Synfacts
Ausgabe 04 · April 2022
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Ausgabe
Synform
A54
SYNFORM
ISSUE 2022/04
FREIER ZUGRIFF
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Synthesis of Natural Products and Potential Drugs
z0345
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PDF (382 kb)
0345
Syntheses of (–)-Crinipellins C and F
FREIER ZUGRIFF
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PDF (133 kb)
0346
Synthesis of MRTX1719
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PDF (83 kb)
0347
Total Synthesis of (–)-Lamellodysidine A
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PDF (83 kb)
0348
Synthesis of the C1–C13 Fragment of Eribulin
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PDF (106 kb)
0349
Total Synthesis of (+)-Madangamine E
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PDF (89 kb)
0350
Total Synthesis of (+)-Shizukaol J
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PDF (89 kb)
0351
Total Synthesis of (–)-Scabrolide A
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PDF (91 kb)
0352
Synthesis of (–)-Triptonide
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PDF (85 kb)
0353
Synthesis of CDK7 Inhibitor SY-5609
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PDF (85 kb)
0354
Total Synthesis of (+)-Dynemicin A
FREIER ZUGRIFF
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Synthesis of Heterocycles
z0355
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PDF (369 kb)
0355
Metal-Free Reduction of Aromatic Nitro Compounds
FREIER ZUGRIFF
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PDF (130 kb)
0356
Synthesis of Trifluoromethylated Azaheterocycles by Radical Chemistry
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PDF (79 kb)
0357
Synthesis of 1,2,4-Triazepines by a Base-Induced Formal [4+3] Cycloaddition
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PDF (81 kb)
0358
Access to Dibenzo[
c
,
e
]azonines by Iron-Catalyzed Alkyne–Carbonyl Metathesis
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PDF (79 kb)
0359
Convergent Synthesis of Isoindolines from Cyclic Imines and Organolithium Intermediates
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PDF (85 kb)
0360
A Solution to Nickel-Catalyzed Cross-Electrophile-Coupling Woes
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PDF (86 kb)
0361
Facile Halogenation of Aminoheterocycles for Rapid Diversification
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PDF (86 kb)
0362
Multicomponent Synthesis of Fluorescent Indolizine Tetracycles
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PDF (88 kb)
0363
Large-Scale Synthesis of 3-Fluoro-6-methoxyquinoline
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PDF (83 kb)
0364
Transition-Metal-Free One-Pot Synthesis of 3-Acylisoxazoles
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PDF (96 kb)
0365
TfOH-Promoted Selective C2–N1 Ring-Expansion Reaction of Indazoles
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PDF (78 kb)
0366
Organophosphorus-Catalyzed Cyclization of
N
-(2-Hydroxyethyl)amides
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PDF (90 kb)
0367
Visible-Light-Induced Transition-Metal-Free C(sp
2
)–H Difluoromethylation of Hetarenes
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PDF (84 kb)
Synthesis of Materials and Unnatural Products
z0369
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PDF (279 kb)
0369
From 3-Arylindole to Polycyclic Heteroarenes: Copper-Catalyzed Aerobic Oxidative Annulation
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PDF (69 kb)
0370
Zigzag Carbon Nanotube Segments from Gold Rings
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0371
Troponoid Porphyrinoids
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PDF (79 kb)
0372
N-Type B–N-Embedded Perylene Diimides
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0373
Do the Twist
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0374
Building BN-Embedded Heteroarenes via Boron Tribromide-Induced Scholl Reaction
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0375
Polymer Diversification: N–O Problem for This Reagent!
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PDF (68 kb)
0376
Synthesis of a New Helicene
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0377
PAH with a Boron Heart
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0378
Aromatic Norcorrole Phosphorous Complexes
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PDF (84 kb)
0379
Crazy (Nitrogen)-Rich Acenes
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PDF (77 kb)
0380
Powerful Barriers for Helicates
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Metals in Synthesis
z0381
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0381
Atroposelective Direct C–H Arylation of Indoles
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PDF (80 kb)
0382
Enantioenriched
N
,
O
-Ketals via Copper-Catalyzed Asymmetric Addition of Alcohols to Ketimines
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PDF (97 kb)
0383
Cyclopropanation of Alkenes via a Siloxycarbene–Palladium Complex
FREIER ZUGRIFF
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PDF (145 kb)
0384
Lights on or Lights off? Controlling Cobalt-Catalyzed Selective Reduction of Ketones or Acids with Light
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PDF (80 kb)
0385
The Direct Coupling of Phenols and Amines under Rhodium Catalysis
FREIER ZUGRIFF
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PDF (126 kb)
0386
Rhodium-Catalyzed Desymmetric Intermolecular Arylation of Cyclohexadienones
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PDF (94 kb)
0387
Palladium-Catalyzed Formal [3+2], [4+2], and [5+2] Heteroannulation of Non-conjugated Alkenyl Amides
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PDF (201 kb)
0388
Iridium-Catalyzed Enantioselective Hydroamination of Terminal Alkenes
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PDF (75 kb)
0389
Open It the Right Way: Ru- and Rh-Catalyzed Access to (Cross-)Conjugated Dienoates from Vinylcyclopropanes
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PDF (74 kb)
0390
Palladium-Catalyzed Annulation of Diene-Tethered Alcohols with Aminals
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PDF (80 kb)
0391
Deuterium Labelling of (Hetero)Arenes Enabled by a Nanostructured Iron Catalyst
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PDF (76 kb)
0392
Un
zinc
able! A Lewis Acid-Mediated Suzuki–Miyaura Cross-Coupling Under Base Free Conditions
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PDF (81 kb)
0393
Enantioselective Palladium-Catalyzed Hayashi–Miyaura Reaction with Coumarins
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PDF (72 kb)
0394
A Nickel-Catalyzed Desymmetrization Approach toward 2,3-Dihydro-1
H
-inden-1-ols
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PDF (86 kb)
0395
Enantioselective Decarbonylative Aryl Addition Across Bicyclic Alkenes
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PDF (82 kb)
0396
Nickel-Catalyzed 1,2-Carboaminocarbonylation of Strained Alkenes
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PDF (96 kb)
0397
Facile Access to Thiocarboxylic Acid Derivatives via Nickel-Catalyzed Cross-Coupling
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PDF (93 kb)
0398
Preparation of Enantioenriched α-Difluoromethylsilanes Enabled by Nickel Catalysis
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PDF (94 kb)
0399
Asymmetric Addition of Aryl Iodides to Aldehydes Catalyzed by a Nickel–CyanoBOX Complex
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PDF (70 kb)
0400
Pyrimidyl Ethers Replace Pivalates in Asymmetric Enolate Arylation
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PDF (89 kb)
0401
Desymmetrization of
exo
-Cyclic Alkenes via Enantioselective Cobalt-Catalyzed Isomerization
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PDF (92 kb)
0402
Deuteration of Benzylic C–H Bonds Enabled by η
6
-Coordination to Rhodium(III)
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PDF (94 kb)
0403
A General Approach for Introducing the Trifluoromethylamino Group into Organic Molecules
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PDF (78 kb)
0404
Copper-Catalyzed Enantioselective Reductive Aldol Reaction
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PDF (97 kb)
0405
Epimerization of Diols under Transient Thermodynamic Control
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PDF (82 kb)
0406
The Fukuyama Reduction of Thio Esters to Aldehydes
FREIER ZUGRIFF
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PDF (117 kb)
Polymer-Supported Synthesis
z0407
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PDF (335 kb)
0407
Polymer-Supported Helical Peptide Catalyst for Enantioselective Nitro-Michael Addition
FREIER ZUGRIFF
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PDF (132 kb)
0408
Carboxylative Cyclization of Propargylic Amines with CO
2
Catalyzed by Silver Nanoparticles
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PDF (78 kb)
0409
Suzuki–Miyaura Cross-Coupling on Polystyrene-Supported Palladium Oxide Nanoparticles in Water
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PDF (86 kb)
0410
One-Pot Synthesis of Quinazoline-2,4-diones Catalyzed by ZnO Immobilized on Dendric Fibrous Nanosilica
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PDF (78 kb)
0411
Palladium-Catalyzed Cyanide-Free Cyanation of Aryl Iodides with Nitromethane
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PDF (82 kb)
0412
Selective Transformation of Anilines to Azoxybenzenes, Azobenzenes, or Nitrosobenzenes Catalyzed by Zr(OH)
4
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PDF (85 kb)
0413
Graphene Oxide-Catalyzed Trifluoromethylation of Alkynes with Quinoxalinones
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PDF (91 kb)
0414
Deuteration and Homocoupling of C(sp)–H Bonds Catalyzed by Cationic Bimetallic Cages
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PDF (94 kb)
0415
Alder-Ene Reaction of Allenynamides on Cellulose-Immobilized Copper Nanoparticles
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PDF (72 kb)
0416
N-Alkylation of Amines and Ammonia with Alcohols Catalyzed by Cobalt Nanoparticles
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PDF (80 kb)
0417
Transfer Hydrogenolysis and Hydrogenation of DNA-Conjugated Substrates in Aqueous Micellar Media
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PDF (130 kb)
0418
Direct Esterification of Carboxylic Acids with Alcohols and Thiols on an Amphiphilic Monolith-SO
3
H Resin
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PDF (69 kb)
Organo- and Biocatalysis
z0419
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PDF (303 kb)
0419
Direct Cyclopropanations of Olefins with Methylene Compounds via Organoelectrocatalysis
FREIER ZUGRIFF
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PDF (143 kb)
0420
Organophotoredox-Catalyzed Carboxylation of C(sp
3
)–O Bonds
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PDF (93 kb)
0421
Organophotocatalytic Benzylation of Nonactivated Allylic C–H Bonds
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HTML
PDF (83 kb)
0422
Imidazoline–Phosphoric Acid-Catalyzed Asymmetric Pictet–Spengler Reaction of α-Keto Esters
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PDF (97 kb)
0423
Dual Hydrogen-Atom Transfer and Photoredox Catalysis Permits Alkyl Radical Addition
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PDF (78 kb)
0424
Enantioselective β-
gem
-Difluoroalkylation of Enals under Organocatalytic Photoredox Conditions
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PDF (113 kb)
0425
Iminophosphorane Catalyst Permits Enantioselective Sulfa-Michael Addition to α,β-Unsaturated Amides
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PDF (100 kb)
0426
Organophotocatalytic [2+1] Cycloaddition Toward the Synthesis of Cyclopropenols
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PDF (91 kb)
Chemistry in Medicine and Biology
z0427
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PDF (1475 kb)
0427
Electrochemical Late-Stage Methylation
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PDF (81 kb)
0428
Double the Bet: Discovery of Dimeric Cinchona Alkaloid-Inspired Macrocycles as LC3 Lipidation Inducers
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PDF (93 kb)
0429
A Novel Thiazolidine Scaffold that Inhibits O-GlcNAcase (OGA)
FREIER ZUGRIFF
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PDF (239 kb)
0430
A Sweet Bonus to Drug Release
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PDF (91 kb)
0431
Structural Diversification of 14-Membered Macrolides
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PDF (94 kb)
0432
Nitrogen Lovers – Azaphilone Natural Products Inspire the Development of Bioconjugation Reagents
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PDF (91 kb)
0433
Iridium, Palladium, Cobalt and Rhodium Came to Hamigeran M’s Party
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PDF (85 kb)
0434
Scalable Synthesis of a Key Fluoro-BPin Fragment towards MCL‑1 Inhibitors
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PDF (76 kb)
0435
Transition Metal Catalysis Enables an Efficient Synthesis of Soraphen A
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PDF (85 kb)
0436
SEAKing Cancer Cells to Locally Activate Prodrugs
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PDF (187 kb)
0437
Late-Stage Photocatalytic C–H Olefination
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PDF (84 kb)
0438
Photoaffinity Probe Identifies New Cellular Targets of Lenalidomide
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PDF (79 kb)
0439
A Cyclic Twist: Enantioselective Formation of Spirocyclic Oxindoles via Double Alkylation
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PDF (84 kb)
0440
Novel Photocleavable Protecting Group for Native Chemical Ligation
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PDF (83 kb)
0441
Synthesis of Toxicodenane A – A Sesquiterpenoid that Protects Cells from Lipotoxicity
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PDF (91 kb)
Peptide Chemistry
z0443
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Volltext
PDF (380 kb)
0443
Photocatalytic Synthesis of Amino Acid Amides
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PDF (77 kb)
0444
Cinchona Alkaloid-Catalyzed α-Selenylation of Amino Acid Derivatives
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PDF (93 kb)
0445
5-Nitro-4,6-dithiocyanatopyrimidine: A Novel Coupling Reagent for Peptide Synthesis
FREIER ZUGRIFF
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PDF (130 kb)
0446
Palladium-Catalyzed Site-Selective Modification
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PDF (70 kb)
0447
Synthesis of Peptide Thioesters via Ynamides
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HTML
PDF (70 kb)
0448
Nickel-Catalyzed C(sp
3
)–C(sp
3
) Cross-Coupling for the Synthesis of Unnatural Amino Acids
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HTML
PDF (67 kb)
0449
Copper-Catalyzed Asymmetric Conjugated Addition to Form Chiral α-Amino Acids
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PDF (98 kb)
0450
Ru- or Rh-Catalyzed C–H Functionalization of Amino Acid-Derived Phosphinamides with Alkynes
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PDF (81 kb)
0451
Peptide Modification by Bicyclobutane–Triazolinedione Cycloadditions
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HTML
PDF (75 kb)
0452
Cobalt-Catalyzed Oxidative Functionalization of Cyclic Ethers to Form Fluorinated Amino Acids
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PDF (78 kb)
0453
Copper-Catalyzed β-Alkylation of Amino Acid Schiff Bases
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PDF (91 kb)
0454
Solid-Phase Synthesis of α-Amino Alkyl or Aryl Phosphonopeptide Derivatives
FREIER ZUGRIFF
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HTML
PDF (142 kb)
Flow Chemistry
z0455
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PDF (120 kb)
0455
Multistep Closed-Loop Optimization for the Synthesis of Edavarone
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HTML
PDF (85 kb)
0456
Synthesis of (
S
)-Rolipram via Continuous Flow
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PDF (99 kb)
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