Synfacts

Issue 02 · February 2019

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Synform
A16
SYNFORM ISSUE 2019/02
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Synthesis of Natural Products and Potential Drugs
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0109
Total Synthesis of Saxitoxin and 11-Saxitoxinethanoic Acid
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0110
Total Synthesis of (–)-Myrocin G

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0111
Synthesis of Grazoprevir
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0112
Synthesis of Crizotinib and Etoricoxib

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0113
Synthesis of Penicillin V
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0114
Synthesis of (+)-Darwinolide

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0115
Formal Synthesis of Rhizoxin D

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0116
Asymmetric Copper-Catalyzed Hydroamination: Maraviroc

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0117
Synthesis of Heterobiaryls by Contractive C–C Coupling

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0118
Synthesis of AZD6738

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0119
Synthesis of (–)-Mitrephorone A

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0120
Total Syntheses of Abies Sesquiterpenoids

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Synthesis of Heterocycles
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0121
Photochemical Cyclopropanation of Indoles

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0122
Visible-Light-Mediated Minisci C–H Alkylation with Dioxygen as Oxidant

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0123
Orthogonal Cross-Coupling of a Trifluoromethylated Chromenone Framework

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0124
N-Heterocyclic Carbene Catalyzed Synthesis of Substituted Oxetanes

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0125
Photocatalytic γ-Lactam Synthesis by Using Carbon Dioxide Activated Amines

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0126
Iron-Catalyzed Synthesis of Fluoroalkylated 2H-Azirines from Alkynes

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0127
Synthesis of Trifluoromethylated Pyrroles from Azirines

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0128
Stereoselective Synthesis of Tetrahydro-1-benzazepines through [4+3] Annulation

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0129
Synthesis of Azepines from 1,2,3-Triazoles and 1,3-Dienes

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0130
[3+2]-Cycloaddition Route to Imidazoles and Imidazolines

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0131
Annulation of Sulfoximines with Diazo Compounds

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0132
Enantioselective Synthesis of 4,9-Dihydrothiopyrano[2,3-b]indol-2(3H)-ones

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0133
Carbene-Catalyzed Synthesis of Pyrrolo[3,2-c]quinolines

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Synthesis of Materials and Unnatural Products
z0135
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0135
1,3a,6a-Triazapentalene Systems: Towards Extended Planar Materials
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0136
Tris-[5]helicenes with a Twist

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0137
Let Me Tell You a Mild Synthesis of Tellurides

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0138
M&M Cascade Polymerization Yields a Palette of Polyenynes

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0139
Tunable Indolo[3,2-b]carbazole-Based Boron Complexes

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0140
Merging C–H Activation and Radical Chemistry to Construct Polysubstituted Carbohelicenes

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0141
Selective Synthesis of Asymmetric Electron-Deficient π-Conjugated Systems

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0142
Mix and Match: PAH Synthesis

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0143
There’s Node Stopping It

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0144
Synthesizing Cross-Conjugated Polymers through Cross-Coupling

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0145
A Rainbow of Fluorescent Thieno[3,2-b]pyridine-5(4H)-ones

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0146
Efficient Singlet Fission in a Pentacene-Based Nanotube

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Metals in Synthesis
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0147
Diastereo- and Enantioselective Conjunctive Cross-Coupling via a Metalate Shift
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0148
Rhodium-Catalyzed Cleavage of Aryl–Aryl Bonds

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0149
Enantioselective α-Functionalization of Ketones
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0150
Lewis Acid Catalyzed Hydroboration of Alkynes and Alkenes

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0151
Ruthenium-Catalyzed Enantioselective Transfer Hydrogenation
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0152
Regio- and Enantioselective Haloazidation of Allylic Alcohols

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0153
1,2-Reduction of Conjugated Ketones: The Luche Reduction
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0154
Synthesis of Complex Polycycles through a Samarium(II)-Mediated Folding Cascade

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0155
Enantiodivergent Palladium-Catalyzed Cross-Couplings

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0156
Catellani Reaction in Tandem with a CMD-Type Process

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0157
Ruthenium-Catalyzed Late-Stage Oxygenation

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0158
Palladium-Catalyzed Ligand-Controlled Regioselective Acylation

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0159
Decarboxylative Heck Coupling via a Cobalt/Photoredox Catalysis

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0160
Acetonitrile as CN-Source in Nickel(0)-Catalyzed Cyanation

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0161
Palladium/Lewis Acid-Catalyzed Transfer Hydrocyanation of Alkenes and Alkynes

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0162
Metal-Catalyzed Oxa[4+2] Cyclization of Quinone Methides with Alkynyl Benzyl Alcohols

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0163
Synthesis of Chiral Alkylboronic Esters via Carbosulfenylation

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0164
Synthesis of (E)-3-Arylmethyleneisoindolin-1-ones via Palladium(II)/Copper(II) Catalysis

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0165
Copper-Catalyzed S_N2′′ Substitution of Penta-2,4-Dienyl Phosphates

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0166
Defluorinative Alkylation using Redox-Active Esters

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0167
Domino Synthesis of α,β-Unsaturated γ-Lactams

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0168
Ruthenium-Catalyzed Amide Arylation Using Arylboronic Esters

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0169
Palladium-Catalyzed C–H Alkenylation of Arenes Gives Alkenyl Chlorides or Trisubstituted Alkenes

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0170
New Access to Trifluoromethylated Ketones

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0171
Copper-Catalyzed Remote Arylation

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0172
Enantioselective Palladium(II)-Catalyzed Synthesis of 1,2,3,4-Tetrahydro-β-Carbolines

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0173
Mild Platinum-Catalyzed Process to Desaturate Lactams, Ketones, and Lactones

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0174
Synthesis of Chiral Tetrahydrofurans via Palladium and Squaramide Cooperative Catalysis

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0175
Dibenzo[b,d]oxepines by Olefinic C–F Bond Functionalization and Intramolecular Pd–Catalyzed C–H Activation

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Polymer-Supported Synthesis
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0177
Hydrosilylation of Alkenes Catalyzed by Platinum on N-Doped Graphene
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0178
Alkyne Homocoupling on Carbon Nitride-Supported PdAu Nanocrystals

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0179
Reduction of Nitroarenes Catalyzed by a Carbon-Supported Iron Catalyst

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0180
Hydrogenation of Cyano and Nitro Compounds by Using Cobalt Nanoparticles on Carbon

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0181
Oxidative C–H Chalcogenation of (Het)aryl-Fused Cyclic Amines on Cobalt Oxide Nanoparticles

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0182
Nucleophilic Substitution of Naphthols with a Supported Eutectic Solvent Catalyst

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0183
Chan–Lam Coupling on a Copper/Covalent Organic Framework Catalyst

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0184
Aza-Michael Addition Catalyzed by Encapsulated Magnetite–Hexamethylenetetramine

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0185
Selective Hydrogenation of Nitroarenes on Supported Palladium Nanoparticles

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0186
Heterogeneous Suzuki Coupling/Asymmetric Transfer Hydrogenation Tandem Reaction

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0187
Oxidation of Alcohols on a Supported Schiff Base–Molybdenum(VI) Complex

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0188
Formylation of Amines with CO₂ by Using a Polymeric N-Heterocyclic Carbene

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0189
α-Alkylation of Ketones and Alcohols with a Heterogeneous Zirconium Catalyst

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Organo- and Biocatalysis
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0191
Catalytic Asymmetric Mukaiyama Aldol Reaction of Acetaldehyde Enolates
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0192
Enantioselective Four-Atom Ring Expansion of Cyclobutanones

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0193
Catalytic Asymmetric α-Hydroxylation of Cyclic α-Branched Ketones

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0194
Brønsted Acid Catalyzed Diastereoselective [4+3] Cycloaddition

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0195
Photoredox-Catalyzed Multicomponent Alkyl Radical Carbonylation

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0196
Chiral Sulfides as Catalysts for Asymmetric Electrophilic Olefin Chlorination

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0197
A Double Umpolung Reaction to Synthesize β-Amino Amides

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0198
Photoredox-Catalyzed Difunctionalization of Olefins with Carbon Dioxide

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0199
Enantioselective Photoorganocatalytic Synthesis of 1,4-Dicarbonyl Compounds

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0200
The Hajos–Parrish–Eder–Sauer–Wiechert Reaction
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Peptide Chemistry
z0201
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0201
A Catalytic One-Step Synthesis of Peptide Thioacids

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0202
Extension of Native Chemical Ligation
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0203
Native Chemical Ligation by Microflow Chemistry
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0204
(4-Mercaptophenyl)acetic Acid-Promoted One-Pot Multiple Peptide Ligation

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0205
Palladium-Catalyzed C(sp³)–H Activation of Amino Acids and Peptide

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0206
Synthesis of Palmitoylated Sonic Hedgehog by Native Chemical Ligation

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0207
Nickel-Catalyzed Innate Radical Coupling Reaction

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0208
Copper-Catalyzed C(sp³)–H Direct Fluorination of Amino Acids

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Flow Chemistry
z0209
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0209
Photoredox Arylation of Enol Acetates via Porphyrin Catalysis

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0210
C–H Functionalization of Aldehydes with Photolabile Diazo Precursors

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0211
Continuous Alcohol Amination by a Hydrogen-Borrowing Protocol

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0212
Generation and Cross-Coupling of Organozinc Reagents in Flow

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0213
Morita–Baylis–Hillman Reaction under Continuous-Flow Conditions

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Erratum
0214
A New Isocyanide Functionalization
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