Synfacts

Issue 10 · October 2018

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A153
SYNFORM ISSUE 2018/10 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
z0999
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0999
Synthesis of a Phosphoinositide 3-Kinase (PI3K) β Inhibitor FREE ACCESS

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1000
Synthesis of (–)-Dendrobine, (–)-Mubironine B, and (–)-Dendroxine

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1001
Asymmetric Total Synthesis of (+)-Aplysiasecosterol A FREE ACCESS

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1002
Synthesis of (–)-Septedine

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1003
Synthesis of AZD1656

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1004
Synthesis of (+)-Cyclocitrinol

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1005
Synthesis of (–)-Xishacorene B

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1006
Synthesis of BMS-978587

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1007
Synthesis of QCA570

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1008
Total Synthesis of (–)-Cycloclavine

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1009
Synthesis of Esomeprazole

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1010
Synthesis of GDC-0853

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1011
Synthesis of OV329

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1012
Total Synthesis of (–)-Actinophyllic Acid

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Synthesis of Heterocycles
z1013
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1013
Synthesis of Enantioenriched 1H/3H-Pyrroles and Pyrroloimidazoles

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1014
Indolo[3,2-c]coumarins and Benzofuro[3,2-c]quinolinones

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1015
Synthesis of Trifluoromethylated Pyrrolidine and Piperidine Amino Acids FREE ACCESS

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1016
Hypervalent Iodine Reagent for the Synthesis of 2-Substituted Indoles

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1017
Phosphonium Salts as Surrogates for Aromatic Carbon–Heteroatom Bond Formation

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1018
Scalable Synthesis of an exo-Triazolylazabicycle

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1019
Synthesis of Cyclic Ureas by a Cross-Metathesis/Aza-Michael Sequence

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1020
Synthesis of Quinolines through Double-Oxidative Dehydrogenative Cyclization

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1021
C5 Alkenylation of Imidazoles and the Synthesis of Benzimidazoles

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1022
Palladium-Mediated Stereoselective Synthesis of 3,4-Fused Indolines

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1023
Samarium(II) Iodide Mediated Synthesis of Five- and Six-Membered N-Heterocycles

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1024
Silver-Mediated Synthesis of Fluorinated Oxazolidinones

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1025
C4-Activated Arylation of Pyrrolidines and Piperidines

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1026
Pyranopyrimidine–Triazole Hybrid Molecules

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1027
Quinoline-4-carboxylic Acids and Esters from N,N-Dimethylenaminones and Isatins

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Synthesis of Materials and Unnatural Products
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1029
Lucky Seven-Membered Rings in N-Doped Nonplanar Nanographenes FREE ACCESS

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1030
One-Step Yamamoto Coupling of Benzophenes and Cyclooctatetraenes

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1031
Counting Up: One-, Two-, and Three-Boron Fused Oligo-Naphthalenes

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1032
No Rotation Allowed: Triply Fused Porphyrin–Nanographene Conjugates

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1033
All About That Strain: C–C Bond Activations of Cycloparaphenylenes by a Pt Complex

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1034
So Retro: Synthesis of Tribenzocarbazoles from Azapropellanes

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1035
To [n]Acenes and Beyond!

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1036
New End-Capping System for Solution-Processable Oligothiophenes

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1037
The Ramberg–Bäcklund Reaction Applied to Poly(arylene Vinylene) Synthesis

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1038
Diastereocontrol by Blocking Nitrogen Inversion in a Quinolino[3,2,1-k]Phenothiazine

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1039
Möbius Molecules

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1040
Flexibility in Macrocycles is Key for Better Electron Transport

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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1041
Asymmetric Decarboxylative Allylic Alkylation of Acyclic Enol Carbonates FREE ACCESS

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1042
Enantioselective Scandium-Catalyzed Formal [4+2] Cycloaddition

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1043
Enantioselective Intermolecular Ruthenium-Catalyzed Cycloaddition FREE ACCESS

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1044
Iridium-Catalyzed Reductive Coupling of Allyl Acetates with Ynals

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1045
C₂-Symmetric Chiral Biscyclosulfinamide–Olefin Ligand

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1046
Scandium-Catalyzed Enantioselective Ring-Opening of Cyclopropyl Ketones with Indoles

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1047
Asymmetric Synthesis of 2,2,3-Trisubstituted Indolines

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1048
Ytterbium-Catalyzed [4+2] Cycloaddition of Cyclobutenones with α-Keto Esters

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1049
Copper-Catalyzed Asymmetric Synthesis of Spirocyclic β-Lactams

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1050
Oxaspirocyclic Ligands for Iridium-Catalyzed Asymmetric Reduction

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1051
Enantioselective Ruthenium(II)-NHC Catalyzed Hydrogenation of 2-Oxazolones

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1052
Copper-Catalyzed Synthesis of Enantioenriched 1,2-Hydroxyboronates

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1053
Iridium/Copper-Catalyzed Asymmetric Radical Cyanoalkylation of Styrenes

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1054
Palladium–Amine-Catalyzed Enantioselective α-Allylation of Ketones

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1055
Cobalt-Catalyzed Enantioselective Nazarov Cyclization/Fluorination Cascade

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1056
Enantioselective Synthesis of Spirooxindole-thiaindans by Cooperative Catalysis

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1057
Gold-Catalyzed Stereoselective Synthesis of β-Fluoro Michael Acceptors

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1058
Reductive Asymmetric Ring-Opening of Azabenzonorbornadienes

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1059
Enantioselective Transfer Hydrogenation of Alkynyl Ketones

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1060
Asymmetric Heck–Matsuda Carbonylation

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1061
Fluoroalkylamines as Nucleophiles in Iridium-Catalyzed Ring Opening

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1062
Palladium-Catalyzed Asymmetric [4+2] Cycloaddition

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1063
Asymmetric Dearomative [3+2] Cycloaddition by Zinc Catalysis

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1064
Catalytic Diastereoselective Multi-Component Cyclopropanation

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1065
Palladium-Catalyzed Asymmetric Rearrangement of Allyl Enol Ethers

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1066
Enantioselective Iridium-Catalyzed Vinylogous Allylic Alkylation of Coumarins

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1067
Diastereoselective Intermolecular Semipinacol Rearrangement

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1068
Rhodium-Catalyzed Asymmetric Synthesis of Tertiary α-Hydroxy Esters

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1069
Enantioselecitve [3+2] Cycloaddition of Aurones with Isocyanoacetates

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1070
Palladium-Catalyzed Enantioselective Allylic C–H Alkylation of 1,4-Pentadienes

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Metal-Mediated Synthesis
z1071
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1071
Asymmetric Synthesis of Vinyl Aziridines

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1072
Intramolecular Glycosyl Stille Cross-Coupling

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1073
meta-Arylation of Fluoroarenes

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1074
Redox-Neutral C–H Olefination Catalyzed by Manganese

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1075
Direct Reaction of Grignard Reagents with Isocyanates in Flow

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1076
Transition-Metal-Free Amination and Etherification of Aryl Alkyl Thioethers

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1077
Iron–Nickel Dual-Catalytic Olefin Functionalization

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1078
Mechanochemical Generation of Organozinc Compounds

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1079
Copper-Catalyzed Trifluoromethylation of Alkyl Iodides

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1080
Selective Monomethylation of Arylacetonitriles and Arylacetamides

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1081
Cobalt-Catalyzed Ring-Opening Coupling of Cyclopropanols with Alkynes

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1082
Copper Iminoarylsulfonate Complex Catalyzed Amination

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1083
Diastereodivergent Hydroarylation of Terminal Alkynes

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1084
Generation of Strained Azacyclic Allenes for Diels–Alder Cycloadditions

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1085
Defluoroalkylation of gem-Difluoroalkenes via Zinc

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Organo- and Biocatalysis
z1087
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1087
Dynamic Kinetic Resolution of Azlactones with a Chiral DMAP Catalyst

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1088
Acid-Catalyzed Rearrangement of Hydroxylated Pinene Derivatives

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1089
Activating Ketones with Low Catalyst Loadings of a Potent Chiral Lewis Acid FREE ACCESS

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1090
Phosphoric Acid Catalyzed Aldehyde Addition to o-Quinone Methides

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1091
Enantioconvergent Biocatalytic Redoxisomerization of Pyranones

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1092
Triazolium-Salt-Catalyzed Dialkylation of Bisoxindoles

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1093
Enzymatic Control of the Stereochemical Course of [4+2] Cycloaddition

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1094
Chiral-Aldehyde-Catalyzed α-Functionalization of Glycine Esters

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1095
Fluorobissulfonylmethyl Iodides as Lewis Acid Catalysts

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1096
Biocatalytic Production of Linear α-Olefins from Carboxylic Acids

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Polymer-Supported Synthesis
z1097
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1097
Formylation of Amines with CO₂ Using a Polymeric Frustrated Lewis Pair FREE ACCESS

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1098
Hf-Based Metal–Organic Framework-Catalyzed Aldol Condensation and Hydrogenation

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1099
Amidation of Amines with Carboxylic Acids Catalyzed by a Metal–Organic Framework

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1100
Transfer Hydrogenation of Nitroarenes on Carbon-Coated Cobalt Nanoparticles

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1101
Photocatalytic Deoxygenation of Sulfoxides and Pyridine N-Oxides

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1102
Cyclic Carbonates from CO₂ and Epoxides on a Supported Imidazole Catalyst

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1103
1,4-Addition of Grignard Reagents to Chalcones on MS 4Å-Supported CuCl₂

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1104
Suzuki–Miyaura Coupling on Water-Soluble Fullerene-Supported PdCl₂

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1105
Controlled Hydrogenation of Alkynes on Bimetallic Gold/Palladium Nanoparticles

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1106
Ring-Opening Diborylation of Cyclopropanes on Nanoporous Gold

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1107
Synthesis of Symmetric Carboxylic Anhydrides from Aldehydes on a Cu-MOF

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Addendum
1108
Hydrogen-Bonding Phase-Transfer Catalyst Enabled Asymmetric Fluorination

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