Synfacts
Issue 07 · July 2023
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A114
SYNFORM
ISSUE 2023/07
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Synthesis of Natural Products
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0637
Syntheses of (–)-Scabrolide A and (–)-Yonarolide
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0638
Total Synthesis of (+)-Ineleganolide
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0639
Total Synthesis of (–)-Daphnezomine A
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0640
Synthesis of (±)-KB343
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0641
Synthesis of (+)-Pedrolide
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0642
Total Synthesis of (–)-Grayanotoxin II
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0643
Synthesis of (–)-Aspidophytine
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Synthesis of Heterocycles
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0645
Aryl Radicals as XAT Promotors Enable Modular Alkyl Iodide Functionalization
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0646
Synthesis of Azabicyclic Cores of the Izidine Alkaloids
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0647
Ion-Paired Rhodium-Catalyzed Enantioselective Aziridination of Alkenyl Alcohols
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0648
Three-Component Reaction for the Synthesis of Isoxazoles
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0649
Stereoselective Synthesis of Six-to Eight-Membered Cyclic Ethers through Homologation/Metathesis
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0650
A Magical Rearrangement of Aryl Peroxyoxindoles to 1,3-Benzooxazin-4-ones
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0651
Cascade Reaction with Preservation of Stereochemistry for the Synthesis of Fused Cyclic Amine Systems
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0652
Synthesis of Functionalized Bicyclic Tetrahydrocyclopentafuran Derivatives
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0653
Operationally Simple Dearomatization of Bicyclic Azaarenes
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0654
Robust Trifluoromethylation of (Hetero)arylboronic Acid Pinacol Esters
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0655
Site Selective C–H Carboxylation of N-Heteroarenes via Electrochemical Reactors
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Synthesis of Materials and Unnatural Products
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0657
Pyrenylenes of Varied Size from One Pot
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0658
Chiral Bowl-Shaped PAHs with Five- and Eight-Membered Rings
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0659
A One-Pot Method from Six- to Seven-Membered Rings
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0660
Dearomatization of Quinolines and Isoqunolines
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0661
π-Extended Chiral [2.2]Cyclophanes
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0662
A Chiral Calix[3]pyrrole Analogue
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0663
Heptacene Analogue with Benzodi[7]annulene
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0664
Pot-Economic Approach to Benzophenanthridine Alkaloids
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0665
Stochastic Bullvalene Architecture Modulates Structural Rigidity in π-Rich Macromolecules
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0666
Functionalizing COFs via Ugi Reaction
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0667
Recyclable and Malleable Polycyanurate Thermosets
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0668
A Modular Strategy for N-Doped PAHs with Nonhexagons
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Metals in Synthesis
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0669
An Asymmetric Intramolecular Heck-Type Reaction of in situ Generated Hydrazones
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0670
Enantioconvergent Trifluoromethoxylation of Propargyl Sulfonates under Copper Catalysis
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0671
Enantioselective Copper-Catalyzed Three-Component Synthesis of
Z
,
Z
-Multifunctional-1,5-dienes
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0672
Metal-Controlled Regiodivergent Hydroamination of α-Methylene-β-Lactams
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0673
Nickel-Catalyzed Asymmetric Vinylogous Addition of Silyloxyfuran to Oxindoles
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0674
Cobalt-Catalyzed Hydroalkylation of Glycals for the Stereoselective Synthesis of 2-Deoxy-β-
C
-Glycosides
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0675
Gone in 60 Seconds: Very Fast Birch Reductions under Ammonia-Free Conditions Using Ball-Milling Technique
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0676
Silver-Catalyzed Formation of Benzo[
d
]oxepines via Ring-Expansive Addition of Diazonium Compounds
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0677
Terminating the Catellani Reaction by C(sp
2
)–I Reductive Elimination to Access
ortho
-Iodobiaryls
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0678
Copper/Chromium-Catalyzed Nucleophilic C(sp
3
)–H Addition of Alkanes to Aldehydes under Visible Light
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0679
Cobalt-Catalyzed Reductive Arylation of
N
-Sulfonyl Imines
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0680
Gold-Catalyzed Heck Reaction with Selective β-Hydride Elimination
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0681
Asymmetric Metalloradical-Catalyzed Synthesis of Cyclopropane-Fused Chromanes and Chromanones
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0682
Functionalized 1,4-Dihydropyridines Using Benzylamines,
N
,
N-
Dimethyl Enaminones and Copper
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0683
Rhodium-Catalyzed Synthesis of Chiral
trans
-γ‑Lactams through Dynamic Kinetic Resolution
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0684
Turning Enol Triflates into Axially Chiral Allenes by Palladium-Catalyzed Enantioselective β-H Elimination
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0685
Cooperative Dihydrogen Activation by a Zinc–Anilide Complex Enables Semi-Hydrogenation of Alkynes
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0686
Photoredox-Catalyzed Trifluoromethylation of C(sp
2
)–H Bonds with Trifluoroacetic Anhydride
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0687
β-Selective C(sp
3
)–H Borylation of Saturated Cyclic Amines and Lactams by Cooperative Catalysis
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0688
Palladium-Catalyzed Benzylic Allyl-/Allenylation of Benzyl Chlorides
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0689
Sulfamidate Imine Derived 1-Azadienes: A New Class of Dipolarophiles in Pd-Catalyzed [3+2] Cycloadditions
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0690
A Ligand-Controlled Stereodivergent Decarboxylative Aldol Reaction under Titanium Catalysis
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0691
Z
-Retentive Asymmetric Allylation of Oxindoles Using Iridium Catalysis
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0692
A General Protocol for Photoinduced C(sp
3
)–H Functionalization under Iron Catalysis
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0693
Enantioconvergent Synthesis of α-Amino Acids by Iron-Catalyzed α-C(sp
3
)–H Amination of Carboxylic Acids
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0694
Synthesis of Functionalized Skipped Dienes via Nickel-Catalyzed Reductive Cross-Coupling
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0695
Synthesis of 2,3-Disubstituted Indoles via Palladium-Catalyzed Cyclization of
ortho-
Alkynyl Anilines
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Polymer-Supported Synthesis
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0697
Cross-Dehydrogenative C(sp
2
)–N Coupling by a Cu–Co Dual-Atom Catalyst Supported on Hierarchical Zeolite
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0698
N-Monomethylation of Primary Amines and Nitroarenes with Methanol Using Pd(II) Dispersed on Zn(Al)O
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0699
Mechanochemical Suzuki–Miyaura Coupling Promoted by PEG-Supported Palladium Complex
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0700
Reductive Amination of Aryl Ethers Catalyzed by Hf-Exchanged Montmorillonite-Supported Pd
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0701
Hydroboration of Olefines with a Cobalt(0)-COF Catalyst
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0702
Bodipy-Based MOFs Transformed from 1D Chain to 2D Layer as Photocatalysts Build C–B and C–C Bonds
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0703
Monophosphine-Ir or -Ru Complexes in Chiral Diphosphine-Based COFs for Asymmetric Hydrogenation
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0704
Photo-Induced Borylation of
N
-Heteroarenes with a β-Keto Enamine-Based Covalent Organic Framework
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0705
Ruthenium Phosphide Nanoparticles Supported on SiO
2
for Hydrogenation of Sulfur-Containing Nitroarenes
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0706
Photocatalytic Oxidative Homo-Coupling of Amines by a Donor–Acceptor Mixed-Ligand MOF
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0707
Synthesis of Tetrasubstituted Pyridines through Solid-Phase Truce–Smiles Rearrangement
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0708
C–H Oxidation and Epoxidation of Alkenes Using a Fe
III
–MOF-253 Complex with O
2
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Organo- and Biocatalysis
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0709
Engineered Methyltransferase-Catalyzed Terminal Prenyl Group Tail Methylation of Linear Terpenoids
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0710
BINOL Catalysis Permits One-Pot Synthesis of Chiral Trifluoromethyl and Trimethylsilyl Allenols
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0711
Asymmetric Conjugate Hydrocyanation of Enals via SET-Induced Umpolung
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0712
Methionine Sulfoxide Reductase as an Efficient Catalyst for Kinetic Resolution of the Chiral Sulfoxides
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0713
Regioselective
meta
-Amination of Arylamines Enabled by in situ Generated Quinone Imine Ketals
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0714
Towards Efficient Synthesis of Chiral β-Amino Amides via Organocatalysis
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0715
Novel C
2
-Symmetric Borinic Acids Expand the Scope of Boron-Based Catalysts for Asymmetric Transformations
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0716
Organocatalytic Enantioselective Reductive Radical Coupling of Ketimines with Dihydropyridines
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0717
Enantioselective Iminium Catalysis-Mediated Vinylcyclopropane–Cyclopentene Rearrangement
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Innovative Drug Discovery and Development
z0719
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0719
Conquering Regioselectivity Issues: Scalable Synthesis to an Alkylated 1,2,4-Triazole Building Block
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0720
Synthesis of Selective HDAC11 Inhibitor with Nanomolar Potency
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0721
Controlling Protein Activity with a Carboxyl Group Cage
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0722
A Dearomative Cyclization Approach Enables Easy Access to Cardenolides from the Hajos–Parrish Ketal
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0723
Semi-Rational Design Expedites Identification of Imine Reductases with Complementary Enantioselectivity
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0724
Discovery of Haloperidol
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0725
Efficient Synthesis of Ketoprofen
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0726
Practical and Environmentally Friendly Manufacturing Process for Ensitrelvir, a SARS-CoV-2 Antiviral Candidate
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0727
Discovery of a Potent and Orally Bioavailable Estrogen Receptor Degrader-Antagonists
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0728
Synthesis of Urazolyl-Tyrosine Macrocyclic Peptides via Chemoselective Oxidative C–N Coupling
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0729
Preparation of Biologically Active Peptide-Isoquinolone Conjugates
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Peptide Chemistry
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0731
C–H Functionalization for the Synthesis of Maleimide-Decorated Peptides and Macrocyclic Peptides
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0732
Regioselective Fluorination of Amino Acid Derivatives
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0733
Electrosynthesis of γ,δ-Unsaturated α-Amino Esters
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0734
Pd-Catalyzed α-Allylation of N-Unprotected Amino Acids
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0735
One-Pot Synthesis of Amnio Acids with Consecutive Tetrasubstituted Stereogenic Center
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0736
Asymmetric Alkylation to Afford Tetrasubstituted Amino Acids
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0737
Copper-Catalyzed Synthesis of α-Amino Acids from Primary Alcohols
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0738
Selective Deprotection of
tert
-Butyl Ester Groups in
N
-Boc-Protected Amino Acid
tert
-Butyl Esters
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Flow Chemistry
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0739
Enantioselective Synthesis of α-Alkylated Aldehydes Using Continuous Flow Chemistry and Visible Light
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