethers is disclosed. It is conducted in water as the only medium and made possible by micellar catalysis by the non-ionic amphiphile PTS. Among a variety of screened ligands, DPEPhos turned out to be most efficient.