Synfacts

Issue 12 · December 2018

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A186
Zanda, Matteo: SYNFORM ISSUE 2018/12 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
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Synthesis of BMS-932481 FREE ACCESS

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1216
Synthesis of Tesirine

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1217
Divergent Route to Gelsedine-Type Alkaloids FREE ACCESS

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1218
Total Syntheses of Bisdehydroneostemoninine and Bisdehydrostemoninine

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1219
Total Synthesis of Aspochalasan Natural Products

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1220
Synthesis of (–)-Shishijimicin A

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1221
Asymmetric Synthesis of Efinaconazole and Albaconazole

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1222
Synthesis of a Ghrelin Receptor Agonist

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1223
Total Synthesis of (–)-Alstoscholarisine A

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1224
Synthesis of (–)-Nodulisporic Acid C

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1225
Synthesis of (+)-Piericidin A

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1226
Synthesis of GDC-0810

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1227
Synthesis of Lorlatinib

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Synthesis of Heterocycles
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1229
Stereoselective Synthesis of Phosphorothioate Nucleotides FREE ACCESS

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1230
Chan–Lam Coupling/Friedel–Crafts Reaction Sequence to Acridines

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1231
Reductive Isoxazoline-to-Pyrrolidone Ring Interconversion

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1232
Rhodium(III)-Catalyzed Synthesis of 1,4-Dihydroisoquinolin-3(2H)-ones

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1233
1-Phenylsulfonyl-3-Oxabicyclo[3.1.0]hexan-2-one for the Synthesis of Spirocycles

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1234
Organocatalytic Route to Tetrahydrochromeno[4,3-b]pyrrol-4(1H)-ones

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1235
Ru-Catalyzed Synthesis of Pyrazines and Pyrroles from Ammonia and Diols

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1236
Synthesis of Indoloquinolines by a Dinitrogen-Extrusion/Cyclization Method

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1237
Electrochemical Coupling of Benzothiophenes with Phenols

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1238
Modified Paal–Knorr Cyclization Route to Substituted Pyrrolodiazepinones

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1239
Enantioselective Synthesis of Pyrimidinones by the Biginelli Reaction

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1240
Diastereoselective Cyclopropanation of Unsaturated Pyrazolones

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1241
Palladium-Catalyzed Synthesis of Indolo[3,2-a]Carbazoles from Indoles

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1242
Iron(III)-Catalyzed Asymmetric Synthesis of Tetrahydroindolizines

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Synthesis of Materials and Unnatural Products
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1243
Rare Fluorescence Observed from Indacenes

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1244
A More Tolerant Initiator for Living Aryl Isocyanide Polymerization

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1245
New Photoactivatable Hydride Donors: Benzothiazole-Containing Terarylenes

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1246
2D Heteroacenes: New Building Blocks for Organic Materials FREE ACCESS

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1247
Mild, One-Pot Balz–Schiemann Reaction Accessible via Organotrifluoroborates

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1248
Indoloindoles through Gold(I)/Rhodium(II) Catalyzed Cascade Cyclizations

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1249
Butterfly in a Flask: Irregular Nanographenes by Highly Regioselective Domino Benzannulation

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1250
Corannulenes with B–N Units on its Spoke

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1251
A Thiophene, Pyrrole, and Furan Walk Into a Bar…

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1252
Serendipitous Synthesis of Expanded Porphyrinoids

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1253
Fluorinated Cycloparaphenylene: The Same and Not the Same

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1254
Tunable Red-Emitting Bismuth-Containing Polymers in the Presence of Oxygen

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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1255
Nickel-Catalyzed Enantioselective Reductive Diarylation FREE ACCESS

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1256
Palladium-Catalyzed Atroposelective C–H Activation

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1257
Nickel-Catalyzed Enantioselective Hydroalkylation of 1,3-Dienes FREE ACCESS

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1258
Palladium-Catalyzed Enantioselective Decarboxylative Allylic Alkylation

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1259
Asymmetric Synthesis of 3-Allyl-3-hydroxyoxindoles

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1260
Asymmetric Allylic Alkylation through Palladium and Copper Dual Catalysis

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1261
Nickel–Catalyzed Diarylation of 1,2-Disubstituted Alkenylarenes

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1262
Asymmetric Propargylation of 5H-Thia(oxa)zol-4-ones

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1263
Rhodium-Catalyst Generates Cyclic Peptide Stereocenters in Sequence

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1264
Palladium-Catalyzed Enantioselective Suzuki–Miyaura Coupling

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1265
Copper-Catalyzed Stereoselective Hydrohalogenation of Internal Alkynes

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1266
Enantioselective Aldol Reaction of Silyl Ketene Imines

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1267
Palladium-Catalyzed Enantioselective Synthesis of 1H-Isoindoles

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1268
Ruthenium-Catalyzed Transfer Hydrogenation of Axial Biaryl Imines via a DKR strategy

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1269
Stereoselective Iridium–Catalyzed Haloamidation of Alkynes

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1270
Diastereoselective Gold-Catalyzed Cyclization of Nitrones

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1271
Ligand-Directed Gold-Catalyzed Annulations of Ynamides and 1,2-Benzisoxazoles

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1272
Palladium-Catalyzed Enantioselective C–H Olefination of Oxime Ethers

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1273
Enantioselective 3-Alkylation of Benzofuranones with α-Diazo Esters

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1274
Copper-Catalyzed Synthesis of Atropisomeric 2′-Iodo[1,1′-biphenyl]-2-yl Thioates

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1275
Ru-Catalyzed Asymmetric Transfer Hydrogenation of Dihalo Keto Esters or Amides

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1276
Enantioselective [4+1] Cycloaddition of Danishefsky’s Diene and Diazoarylacetates

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1277
New Ligands for the Iridium-Catalyzed Asymmetric Hydrogenation of Olefins

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1278
Palladium-Catalyzed Carboannulation for Chiral Indane Synthesis

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1279
Application of Novel N-Tosyl Bisimidazoline Ligands in Palladium(II)-Catalyzed Arylation

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1280
Gold-Catalyzed Enantioselective Synthesis of Indolyl Cyclopenta[c]furans

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1281
Nickel-Catalyzed Carboiodination

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1282
Spiroketal Bisphosphine Rhodium Complexes for Asymmetric Hydrogenation

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Metal-Mediated Synthesis
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1283
para-Ketonization Using Electrophilic Vinyl Ethers FREE ACCESS

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1284
Transition-Metal-Free Synthesis of Chiral Aniline Derivatives

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1285
Carbozincation of Alkynes Catalyzed by Rhodium Complexes

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1286
Bimetal-Catalyzed Benzylic Arylation of Toluenes

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1287
Asymmetric Synthesis of C,C-Diaryl Hydantoins

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1288
Nickel-Catalyzed α-Alkylation of Ketones with Alcohols

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1289
C–F Bond Functionalization via a Nickel-Catalyzed Cross-Coupling

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1290
A New Isocyanide Functionalization

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1291
A New Di-trifluoromethylation of Arynes

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1292
Chiral Diamine Enantioselective Addition of Me₂Zn to Fluorinated Ketones

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1293
Diastereoselective Copper-Catalyzed Synthesis of Unsaturated Trialkylsilyl Esters

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1294
Palladium(I)-Catalyzed Oxidative Cross-Coupling

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1295
Copper-Mediated Direct C–H Difluoromethylation of Heteroarenes

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Organo- and Biocatalysis
z1297
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1297
Asymmetric Phosphoric Acid Catalyzed Four-Component Ugi Reaction FREE ACCESS

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1298
Photoredox-Catalyzed Decarboxylative Radical Cyclization Cascade

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1299
Asymmetric Organocatalytic Vicinal Difluorination of Styrenes

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1300
Asymmetric Enzymatic Hydration of Nonactivated Olefins

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1301
Asymmetric Oxidative Coupling of Carboxylic Acids to α-Branched Aldehydes

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1302
Synthesis of Axially Chiral Anilides by Atroposelective Allylic Alkylation

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1303
N-Heterocyclic Carbene Catalyzed Umpolung Acylation in Fullerene Chemistry

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1304
Functionalization of Enamides Catalyzed by a Chiral Phosphoric Acid

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1305
Application of Nitrones for the Asymmetric Synthesis of Substituted Piperidines

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Polymer-Supported Synthesis
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1307
Palladium Nanoparticle Catalyzed Cyanation of Iodobenzenes

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1308
Huisgen Reaction Catalyzed by Silica-Coated Magnetic Copper Nanoparticles

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1309
Alkyne–Azide Cycloaddition on Water-Soluble Copper NP–Cobaltocene Catalyst FREE ACCESS

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1310
Three-Component Reactions in Water with a Supported Cu(I) Acetylacetonate Composite

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1311
Oxidative C=C Cleavage of Styrenes with Supported Cobalt Vanadium Oxide

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1312
Photooxidative Coupling of Amines Catalyzed by Mixed-Phase 2D-Molybdenum Sulfide

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1313
Oxidative Esterification with N-Doped Carbon-Incarcerated Co/Cu Nanoparticles

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1314
Transfer Hydrogenation with Formic Acid Catalyzed by Cobalt on Mesoporous Carbon

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1315
Ruthenium-Catalyzed Carbonylative Synthesis of Quinazolinones

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1316
Oxidative Coupling of Phenylglyoxals with Amines on Gold Nanoparticles in Water

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1317
Aerobic Oxidation of Alcohols with a Heterogeneous Iodine Catalyst

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1318
Petasis Reaction on Reduced Graphene Oxide Supported CuO Nanoparticles

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1319
Halogenation of Anilides and Quinolines on a MnO-Supported Copper Catalyst

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Flow Chemistry
z1321
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1321
Synthesis of N-Carboxyanhydrides in a Microflow Reactor

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1322
Combined Photoredox/Hydrogen Transfer for Functionalization of Nonactivated Alkanes

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1323
Iron-Catalyzed Arylhydroxylation in Continuous Flow

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1324
Light Absorption of a Palladium–Zinc Complex allows Negishi Cross-Couplings

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1325
Enantioselective Synthesis of Quaternary α-Amino Acids in Flow

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1326
Flow Synthesis of a Doravirine Fragment

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