Synthesis

Issue 16 · November 2002

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review
2319
Chambert, Stéphane; Désiré, Jérôme; Décout, Jean-Luc:
The 2-(Trimethylsilyl)ethyl Sulfur Group in Synthesis

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short paper
2335
Zeng, Bu-bing; King, S. Bruce:
Palladium-Catalyzed Synthesis of Water-Soluble Symmetric 9,10-Disubstituted Anthracenes

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2338
Braga, Antonio L.; Rodrigues, Oscar E. D.; Paixão, Marcio W.; Appelt, Helmoz R.; Silveira, Claudio C.; Bottega, Diana P.:
One-Pot Synthesis of New Chiral Sulfides and Selenides Containing Oxazolidines: Catalyst in the Enantioselective Addition of Diethylzinc to Benzaldehyde

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2341
Sosnovskikh, Vyacheslav Ya; Usachev, Boris I.:
A Simple and Efficient Synthesis of 2-Methyl-2-trifluoromethylchroman-4-ones from 2-Trifluoromethyl-4H-chromen-4-imines and Malonic Acid

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2344
Yadav, Lal Dhar S.; Kapoor, Ritu:
An Expeditious One-Pot Synthesis of Thiiranes from α-Halo Ketones in Solvent-Free Conditions Using Microwaves

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paper
2347
Du, Da-Ming; Wang, Zhan-Yue; Xu, Dong-Cheng; Hua, Wen-Ting:
Synthesis of Novel Chiral Bisoxazoline Ligands Containing 2,5-Diaryl-1,3,4-oxadiazole and Enantioselective Cyclopropanation of Styrene

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2353
Martins, Marcos A. P.; Sinhorin, Adilson P.; da Rosa, Adriano; Flores, Alex F. C.; Wastowski, Arci D.; Pereira, Claudio M. P.; Flores, Darlene C.; Beck, Paulo; Freitag, Rogerio A.; Brondani, Sergio; Cunico, Wilson; Bonacorso, Helio G.; Zanatta, Nilo:
Regiospecific Allylic Mono- and Dibromination of 4-Methoxy-1,1,1-trihalo-3-alken-2-ones and 5-Methoxy-1,1,1,2,2-pentafluoro-4-hexen-2-one, and their Applications to the Synthesis of Heterocycles

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2359
Yamada, Koichiro; Flippen-Anderson, Judith L.; Jacobson, Arthur E.; Rice, Kenner C.:
Probes for Narcotic Receptor Mediated Phenomena; 29: Synthesis of rac-(4R,6aR,11bR)-3-Methyl-...

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2365
Kálai, Tamás; Balog, Mária; Jekő, József; Hubbell, Wayne L.; Hideg, Kálmán:
Palladium-Catalyzed Coupling Reactions of Paramagnetic Vinyl Halides

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2373
Göksu, Süleyman; Seçen, Hasan; Sütbeyaz, Yasar:
One-Pot and Stereospecific Synthesis of cis-1,2-Diazides via Mitsunobu Reaction of Epoxides

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2379
Holland, Richard; Spencer, John; Deadman, John J.:
Synthesis of para-Substituted 3-Formyl Arylboronic Esters

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2383
Yadav, Jhillu S.; Subba Reddy, Basi V.; Parimala, G.; Venkatram Reddy, P.:
Lithium Perchlorate Catalyzed Regioselective Ring Opening of Aziridines with Sodium Azide and Sodium Cyanide

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2387
Ludwig, Peter S.; Schwendener, Reto A.; Schott, Herbert:
A New Laboratory Scale Synthesis for the Anticancer Drug 3′-C-Ethynylcytidine

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2393
Alajarín, Mateo; Vidal, Angel; Ortín, María-Mar; Tovar, Fulgencio:
Intramolecular [4 + 2] Cycloaddition Reactions of Ketenimines: A New Synthesis of Benz[b]acridines

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2399
Rozas, María F.; Piro, Oscar E.; Castellano, Eduardo E.; Mirífico, María V.; Vasini, Enrique J.:
Novel Synthesis of 3,4,4-Trisubstituted Thiadiazolines from 3,4-Diphenyl-1,2,5-Thiadiazole 1,1-Dioxide. Competition with the Intra-Molecular Aryl-Aryl Cyclization of 3,4-Diphenyl-1,2,5-Thiadiazole 1,1-Dioxide

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2404
Zanatta, Nilo; Rosa, Luciana S.; Cortelini, Maria F. M.; Beux, Simone; Santos, Ana P. D.; Bonacorso, Helio G.; Martins, Marcos A. P.:
One-Pot Synthesis of a New Series of 3-Alkoxy-5-hydroxy-5-trifluoromethylpyrrolidin-2-ones from 1,1,1-Trifluoro-4-alkoxyalk-3-en-2-ones

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2409
Zanatta, Nilo; Squizani, Adriana M. C.; Fantinel, Leonardo; Nachtigall, Fabiane M.; Bonacorso, Helio G.; Martins, Marcos A. P.:
Application of 4-Alkoxy-1,1,1-trifluoro[chloro]alk-3-en-2-ones as Selective Protecting Groups of Amino Acids

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2416
Smaliy, Radomir V.; Chaikovskaya, Aleksandra A.; Pinchuk, Aleksandr M.; Tolmachev, Andrei A.:
Isocyanatophosphoric Acid Dichloride: A Novel Reagent for the Introduction of a Cyano Group into the Molecules of Electron-Rich Heterocycles and Enamines

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2421
Selvakumar, Natesan; Srinivas, Deekonda; Azhagan, Azagarsamy Malar:
Observation of O→N Type Smiles Rearrangement in Certain Alkyl Aryl Nitro Compounds

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2426
Cheng, Ying; Zhan, Yu-Hua; Guan, Hai-Xia; Yang, Hua; Meth-Cohn, Otto:
Synthetic Applications of Aminochlorocarbenes: A Two-step Conversion of N-Methylformanilides into 3-Arylamino-2-chloroindoles

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2431
Ward, Robert S.; Davies, Joanna; Hodges, Geoffrey; Roberts, David W.:
Synthesis of Quaternary Alkylammonium Sulfobetaines

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2440
Subramaniyan, G.; Raghunathan, R.; Martin Castro, Ana M.:
3-Arylidene-4-flavanones Acting as 2π Components in an Intermolecular 1,3-Dipolar Cycloaddition Reaction of Azomethine Ylides

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2445
Besada, P.; González-Moa, M. J.; Terán, C.; Santana, L.; Uriarte, E.:
Novel 1,2-Disubstituted Carbocyclic Nucleoside Analogues of Purine with a Cyclopentene Ring

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2450
Calvo, Luis; González-Ortega, Alfonso; Sañudo, M. Carmen:
Synthesis of 2,3-Dihydropyrrolizines from Weinreb 3-(Pyrrolidin-2-ylidene)propionamides or Weinreb N-Vinylprolinamides

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feature article
2457
Lin, Wen-Li; Taduri, B. Pratap; Liu, Rai-Shung:
Stereocontrolled Construction of Tricyclic Furan and Pyrrolyl Derivatives via Tungsten-Mediated [3+2] Cycloaddition and Intramolecular Diels-Alder Reaction

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synthesis alerts
2464
Kocienski, P. J.:
Synthesis Alerts 16/02
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book review
2472
Klok, H.-A.:
Functional Condensation Polymers
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Synthesis

The 2-(Trimethylsilyl)ethyl Sulfur Group in Synthesis

Palladium-Catalyzed Synthesis of Water-Soluble Symmetric 9,10-Disubstituted Anthracenes

One-Pot Synthesis of New Chiral Sulfides and Selenides Containing Oxazolidines: Catalyst in the Enantioselective Addition of Diethylzinc to Benzaldehyde

A Simple and Efficient Synthesis of 2-Methyl-2-trifluoromethylchroman-4-ones from 2-Trifluoromethyl-4H-chromen-4-imines and Malonic Acid

An Expeditious One-Pot Synthesis of Thiiranes from α-Halo Ketones in Solvent-Free Conditions Using Microwaves

Synthesis of Novel Chiral Bisoxazoline Ligands Containing 2,5-Diaryl-1,3,4-oxadiazole and Enantioselective Cyclopropanation of Styrene

Regiospecific Allylic Mono- and Dibromination of 4-Methoxy-1,1,1-trihalo-3-alken-2-ones and 5-Methoxy-1,1,1,2,2-pentafluoro-4-hexen-2-one, and their Applications to the Synthesis of Heterocycles

Probes for Narcotic Receptor Mediated Phenomena; 29: Synthesis of rac-(4R,6aR,11bR)-3-Methyl-...

Palladium-Catalyzed Coupling Reactions of Paramagnetic Vinyl Halides

One-Pot and Stereospecific Synthesis of cis-1,2-Diazides via Mitsunobu Reaction of Epoxides

Synthesis of para-Substituted 3-Formyl Arylboronic Esters

Lithium Perchlorate Catalyzed Regioselective Ring Opening of Aziridines with Sodium Azide and Sodium Cyanide

A New Laboratory Scale Synthesis for the Anticancer Drug 3′-C-Ethynylcytidine

Intramolecular [4 + 2] Cycloaddition Reactions of Ketenimines: A New Synthesis of Benz[b]acridines

Novel Synthesis of 3,4,4-Trisubstituted Thiadiazolines from 3,4-Diphenyl-1,2,5-Thiadiazole 1,1-Dioxide. Competition with the Intra-Molecular Aryl-Aryl Cyclization of 3,4-Diphenyl-1,2,5-Thiadiazole 1,1-Dioxide

One-Pot Synthesis of a New Series of 3-Alkoxy-5-hydroxy-5-trifluoromethylpyrrolidin-2-ones from 1,1,1-Trifluoro-4-alkoxyalk-3-en-2-ones

Application of 4-Alkoxy-1,1,1-trifluoro[chloro]alk-3-en-2-ones as Selective Protecting Groups of Amino Acids

Isocyanatophosphoric Acid Dichloride: A Novel Reagent for the Introduction of a Cyano Group into the Molecules of Electron-Rich Heterocycles and Enamines

Observation of O→N Type Smiles Rearrangement in Certain Alkyl Aryl Nitro Compounds

Synthetic Applications of Aminochlorocarbenes: A Two-step Conversion of N-Methylformanilides into 3-Arylamino-2-chloroindoles

Synthesis of Quaternary Alkylammonium Sulfobetaines

3-Arylidene-4-flavanones Acting as 2π Components in an Intermolecular 1,3-Dipolar Cycloaddition Reaction of Azomethine Ylides

Novel 1,2-Disubstituted Carbocyclic Nucleoside Analogues of Purine with a Cyclopentene Ring

Synthesis of 2,3-Dihydropyrrolizines from Weinreb 3-(Pyrrolidin-2-ylidene)propionamides or Weinreb N-Vinylprolinamides

Stereocontrolled Construction of Tricyclic Furan and Pyrrolyl Derivatives via Tungsten-Mediated [3+2] Cycloaddition and Intramolecular Diels-Alder Reaction

Synthesis Alerts 16/02

Functional Condensation Polymers