Synfacts

Issue 12 · December 2015

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A167
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Synthesis of Natural Products and Potential Drugs
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Synthesis of (–)-Incarviatone A FREE ACCESS

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Synthesis of NVP-CGM097

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Synthesis of LY2886721 FREE ACCESS

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Synthesis of Erlotinib

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Synthesis of Olmesartan Medoxomil

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1236
Total Synthesis of (±)-Goniomitine

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Total Synthesis of (+)-Batzelladine B

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1238
Synthesis of (S)-Pregabalin

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1239
Synthesis of (–)-Conolutinine

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1240
Synthesis of Silodosin

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1241
Synthesis of Leustroducsin B

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1242
Total Synthesis of (–)-Pallavicinin and (+)-Neopallavicinin

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1243
Synthesis of KAE609 via an Asymmetric aza-Diels–Alder Reaction

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1244
Synthesis of Pevonedistat

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1245
Total Syntheses of Rhodomyrtosones A and B

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Synthesis of Heterocycles
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1247
Synthesis of Highly Functionalized Oxetanes FREE ACCESS

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1248
Acid-Catalyzed Synthesis of Carbazoles from Indoles and 2-Amidodihydrofurans

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1249
Synthesis of Six- and Seven-Membered Heterocycles

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1250
Synthesis of 2-Aminoindoles and 5-Amino-indolo[1,2-a]quinazolines

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1251
Nickel-Catalyzed Anti-Markovnikov Hydroheteroarylation of Nonactivated Alkenes

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1252
Synthesis of Cyclic Ethers by Alkoxylation of Nonactivated sp³ C–H Bonds

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1253
Manganese(I)-Catalyzed C–H Bond Amidation of Heteroarenes

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1254
Silver-Catalyzed Synthesis of 2-Aryl-5-(trifluoromethyl)tetrazoles

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1255
Imidazotetrazolodiazepinones by a Ugi–Azide Multicomponent Reaction

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1256
Rhodium Carbenoid-Catalyzed Synthesis of 2,5-Epoxybenzo[f][1,4]oxazepines

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1257
Potassium Persulfate Mediated Synthesis of Dihydrofurans

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1258
Oxidative Radical Decarboxylation Route to 6-Alkyl- or 6-Arylphenanthridines

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1259
Radical-Mediated Difluoromethylenephosphonation

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1260
Highly Substituted Pyrimidines by Multicomponent Reactions

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1261
Synthesis of Tetrasubstituted Furopyridazinones from Nitrile Imines

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Synthesis of Materials and Unnatural Products
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1263
Two Steps to Porosity FREE ACCESS

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1264
2- and 6-Thienylazulenes by Direct Arylation

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1265
Aminocyclopropanation on Fullerene

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1266
Facile Method for the Synthesis of Dibenzo[g,p]chrysenes

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1267
[2+2+2] Cyclotrimerization in a Porous Coordination Framework

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1268
C–H Functionalization Furnishes Thieno-Fused Cycles and Heterocycles

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1269
Persistent COF: A Stable Platform for Asymmetric Organocatalysis

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1270
A New Class of Classical and Nonclassical Aggregation-Induced Emitters

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1271
Dimerized to Bend: Radilenes from Cumulenes

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1272
Electrophilic Borylation Leads to Efficient OLED Materials

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1273
High Mobility Conjugated Polymers through Direct Arylation

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1274
One Stone Two Birds with a NHC Sponge

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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1275
Ruthenium-Catalyzed Asymmetric Yne–Enone Cyclizations FREE ACCESS

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1276
Asymmetric Oxygen Atom Transfer to Oxindoles by Copper Catalysis

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1277
Asymmetric Gold(I)-Catalyzed [3+2] Cycloadditions

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1278
Tetrahydrofurans by Enantioselective Gold(I)-Catalyzed Desymmetrization of 1,3-Diols

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1279
Enantioselective Palladium-Catalyzed 1,1-Fluoroarylation

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1280
Asymmetric Alkoxycarbonylative Amination of Allenes

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1281
Scandium-Catalyzed Asymmetric Ring-Opening of Cyclopropanes

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1282
Diastereodivergent Asymmetric [4+2] Cycloaddition

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1283
Palladium-Catalyzed Enantioselective Synthesis of Chromans

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1284
Copper-Catalyzed Asymmetric Synthesis of 3,4-Diaminopyrrolidines

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1285
Enantioselective Synthesis of Pyrrolidine-thia(oxa)zolidinediones

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1286
Rhodium-Catalyzed Asymmetric Ring Opening of Oxabicycles

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1287
Enantioselective Palladium-Catalyzed Carboalkyoxylation Forming Tetrahydrofurans

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1288
8-Oxa-6-Azabicyclo[3.2.1]octanes by Asymmetric Copper-Catalyzed Iodocyclization

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1289
Asymmetric Copper-Catalyzed Propargylic Substitution

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1290
Rhodium(I)-Catalyzed Asymmetric 1,4-Addition of Boronic Acids to Cumarins

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1291
Transfer Hydrogenation with Chiral N-Heterocyclic Carbene/Iridium Complex

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1292
Enantioselective Fluorination of Allylic Trichloroacetimidates

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1293
Enantioselective Palladium-Catalyzed Ene Reaction and [2+2] Cyclization

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1294
Asymmetric Zinc-Catalyzed Synthesis of Polycyclic Spirooxindoles

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1295
Povarov Reaction Catalyzed by Anionic Chiral Cobalt(III) Complexes

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1296
Synthesis of trans-1,2-Diamine through Asymmetric Ring-Opening Reaction

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1297
Asymmetric Hydrophosphination of α,β,γ,δ-Unsaturated Ketones

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1298
Asymmetric Addition of Heteroarylboronates to Arylimines

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1299
Cobalt-Catalyzed Allylation and Asymmetric Ring-Opening of Heterobicyclic Alkenes

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1300
Enantioselective Copper-Catalyzed Synthesis of Benzofuranones

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1301
Enantioselective Intramolecular C–H Arylation of Cyclopropanes

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1302
Functionalized Furans by Asymmetric Gold-Catalyzed Intermolecular Annulation

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Metal-Mediated Synthesis
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1303
Asymmetric Bromine–Lithium Exchange

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1304
Diastereoselective Addition of Organozinc Reagents to 1,2-Anhydro Sugars

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1305
Enantioselective Bromocyclopropanation of Allylic Alcohols

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1306
Negishi Cross-Coupling of Aminotriazoles

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1307
Palladium-Catalyzed Carbofluoroalkylation FREE ACCESS

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1308
Zinc-Catalyzed Borylation

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1309
Enantioselective Homocrotylation of Aldehydes

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1310
Palladium-Catalyzed Alkylsulfonylation of Boronic Acids

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1311
Ruthenium-Catalyzed Cross-Coupling of Naphthamides

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1312
Nickel-Catalyzed Direct Borylation of Unactivated Fluoroarenes

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1313
Copper-Catalyzed Carboxylation of Alkenylzirconocenes

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1314
Silver-Catalyzed Diastereoselective Coupling

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1315
Trifluoromethylation of Carbonyl Compounds

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1316
Addition of Boronic Acids to Cyclic Sulfonylketimines

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1317
3-Substituted 2-Aminochromones by Tin(IV)-Promoted Annulation

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Organo- and Biocatalysis
z1319
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1319
Organocatalytic Photoredox C–H Amination of Arenes

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1320
1,6-Conjugate Addition of Pyrroles to para-Quinone Methides

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1321
Biocatalytic Hydrogen-Borrowing Amination of Ketones

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1322
Organocatalytic Carbonyl–Ene Cyclization

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1323
C–H Alkylation of Alcohols

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1324
The Mitsunobu Reaction Catalytic in Phosphine and Azodicarboxylate

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Polymer-Supported Synthesis
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1325
Silver-Foil-Catalyzed Cyclopropanation of Alkenes Under Mechanochemical Conditions

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1326
Bisoxazoline/Palladium Complex Microsphere Catalyzed Heck Reactions

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1327
Ullmann-Type Coupling of Phenols with Aryl Halides on Cuprian Zeolite USY FREE ACCESS

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1328
Cobalt Ferrite Nanoparticle Catalyzed Petasis–Borono–Mannich Reaction

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1329
Enantiospecific C–H Activation with Ruthenium Nanocatalysts

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1330
Microwave-Assisted Click Reaction Using Copper(I) Iodide on Alumina

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1331
C–C Bond Formation with Heterogeneous Lewis Acids in Aqueous Media

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1332
Oxidation of Alcohols by Using a Supported Manganese(lll) Salophen Complex

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1333
Solid-Phase Total Synthesis of Spiruchostatin A

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1334
Synthesis of Benzothiazoles by Using Piperazinylpyrimidine-Modified MCM-41

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1335
Zirconia–β-Cyclodextrin Catalyst for Synthesis of Substituted Imidazoles

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1336
Palladium/Carbon-Catalyzed Aminocarbonylation of Aryl Iodides

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1337
Copper/Manganese(II) Oxide Catalyzed ortho-Halogenation of 2-Arylpyridines

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1338
Multicomponent Synthesis of Dibenzo-diazepines with Iron(III) Tosylate/Silica

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1339
Sulfonated Carbon Nanotubes: A Supported Acid Catalyst for Pyrrole Synthesis

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1340
Synthesis of β-Enaminones by Using a Ag/γ-Fe₃O₄@meso-TiO₂ Nanocatalyst

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Erratum
1341
Prakash, G. K. S.; Rapp, A.; Munoz, S. B.; May, N.; Jones, J.-P.; Haiges, R.; Esteves, P. M.; Mathew, T.: Lewis Acid Catalyzed Synthesis of Di/Trifluoromethyl- 1,2,3,4-Tetrahydroquinazolines

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1341
Prakash, S.; Muralirajan, K; Cheng, C.-H.: Rhodium-Catalyzed Vinylation

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1342
Lao, J. R.; Fernández-Pérez, H.; Vidal-Ferran, A.: Kinetic Resolution of Vinyl Sulfoxides by Rhodium Catalysis

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PDF (98 kb)
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