Synlett

Issue 04 · April 1996

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289
Kita, Yasuyuki; Shibata, Norio: Asymmetric Pummerer-Type Reactions Induced by O-Silylated Ketene Acetals

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297
Skibo, Edward B.; Islam, Imadul; Schulz, William G.; Zhou, Ru; Bess, Laura; Boruah, Romesh: The Organic Chemistry of the Pyrrolo[1,2-a]benzimidazole Antitumor Agents. An Example of Rational Drug Design

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310
Boons, Geert-Jan; Burton, Andrew; Wyatt, Paul: Glycosyl Phosphates: A New Latent-Active Anomeric Phosphorylation Strategy

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313
Duynstee, Howard I.; Wijsman, Eric R.; Marel, Gijs A. van der; Boom, Jacques H. van: Synthesis of 2’-O-[(4’’-O-sorboyl)-α-L-fucopyranosyl]inosine: A Shimofuridin analogue

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315
Schmittel, Michael; Levis, Michael: Electron Transfer Induced Deprotection of Benzyl Substituted 1,3-Dithianes with Iron(III)phenanthroline Complexes

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317
Ewin, Richard A.; Simpkins, Nigel S.: Regioselective and Enantioselective Metallation of A Tricarbonyl(η⁶-arene)chromium Complex Derived from 1,3-Dihydroisobenzofuran

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319
Sugahara, Tsutomu; Ogasawara, Kunio: An Expedient Route to (-)-cis-2-Oxabicyclo[3.3.0]oct-6-en-3-one via a meso-Asymmetrization

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321
Otera, Junzo; Chen, Jianxie: Unprecedented Preference for Aldehyde over Acetal in Organotin Lewis Acid-Promoted Mukaiyama-Aldol Reaction of Ketene Silyl Acetals

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324
Hashimoto, Shun-ichi; Miyazaki, Yoji; Ikegami, Shiro: A Regio- and Stereocontrolled Synthesis of 13,14-Didehydroisocarbacyclin

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327
Tenaglia, Alphonse; Karl, François: Intramolecular Heck Reaction of Hex-2-enopyranosides: an Easy Entry to Cis-Fused Furo- or Pyrano[2,3b]pyranones

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330
Nagashima, Tadamichi; Curran, Dennis P.: Reactions of Tempo with Alkylsamarium and Other Organometallic Reagents

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333
Curini, Massimo; Rosati, Ornelio; Pisani, Emanuela; Costantino, Umberto: Heterogeneous Catalysis in Carbonyl Regeneration from Oximes, Semicarbazones, and Tosylhydrazones by Zirconium Sulfophenyl Phosphonate

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335
Ishihara, Jun; Sugimoto, Tetsuya; Murai, Akio: Asymmetric Synthesis of Syringolide 1, a Novel Nonproteinaceous Elicitor

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337
Pan, Weidong; Feng, Xiaoming; Gong, Liuzhu; Hu, Wenhao; Li, Zhi; Mi, Aiqiao; Jiang, Yaozhong: Asymmetric Synthesis XXIV: Chiral Salen-Titanium Complexes-Efficient Catalysts for Asymmetric Trimethyl Silylcyanation of Benzaldehyde

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339
Lavoisier, Tania; Rodriguez, Jean: C-O versus C-C Tandem Cycloalkylation of Stabilized Carbanions. Facile One-Pot Stereoselective Preparation of Functionalized Cyclic Enol Ethers

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341
Couladouros, Elias A.; Apostolopoulos, Costas D.: 1,4-Reductive Addition of Hydrazoic Acid

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343
Sibi, Mukund P.; Deshpande, Prasad K.; La Loggia, Anthony J.: Regio- and Stereoselective Functionalization of Linear Dicarboxylic Acid Derivatives. A Sequential Aldol-Lactonization Strategy for the Synthesis of (-)-Roccellaric Acid, (-)-Protolichesterinic Acid, and (-)-Methylenolactocin

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346
Teng, Kelly; Bharadwaj, Ramesh; Cook, P. Dan: Utility of 1-(5’-Acetoxy-4’-Benzoyltetrahydrofuran-2’-yl)-3-Benzyloxymethylthymine for the Synthesis of 5’-Modified Furanoid Nucleoside Analogs¹

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349
Fielder, Simon; Rowan, Daryl D.; Sherburn, Michael S.: Synthesis of α-Farnesene Hydroperoxides

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351
Hosokawa, Seijiro; Isobe, Minoru: Partial Synthesis of Ciguatoxin, an A/B/C Fragment

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353
Takahashi, Ichiro; Kawakami, Teruki; Hirano, Etsushi; Yokota, Hiroshi; Kitajima, Hidehiko: Novel Phthalimidine Synthesis. Mannich Condensation of o-Phthalaldehyde with Primary Amines using 1,2,3-1H-Benzotriazole and 2-Mercaptoethanol as Dual Synthetic Auxiliaries

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356
Rossi, Renzo; Bellina, Fabio; Carpita, Adriano: New Efficient Procedures for Direct Introduction of the Agrochemically Important β-Methoxypropenoate Unit into Substituted Aromatic Derivatives

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359
Congreve, Miles S.: Synthesis of 5-N-Substituted Tetrazole Derivatives of the Potent NK₁ Receptor Antagonist GR203040

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361
Malmberg, Mats; Rehnberg, Nicola: A Facile Synthesis of N-substituted D-arabino-piperidinol Phosphates from the Inositol Phosphate α-Trinositol

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363
Ishihara, Jun; Murai, Akio: Absolute Construction of the Whole Mother Skeleton of Hemibrevetoxin-B

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366
Matsumoto, Masakatsu; Ishikawa, Hiromi; Ozawa, Takayuki: Pd-Catalyzed Alkylation of 1,6-Anhydro-2-chloro-2,3,4-trideoxy-β-D-erythro-hex-3-enopyranose

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369
Sudrik, S. G.; Balaji, B. S.; Singh, A. P.; Mitra, R. B.; Sonawane, H. R.: Zeolite-mediated Synthesis of β-Keto Esters: Condensation of Ethyl Diazoacetate with Aldehydes

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371
Shi, Guo-qiang; Cai, Wei-ling: 3,3-Difluoro-2-ethoxy-2-propenol: Preparation and Utility as a Novel Synthon of α,α-Difluoroketones

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373
Kawatsura, M.; Dekura, F.; Shirahama, H.; Matsuda, F.: Samarium(II) Iodide Promoted Ketone-Olefin Couplings Chelation-Controlled by (Alkoxycarbonyl)amino Groups

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377
Lhermitte, Frédéric; Carboni, Bertrand: Radical Reactions in Organoboron Chemistry. III -Addition Reactions to Alkynylboranes as Efficient Routes to New Regio- and Stereodefined Alkenyl Diamino- and Dialkoxyboranes

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380
Maywald, Frank; Eilbracht, Peter: A Chiral 1-Aza-1,3-butadiene Tricarbonyliron Complex as Fe(CO)₃-Transfer Reagent for the Enantioselective Complexation of 1,3-Dienes

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383
Singaram, Bakthan; Jackson, Thomas C.; Harrison, John: Synthesis of Alkylborohydrides by Addition of Alkoxides, Amides and Thiolates to the Corresponding Alkylboranes

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385
Miesch, Michel; Mislin, Gaëtan; Franck-Neumann, Michel: Access to the Bicyclo[5.3.1]undecadiene Ring System by Two Carbon Ring Enlargement of Bicyclo[3.3.1]nonane Derivatives

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387
Bolm, Carsten; Derrien, Nadine; Seger, Andreas: Hyperbranched Macromolecules in Asymmetric Catalysis

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389
Motorina, Irina A.; Parly, Florence; Grierson, David S.: Selective O-Allylation of Amidoalcohols on Solid Support

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391
Dulcère, Jean-Pierre; Dumez, Estelle; Faure, Robert: Preparation of 3-Butadienyl Tetrahydrofurans and α-Butadienyl γ-Butyrolactones by Radical Cyclization of β-Bromopent-4-en-2-ynyl Ethers and mixed Acetals

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393
Basavaiah, D.; Pandiaraju, S.; Padmaja, K.: The Friedel-Crafts Chemistry: Acetates of the Baylis-Hillman Adducts as Novel Stereodefined β-Electrophiles

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396
Beifuss, Uwe; Gehm, Henning; Taraschewski, Michael: Diastereoselective Synthesis of cis- and trans- Annulated Hexahydrothioxanthenes: The First Stereochemical Study on the Intramolecular Polar Cycloaddition of Cationic 2-Thiabutadienes

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399
Abouabdellah, Ahmed; Bégué, Jean-Pierre; Bonnet-Delpon, Danièle: First Synthesis of Methyl syn 3-CF₃-Isoserinate

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401
Batsanov, Andrei S.; Byerley, Andrew L. J.; Howard, Judith A. K.; Steel, Patrick G.: Chiral Auxiliaries in the Vinyl Epoxide - Dihydrofuran Rearrangement

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404
Brunel, Jean Michel; Kagan, Henri B.: Catalytic Asymmetric Oxidation of Sulfides With High Enantioselectivities

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