Synthesis

Issue 08 · June 2003

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review
1137
Merlic, Craig A.; Zechman, Andrea L.: Selectivity in Rhodium(II) Catalyzed Reactions of Diazo Compounds: Effects of Catalyst Electrophilicity, Diazo Substitution, and Substrate Substitution. From Chemoselectivity to Enantioselectivity

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short paper
1157
Inagaki, Tomotake; Fukuhara, Tsuyoshi; Hara, Shoji: Effective Fluorination Reaction with Et₃N˙3HF Under Microwave Irradiation

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1160
Braibante, Mara E. F.; Braibante, Hugo T. S.; da Roza, Juliano K.; Henriques, Danielle M.; de Carvalho Tavares, Luciana: Synthesis of Aminopyrazoles from α- Oxoketene O,N-Acetals Using Montmorillonite K-10/Ultrasound

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1163
Alcaide, Benito; Almendros, Pedro; Aragoncillo, Cristina; Rodríguez-Acebes, Raquel: New Aspects of the Indium Chemistry of Carbonyl-β-lactams

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1171
Xu, Ping; Zhang, Ting; Wang, Wenhao; Zou, Xiaomin; Zhang, Xin; Fu, Yiqiu: Synthesis of PNA Monomers and Dimers by Ugi Four-Component Reaction

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1177
Hu, Yimin; Zhou, Jie; Lian, Hongzhen; Zhu, Chengjian; Pan, Yi: Palladium-Catalyzed Cascade Cyclization of Benzyl Halides with Diethyl Diallylmalonate

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1181
Hasegawa, Tomoyuki; Yamamoto, Hisashi: Development of New Chiral Auxiliary Derived from (S)-(-)-Phenylethylamine for a Synthesis of Enantiopure (R)-2-Propyloctanoic Acid

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1187
Passaro, Linda C.; Webster, Francis X.: Synthesis of (9E,11Z)-Hexadeca-9,11-dienal, Sex Pheromone of the Pecan Nut Casebearer, Acrobasis nuxvorella (Neunzig)

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1191
Shevchenko, Nikolay E.; Nenajdenko, Valentine G.; Balenkova, Elizabeth S.: Triflic Anhydride-Promoted Cyclization of Sulfides: A Convenient Synthesis of Fused Sulfur Heterocycles

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1201
Karanik, Magdalena; Pätzel, Michael; Liebscher, Jürgen: Bicyclic Aminoalkyl N-Heterocycles by Ring-Chain-Transformation of Bridged 1,3-Dicarbonyl Heteroanalogues with Aminopyrazoles and Aminotriazole

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1209
Otto, Andreas; Liebscher, Jürgen: Synthesis of Hydroxyalkyl Heterocycles by Ring Transformation of Spiroepoxy Lactones with Binucleophiles

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1215
Geisler, Karlheinz; Pfeiffer, Wolf-Diethard; Müller, Cornelia; Nobst, Elvira; Bulka, Ehrenfried; Langer, Peter: Synthesis and Functionalization of 4-Halomethyl-1,3-selenazoles

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1221
Chevrier, Carine; Defoin, Albert: Simple Preparation of N-Benzyl-β-aminohydroxamic Acids by 1,3-Dipolar Cycloaddition of Nitrones

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1225
Barbero, Margherita; Degani, Iacopo; Dughera, Stefano; Fochi, Rita: An Improved, General Procedure to S-Aryl Thiol Esters: A New Synthetic Application of Dry Arenediazonium o-Benzenedisulfonimides

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1231
Wang, Quanrui; Li, Zheng; Yang, Haiyan; Li, Feng; Ding, Zongbiao; Tao, Fenggang: Annulated 1,2,4-Triazoles. A Convenient Synthesis of Thieno[2,3-f][1,2,4]triazolo[1,5-a]azepines: A Novel Triheterocyclic Ring System

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1236
Uchida, Hitoshi; Shimizu, Takashi; Reddy, Paidi Yella; Nakamura, Shuichi; Toru, Takeshi: Solvent-Free Efficient Synthesis of 2,4,5-Triarylimidazolines from Aromatic Aldehydes and Hexamethyldisilazane

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1241
Wang, Limin; Xia, Jianjun; Qin, Fang; Qian, Changtao; Sun, Jie: Yb(OTf)₃-Catalyzed One-Pot Synthesis of Quinazolin-4(3H)-ones from Anthranilic Acid, Amines and Ortho Esters (or Formic Acid) in Solvent-Free Conditions

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1248
Rodrigues, Alessandro; Vinhato, Elisângela; Rittner, Roberto; Olivato, Paulo Roberto: A Practical Synthesis of Diethyl 1-Methylthio-2-oxo-2-phenylethylphosphonates from Diethyl Methylthiomethylphosphonate

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1253
Schulz, Tobias; Eicher, Theophil: Synthesis of 1,6-Ansaglycosides

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1262
Zhu, Xiangming; Schmidt, Richard R.: Selective Conversion of N-Trichloroethoxycarbonyl (Troc) Groups into N-Acetyl Groups in the Presence of N-tert-Butoxycarbonyl (Boc) Protecting Groups

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1267
Sabitha, Gowravaram; Kumar Reddy, G. S. K.; Reddy, Ch. Srinivas; Fatima, Narjis; Yadav, J. S.: Zr(NO₃)₄: A Versatile Oxidizing Agent for Aromatization of Hantzsch 1,4-Dihydropyridines and 1,3,5-Trisubstituted Pyrazolines

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1272
Trofimov, Boris A.; Sobenina, Lyubov’ N.; Mikhaleva, Al’bina I.; Ushakov, Igor A.; Vakul’skaya, Tamara I.; Stepanova, Zinaida V.; Toryashinova, Dar’ya-Syren D.; Mal’kina, Anastasiya G.; Elokhina, Valentina N.: N- and C-Vinylation of Pyrroles with Disubstituted Activated Acetylenes

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1279
Mohr, Wolfgang; Horn, Clemens R.; Stahl, Jürgen; Gladysz, J. A.: Convenient and Convergent Syntheses of Long-Chain α,ω-Dibromides and Diphosphines of the Formula X(CH₂)_nX (n = 18-32)

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feature article
1286
Cravotto, Giancarlo; Nano, Gian Mario; Palmisano, Giovanni; Tagliapietra, Silvia: The Reactivity of 4-Hydroxycoumarin under Heterogeneous High-Intensity Sonochemical Conditions

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practical synthetic procedures
1292
Enders, Dieter; Breuer, Klaus; Kallfass, Ulrike; Balensiefer, Tim: Preparation and Application of 1,3,4-Triphenyl-4,5-dihydro-1H-1,2,4-triazol-5-ylidene, A Stable Carbene

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synthesis alerts
1296
Kocienski, P. J.: Synthesis Alerts 08/03 FREE ACCESS

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book review
1304
Hilt, G.: Catalysts for Fine Chemical Synthesis; Volume 1: Hydrolysis, Oxidation and Reduction FREE ACCESS

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1305
Harvey, J. E.: Titanium and Zirconium in Orgnanic Synthesis FREE ACCESS

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addendum
1306
Reger, D. L.; Gratten, T. C.: Synthesis of Modified Tris(pyrazolyl)methane Ligands: Backbone Functionalization FREE ACCESS

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