Synfacts

Issue 01 · January 2019

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SYNFORM ISSUE 2019/01 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
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Synthesis of Isopalhinine A and Palhinine D FREE ACCESS

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0002
Enantioselective Syntheses of Divergolides E and H

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Synthesis of Beclabuvir FREE ACCESS

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Synthesis of an Atropisomer of Schiglautone A

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Synthesis of Efavirenz via Asymmetric Alkynylation FREE ACCESS

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0006
Synthesis of (±)-Repraesentin F

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0007
Synthesis of Prostaglandins F_2α and E₂ FREE ACCESS

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0008
Synthesis of Flibanserin

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0009
Total Synthesis of (+)–Chaetoglobin A

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0010
Synthesis of BMS-214662

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Synthesis of Cefiderocol

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Synthesis of Quetiapine via Cobalt-Catalyzed C–H Thiolation

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Total Synthesis of Brasilicardins A–D

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Synthesis of Heterocycles
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Synthesis of N-Doped Polycyclic Aromatic Hydrocarbons

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0016
Organocatalytic Approach to cis-Octahydroacridines

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0017
Synthesis of Perfluoroalkylated Spirobarbiturates

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0018
Iridium-Catalyzed C–H Alkenylations: Synthesis of 3-Alkylisobenzofuran-1(3H)-ones

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0019
Reaction of Cyclobutanones with Allenylsilanes to form Oxabicyclo[3.2.1]octanes

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Photocatalytic Synthesis of 8- to 11-Membered Lactams by C–C Bond Cleavage

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Multicomponent Reaction Approach to Aza Analogues of Tropane Alkaloids

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Functionalized 2H-Isoindoles by Rhodium-Catalyzed C–H Activation

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Metallophotoredox-Catalyzed C–H Arylation of C(sp³)–H Bonds

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Ionic-Liquid-Mediated Syntheses of Fused Pyrimidines and Quinazolines

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Carbocyclization through an Interrupted Carbonyl–Olefin Metathesis

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Synthesis of Pyrrolopyrazinones from N-Substituted 2-Cyanopyrroles

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0027
Synthesis of 2‑Aminoquinolines from N‑Acyl‑o‑alkynylanilines

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Borane-Catalyzed Synthesis of Azasilaheterocycles

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One-Pot Synthesis of Isoquinolinones by Rhodium-Catalyzed C–H Activation

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Synthesis of Materials and Unnatural Products
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Catalytic, Oxidative Alkene Arylation for Polycyclic Aromatic Hydrocarbons

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Synthesis of Corannulenes Revisited FREE ACCESS

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Endo, Exo, and What? FREE ACCESS

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0034
Sequence-Regulated Synthetic Polymers are Just a Few Clicks Away

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0035
Some Like It Branched: Fluorous Tags for Enhanced Solubility and Biocompatibility

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Construction of Axial Chirality by Intramolecular Consecutive Dehydro-Diels–Alder Reaction

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One-Pot, Multicomponent Synthesis of Helical Quinolines

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Not so Boring Boron: C-Halogenated 9,10-Diboraantharcenes

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Breaking Up Kekulene, Resulting in π-Expanded Helicene

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Modular Route to N-Substituted peri-Xanthenoxanthene Mono- and Diimides

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0041
Ring-Opening Metathesis Oligomerization to Close Macromolecular Cages

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0042
Synthesis of a Photoisomerizable Bis-cyclooctyne Cross-Linker

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Metals in Synthesis
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0043
C–C Bond Formation Using Nickel-Photoredox Catalysis FREE ACCESS

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0044
Palladium Catalyzed Enantioselective α-Allylation of Aryl Acetic Acids

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0045
Enantioselective Palladium-Catalyzed Dearomative Heck Reaction FREE ACCESS

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0046
Photochemical Gold-Catalyzed Arylations

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0047
Biaryl Ligands for C–N Coupling FREE ACCESS

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0048
Palladium-Catalyzed Domino Ring-Opening/Spirocyclization Process

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0049
The First Csp²–Csp² Cross-Coupling Using Organozinc Reagents FREE ACCESS

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0050
Rhodium-Catalyzed Allylic C–H Etherification

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0051
Iridium-Catalyzed Alkylations of Aromatic Aldehydes

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0052
para-Selective Difluoromethylation of Aromatic Ketones

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0053
Rhodium-Catalyzed Kinetic Resolution of Homoallylic Secondary Alcohols

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0054
Copper-Catalyzed Radical Cross-Coupling Multicomponent Reaction

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0055
Rhodium(III) C–H Activation Combined with N- and C-Annulations

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0056
Enantioselective Addition of Chiral Metal Enolates to ortho-Quinone Methides

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0057
Simple and Environmentally Friendly Synthesis of Amides

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0058
Enantioselective Alkylation of Imines via Copper-Catalyzed Asymmetric Photoredox

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0059
Nickel-Catalyzed Suzuki–Miyaura Reaction with no Exogenous Base

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0060
Copper-Catalyzed Dichloromethylation and Subsequent Azide Trap

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0061
A Nickel-Catalyzed Photoredox Tsuji–Trost Reaction

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0062
Nickel-Catalyzed Alkylation using Anhydrides

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0063
Iodine Atom Transfer Catalysis via Ketyl Radicals

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0064
Iron-Catalyzed Carbenoid Transfer Heterocycle Synthesis

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0065
Iridium-Photocatalyzed Synthesis of Complex Alkylamines

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0066
Reductive Coupling of Tertiary Alkyl Halides and Electron-Rich Aryl Iodides

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0067
Enantioselective Intramolecular Dearomative Allylic Alkylation

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0068
Suzuki–Miyaura Cross-Coupling of Dimethyl Aryl Amines

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0069
Palladium-Catalyzed Allylations Using Hydrazones as Carbanion Surrogates

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Ruthenium-Catalyzed Photoredox Alkylamination

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Polymer-Supported Synthesis
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Desilylative or Decarboxylative Photoadditions with Graphitic Carbon Nitride FREE ACCESS

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0072
N-Formylation of Amines Catalyzed by Self-Supported N-Heterocyclic Carbene–Iridium

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0073
Reductive Amination and Hydroaminomethylation with a Bifunctional Catalyst

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0074
Synthesis of Pyrroles from 3,6-Dihydro-2H-1,2-oxazines on Cu/C

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0075
Hydrogenation of Pyridines on Titania-Supported Cobalt Nanoparticles

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0076
Graphene Oxide Catalyzed Synthesis of Spiropyrrolizines

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0077
Photocatalytic Aerobic Oxidation of Alkylaromatics on Pt/Bi₂MoO₆

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0078
Reduction of Nitroarenes to Azoarenes on Cage-Encapsulated Gold Nanoparticles

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0079
Molybdenum Sulfide-Mediated C–H Arylation of Heteroarenes with Arenediazonium Salts

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0080
Synthesis of Benzoxanthenes and Pyrroles on a Supported Lewis Acidic Ionic Liquid

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0081
Asymmetric Fluorination on a Polystyrene-Supported Copper Complex

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0082
Reduction of Nitroarenes on N-Doped Porous Carbon-Supported Cobalt

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Organo- and Biocatalysis
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0083
Chiral Lewis Base Catalyzed Aldol Reaction of Unprotected Carboxylic Acids FREE ACCESS

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0084
Stereodynamic Redox-Interconversion Network of Hybrid Dihydrobenzofurans

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0085
The Dawn of Directed Evolution FREE ACCESS

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0086
Bienzymatic Oxidative Lactamization of Aliphatic Amino Alcohols

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0087
Carbon–Fluorine Bond Cleavage by an Engineered Enzyme

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0088
Reductive C–N Cross-Coupling of Nitroarenes by P^III/P^V=O Catalysis

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0089
Cinchona-Amine-Catalyzed Stepwise [6+4] Cycloadditions

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0090
Catalytic Diels–Alder Reaction of α,β-Unsaturated Methyl Esters

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0091
Organocatalytic Synthesis of γ,γ-Disubstituted Butenolides

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0092
From CO₂ to Cyclic Carbonates: Organocatalysts Do It under Mild Conditions

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0093
Improved Efficiency with New Cinchona-Based Catalysts in Umpolung Reactions

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Peptide Chemistry
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0095
Stereoselective Synthesis of α-Aryl Amino Acids FREE ACCESS

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0096
Peptide Macrocyclization by Palladium-Catalyzed δ-C(sp²)–H Olefination

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0097
Synthesis of Backbone-Engineered HIV Protease by Selective Chemical Ligation FREE ACCESS

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0098
Direct Peptide Synthesis via N-Acyl Imidazolium Intermediates

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0099
2,4-Bis(trifluoromethyl)phenylboronic Acid Catalyzed Amidation

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0100
Modified Yamaguchi Reagent Mediated Coupling Reactions

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0101
Tris(2,2,2-Trifluoroethyl) Borate Catalyzed, Protecting-Group-Free Amidation

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0102
Native Chemical Ligation by Flow Chemistry

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Flow Chemistry
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0103
Synthesis of Substituted Allylic Alcohols in Continuous Flow under UV-Light

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0104
A Catalytic Hydrogenation of Arenes: Batch versus Flow

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0105
Versatile Flow-Based Automatic Reaction Optimization Platform

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0106
Continuous Flow Synthesis of Eflornithine

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0107
Continuous-Flow Synthesis of Amines and Hydroxylamines

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0108
Chloroacetate Claisen Reactions in Continuous Flow

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