Synfacts

Ausgabe 12 · Dezember 2020

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Ausgabe
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A171
SYNFORM ISSUE 2020/12 FREIER ZUGRIFF

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Synthesis of Natural Products and Potential Drugs
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1383
Total Synthesis of (±)-Tronocarpine FREIER ZUGRIFF

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1384
Synthesis of a Remdesivir Intermediate

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1385
Synthesis of Olodanrigan FREIER ZUGRIFF

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1386
Synthesis of (±)-Liangshanone

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1387
Total Synthesis of (+)-Formosalides A and B

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1388
Synthesis of Ritobegron Ethyl Hydrochloride

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1389
Synthesis of MK-5204

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1390
Enantioselective Synthesis of (–)-Deoxoapodine

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1391
Synthesis of (–)-Flueggenines D and I

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1392
Synthesis of BMS-986235/LAR-1219

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1393
Asymmetric Synthesis of an hNK₁ Inhibitor

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1394
Synthesis of A-1331852

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1395
Formal Synthesis of (–)-Quinine FREIER ZUGRIFF

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1396
Total Synthesis of (+)-Jolantidine

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Synthesis of Heterocycles
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1397
Iodine/Trifluoroacetic Acid-Assisted Multicomponent Synthesis of 4(3H)-Quinazolinones

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1398
Electrocatalytic Decarboxylative Synthesis of 1,3,4-Oxadiazoles

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1399
Tuning Redox Properties of Bistetronates through Spacer Selection

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1400
Stereoselective Synthesis of Cyclopenta[c]pyrazoles by an Interrupted Ohira–Bestmann Reaction

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1401
Hypervalent Iodine(III)-Mediated Synthesis of Spirooxazolines

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1402
Regioselective C–H Arylation of Quinolone Derivatives

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1403
Synthesis of Oxygen-Rich Polycyclic Scaffolds

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1404
[4+1]-Spiroannulation of Bromophenols with α,β-Unsaturated Imines: Synthesis of Azaspirocycles

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1405
Cobalt-Catalyzed Synthesis of Pyrroles from Nitroarenes

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1406
Synthesis of 1,3,4,11-Tetrahydrooxocino[3,4-b]indoles

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1407
Synthesis of 1,2,3-Benzothiazaphosphole 1,1-Dioxides

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1408
Diverse Syntheses of Furochromone-Based Antimicrobial Agents

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1409
Asymmetric Synthesis of Spiro-Benzofurans and Fused Benzopyrans

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Synthesis of Materials and Unnatural Products
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1411
Peeling Carbon Onions

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1412
Mechanochemistry at its Best! An Improved Synthesis of Corannulene-Based Nanographene

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1413
Extended Porphyrins Containing One or Two Naphthalimide Subunits

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1414
Dioxa[6]helicenes, Expedited

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1415
Naphthalene Diimides with Fused Sulfur Heterocycles

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1416
Metal-Free Synthesis of 7-Hydroxy-6H-naphtho[2,3-c]coumarins

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1417
In with the Old, Out with the New: Homologation of Fischer Indolization to Synthesize Quinolines

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1418
Pick Your Own (Regioselective) Addition

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1419
Expanding the Library of Cationic [5]Helicenes

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1420
Working the Strain Off Cyclooctadiene-Diynes to Scale-Up Cyclic Polymer Synthesis

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1421
Synthesis of a Condensed Phenoxazine Dimer and Its Radical Cation Salt

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1422
Unsymmetrical Diarylation of Perylene Diimides

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Metals in Synthesis
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1423
Deoxygenation and Borylation of Ketones via Rhodium Catalysis FREIER ZUGRIFF

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1424
Regiodivergent Hydrofunctionalization of α,β-Unsaturated Carboxylic Acids

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1425
Asymmetric Synthesis of Amino Alcohols Using a Catalytically Formed Chiral Auxiliary FREIER ZUGRIFF

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1426
Direct Chlorination of Acrylamide Derivatives

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1427
α-Alkylation of Unprotected Alicyclic Amines

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1428
Manganese-PN³ Catalyst Generating Tetrahydro-quinolines via a Hydrogen-Borrowing Mechanism

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1429
Aza-Paternò–Büchi Reaction for Synthesis of Fused Azetidines

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1430
Ruthenium-Catalyzed C(sp³)–H Bond Oxygenation of N-Benzoyloxycarbamates

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1431
Air-Stable Palladium(I) Dimer for Olefin Migration and C–C Coupling

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1432
Ligand-Free Regioselective Iron-Catalyzed Hydroboration of Terminal Alkenes

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1433
Remote Catalytic Reductive C–H Carboxylation of Arenes with CO₂ via 1,4-Nickel Migration

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1434
Copper-Catalyzed C–N Cross-Coupling of Sterically Hindered Aryl Halides and Amines

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1435
Iron-Catalyzed Preparation of Sulfinamides from Thiols

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1436
Rhodium-Catalyzed Preparation of Pyrrolidines from Primary Amines

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1437
Iridium-Catalyzed Asymmetric Synthesis of 1,2-Fluorohydrins

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1438
Direct and Selective Palladium-Catalyzed Carbonylation of Allylic Alcohols

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1439
Accessing (Multi)Fluorinated Piperidines Using Heterogeneous Hydrogenation

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1440
Enantioselective [4+1] Cycloaddition by a Dinuclear Nickel Catalyst

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1441
Nickel-Catalyzed Enantioselective Migratory Hydrocyanation of Nonconjugated Dienes

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1442
Enantioconvergent Coupling of Racemic Alkyl Bromides with Azole C–H Bonds

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1443
Titanium-Catalyzed Deoxygenative Radical C−C Bond-Forming Reaction of Tertiary Alcohols

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1444
Palladium-Catalyzed Synthesis of Coumarins with β-Borylacrylates

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1445
Migratory Cross-Coupling of Alkyl Halides via Nickel Catalysis

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1446
α-C–H Alkynylation of N‑Alkylamines by Copper/Lewis Acid Catalysis

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1447
para-Selective Arylation via Norbornene Relay Palladation

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1448
Electrophotocatalytic Azidation of C(sp³)–H Bonds

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1449
Nickel-Catalyzed Defluorination of Aromatic Amides

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1450
Regioselective Markovnikov Cobalt-Catalyzed Hydroboration of Alkynes

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1451
Cross-Coupling of Organosilanes with Organic Halides Mediated by Palladium Catalyst and TASF FREIER ZUGRIFF

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Polymer-Supported Synthesis
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1453
One-Pot Two-Step Catalytic Asymmetric Michael Addition/Hydrogenation FREIER ZUGRIFF

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1454
Photocatalytic Pinacol Coupling of Benzaldehydes Using ZnIn₂S₄ Nanosheets

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1455
Heterogeneous Ruthenium/Tungsten-Catalyzed One-Pot Reductive Amination of Carboxylic Acids

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1456
Indenoquinoxalines Synthesis on Chitosan-Modified MnFe₂O₄ Magnetic Nanoparticles

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1457
Hydrogenation of N-Hetarenes on Silica-Supported Cobalt/Carboxylic Acid Nanoparticles

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1458
Synthesis of Benzimidazoles and Benzothiazoles on Pt NPs Supported on a Sulfur-Containing Dendrimer

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1459
Decarboxylative Alkynylation of Carboxylic Acid Promoted by Graphitic Carbon Nitride

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1460
Ruthenium/Magnesium Oxide-Catalyzed Direct Amination of Alcohols with Ammonia

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1461
Gold-Catalyzed Carboxylation and Hydration of Terminal Aralkynes

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1462
Aromatic Hydrogenation under Ambient Conditions

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Organo- and Biocatalysis
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1463
A Selenium-Catalyzed Oxidative Allylic Sulfonamidation FREIER ZUGRIFF

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1464
Organic Photocatalyzed Radical–Radical Cross-Coupling toward Heteroarylamines

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1465
Organophotoredox-Catalyzed Reductive Cleavage of Oxidized Lignin Model Substrates

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1466
Enantioselective Acylation of 3-Hydroxyphthalides by Pyrrolomidazole-Catalyzed Dynamic Kinetic Resolution

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1467
Radical-Cation-Accelerated Nucleophilic Aromatic Substitution of Electron-Rich Aryl Fluorides

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1468
Tandem Catalytic Dynamic Kinetic Resolutions toward Two-Axis Atropisomers

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1469
Ene-Reductase Permits Asymmetric Reductive Cyclization via Photoenzymatic Generation of Radicals

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1470
Chiral Confinement Permits Enantiocontrolled Reactions To Proceed via Nonclassical Carbocations

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1471
P(III)/P(V)-Catalyzed Reductive Methylamination of Arylboronic Acids and Esters with Nitromethane

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1472
Asymmetric 1,4-Reduction of 2-Vinylazaarenes with Pinacolborane

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1473
Carbocationic Rearrangements: Aryl-Iodide-Catalyzed Enantioselective Synthesis of 1,3-Difluorides

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Chemistry in Medicine and Biology
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1475
Next Generation Vancomycin Total Synthesis FREIER ZUGRIFF

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1476
Introducing a Chiral Tricycle that Renders a Selective JAK Inhibitor

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1477
Overcoming Vat Resistance with de Novo Synthesis of New Group A Streptogramin Analogues

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1478
Radical Difluorination

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1479
Local Labeling of Lipids

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1480
Diversity-Oriented Synthesis of Acylphloroglucinol Scaffolds

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1481
First Simultaneous Removal of SIRT2 Deacetylase and Defatty-Acylase Activities with PROTACs

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1482
A New Generation of Molecular Imaging Probes for Carbon Monoxide Detection in Living Systems

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1483
Optical Control of the Peroxisome Proliferator-Activated Receptor γ (PPARγ)

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1484
Stereoselective Covalent Inhibitors of T-Cell Activation

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1485
Progesterone from Mexican Yams FREIER ZUGRIFF

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1486
Sulfuramidimidoyl Fluorides as SuFEx Electrophiles for the Inverse Drug Discovery of Covalent Drugs

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Peptide Chemistry
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1487
Visible-Light-Mediated Functionalization of Cysteine Derivatives and Cysteine-Containing Peptides FREIER ZUGRIFF

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1488
Synthesis of Hexahydropyrrolo[3,4-b]pyrrole-Fused Quinolines from α-Amino Acid Methyl Esters

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1489
Iridium-Catalyzed Synthesis of Quaternary α- through ε-Amino Acid Derivatives

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1490
Palladium-Catalyzed Synthesis of Azatryptophan Analogues

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1491
Copper-Catalyzed Synthesis of Peptide-Containing Macrocyclic Alkynyl Sulfides

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1492
Photoredox-Catalyzed Synthesis of γ-Amino Acids from Styrenes, Amines, and CO₂

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1493
Three-Component Reaction Toward γ-Carbonyl-α-Amino Acids

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1494
Modification of the N-Terminus of Peptides

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1495
Synthesis of Reactive Amino Acid Esters by Using Amino Acid Chlorides in a Biphasic System FREIER ZUGRIFF

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Flow Chemistry
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1497
Rhodium-Catalyzed Hydrogenation of Enamides and α-or β-Dehydroamino Acids

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1498
Asymmetric Conjugate Addition–Oxidation Sequence in Flow Generating GABA Analogues

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1499
Preparation and Use of Halomethyl Grignard Reagents in Continuous Flow

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1500
Progress toward Fully Automated Chemical Synthesis

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