Synfacts

Issue 05 · May 2019

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A63
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It Takes Alkynes

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Harp on HaRP FREE ACCESS

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Honey, I Shrunk the Polymers

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Chan–Lam–Evans Coupling is Now Available on Carbon Nanotubes

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Breaking the Habit: Synthesis of Unsymmetrically Substituted Tetravinylethylenes

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Turning Nanohoops On

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0500
Full to the Brim: Rim-Substituted Corannulenes as Non-fullerene Electron Acceptors

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Metals in Synthesis
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0501
Ag⁺/Proton Relay Catalysis for Stereoselective Synthesis of Spiro-2-oxabicyclo[2.2.2]octanes

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0502
Synthesis of 4-Substituted Isoxazolines via a Gold-Catalyzed Skeletal Rearrangement

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0503
Controlling Facial Selectivity Towards Carbocations via a Docking Strategy FREE ACCESS

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0504
Copper-Catalyzed C–H Carbamoyloxylation of Aryl Carboxamides

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Palladium-Catalyzed Enantioselective Aminotrifluoromethoxylation of Alkenes FREE ACCESS

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Enantioselective Synthesis of α-Chiral Silanes

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0507
Nickel-Catalyzed Hydroarylation

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0508
Copper-Catalyzed Enantioselective Allylation Using Allene

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Enantioselective Copper-Catalyzed Synthesis of α-Arylpyrrolidines

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0510
Nickel-Catalyzed Asymmetric Synthesis of Organosilanes

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0511
Deaminative Nickel-Catalyzed Alkyl–Alkyl Cross-Couplings

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Iridium-Catalyzed ‘Chain-Walking’/Cope Rearrangement

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Palladium-Catalyzed Dual Annulation: Towards the Norneocryptolepine Core

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Nickel-Catalyzed N-Arylations via Nitrogen Radicals

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Photoredox-Catalyzed α-Alkylation of Amines

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0516
Asymmetric Diarylation of Vinylarenes

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0517
The Jacobsen Epoxidation FREE ACCESS

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0518
Nickel-Catalyzed Electrochemical Thiolation

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0519
Photochemical Giese Addition to Olefins

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0520
Catalytic Radical Difluoromethoxylation

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0521
Rhodium-Catalyzed Reverse Hydroboration

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0522
Palladium-Catalyzed Synthesis of Difluoromethylated Esters

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0523
The Takai Olefination: Simple Access to E-Alkenyl Halides FREE ACCESS

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0524
Copper-Catalyzed C–H Oxidative Radical Functionalization of Olefins

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0525
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Selective C–N Bond Cleaving Kumada Cross-Coupling

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Heck Coupling of Cyclopropanated Heterocycles

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0528
Dinickel-Catalyzed [4+1] Cycloadditions

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0529
ortho-Borylation of Arylphosphines

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Synthesis of N-Alkylcyclohexylamines on Supported Rh/Pt Nanoparticles FREE ACCESS

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0532
Cobalt-Catalyzed Regio- and Stereoselective Hydrosilylation of Alkynes

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0533
Dehydrative Allylation of Amines with Allyl Alcohol on Supported Molybdenum Oxide

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0534
Cyclization of Propargylic Alcohols with CO₂ on a Cu₄I₄ Metal–Organic Framework

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0535
Palladium-Catalyzed Coupling of 2-Hydroxy-1,4-naphthoquinones with Olefins

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0536
Pd-Catalyzed Cyclization of 2-Iodoanilines with Alkynes and Oxalic Acid

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0537
Hydrodeoxygenation of Carboxylic Acids on N-Doped-Carbon-Supported Iron

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0538
Synthesis of 1H-Tetrazoles with a Resin-Supported Tin Catalyst

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0539
Dehydrogenation of Amines and Transamination on Pd-Doped Hydrotalcites

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0540
Cycloaddition of CO₂ to Epoxides with an Al(III)–Salen Molecular Cage

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0541
Oxidative Heck Reaction on a Porous-Polymer-Supported Palladium Catalyst

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0542
Hydrogenation of Ketones on Silver Nanoparticles

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Organo- and Biocatalysis
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0543
N-Heterocyclic Carbene Catalyzed Alkylation of Aromatic Aldehydes

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0544
Acid-Catalyzed Intramolecular Hydroindolation of cis-Methindolylstyrenes

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0545
Hydrogen-Bonding Phase-Transfer Catalysis toward β-Fluoroamines FREE ACCESS

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0546
Chiral Brønsted Acid Catalyzed Asymmetric Oxidation of Sulfenamides

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0547
Enantioselective Aminocatalytic Heterocycloadditions

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0548
Asymmetric Organocatalytic Oxidative Coupling of Indoles with Aldehydes

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0549
Stereospecific Biocatalytic Friedel–Crafts Alkylation of Resorcinols

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0550
Asymmetric Countercation Directed Catalysis of an S_N2X Reaction

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0551
Enzymatic Carboxylation of 2-Furoic Acid to 2,5-Furandicarboxylic Acid

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0552
The Asymmetric Nazarov Cyclization of Simple Divinyl Ketones

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0553
Asymmetric Countercation Directed Catalytic Resolution of BINOLs

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Cinchona Alkaloids in Organic Catalysis FREE ACCESS

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Four New DNA Building Blocks FREE ACCESS

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0556
Organelle-Targeted Membrane Tension Probes

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0557
Bioactive Analogues of TAN-2483B

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A Manganese-Based Contrast Agent for Imaging Calcium Ions

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0559
Functionalization of Palladium Oxidative Addition Complexes Derived From Pharmaceuticals

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0560
Targeting the RAS–SOS1 Interaction

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0561
Ethynylphosphonamidate-Cysteine Bioconjugation

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A High Affinity Fluorescent Sensor for Norepinephrine

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Ring-Closing Metathesis in the Synthesis of Simeprevir

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Antimalarial 1,2,4-Triazine Dimers

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New Methods to Access DNA-Encoded Libraries (DELs)

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Peptide Chemistry
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Pd-Catalyzed Oxazoloisoindolinone Synthesis from N-Benzoyl-α-Amino Acids

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C-Terminal Elongation of Dipeptide Isopropenyl Esters

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Efficient Macrocyclization of Small Peptides FREE ACCESS

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Cleavage of Fmoc Groups with Sodium Hydroxide in 2-Methyltetrahydrofuran–Methanol

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0571
Copper-Catalyzed Multicomponent Synthesis of Quaternary α-Amino Esters

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0572
Thiourea-Catalyzed Asymmetric Mannich Reaction

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0573
Synthesis of Peptides by Using Recombinant Proteins FREE ACCESS

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0574
Chemoselective Ligation by Using an Adipic Acid Dihydrazide Crosslinker

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Flow Chemistry
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Continuous-Flow, Michaelis−Arbuzov Rearrangement

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0576
DFT Guides the Optimization of Photosensitized [2+2] Cycloadditions in Flow

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0577
Synthesis of Ketones from Organolithium Reagents in Continuous Flow

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Flow Synthesis of Ciprofloxacin

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Flow Synthesis of Lomustine

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