Synfacts

Ausgabe 04 · April 2023

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Ausgabe
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A59
SYNFORM ISSUE 2023/04 FREIER ZUGRIFF

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Synthesis of Natural Products
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0323
Synthesis of (+)-Chejuenolide A

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0324
Total Synthesis of (–)-Taxol

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0325
Total Synthesis of (+)-Bufogargarizin B FREIER ZUGRIFF

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0326
Total Synthesis of (–)-Prorocentin

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0327
Synthesis of (–)-Lissodendoric acid A

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0328
Synthesis of Atrachinenins A and B

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0329
Total Synthesis of (–)-Strychnine FREIER ZUGRIFF

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Synthesis of Heterocycles
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0331
Modular Synthesis of Benzimidazoles from Nitroarenes

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0332
Oxidant-Free Synthesis of Fully Substituted Pyrroles through Multicomponent Cyclization

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0333
Circumventing the Aryldiazonium Salt Isolation in Intramolecular Heck–Matsuda Coupling

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0334
Direct and Practical Approach for the Synthesis of δ-Carbolines and Benzofuro[3,2-b]pyridines

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0335
Rational Design of a Palladium Catalyst System for C–N Bond Formation of Five-Membered Heteroaryl Halides

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0336
Robust Conditions for Nickel-Catalyzed Suzuki–Miyaura Cross-Couplings of Complex Molecules

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0337
Palladium-Catalyzed Synthesis of Benzazocines via [6+2] Double Allene Annulation

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0338
Catalyst-Free Synthesis of Oxacyclic Spirooxindoles through Oxonium Ylide Mediated Ring Expansion

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0339
Scalable Syntheses of Functionalized 2-Oxabicyclo[2.2.2]octanes

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0340
Construction of Functionalized Oxazole via Three-Component Cyclization Using a Lewis Acid

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0341
Bicyclic Silaazacycles Featuring Silicon at the Ring Junction: Synthesis and Further Transformations

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0342
Nickel-Catalyzed One-Pot Cascade Synthesis of N‑Substituted Indoles

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0343
Three-Step Modular Synthesis of N-Substituted Bicyclic Systems

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0344
Efficient Access to Pharmacologically Relevant 2-Arylpiperazines

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Synthesis of Materials and Unnatural Products
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0345
9-Fluorenol-Assisted Tertiary Radical Generation and Functionalization

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0346
Build-Up BN-Rings Step by Step

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0347
Catenation of Chiral Cubes FREIER ZUGRIFF

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0348
Double Annulation with Three C–C Bond Formations

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0349
“Click” a Phenanthrene

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0350
Three-Component Synthesis of Bicyclic Diphosphacycles

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0351
B(III)Br-B(II)-Stabilized Neutral Boryl Radical

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0352
Carbene-Mediated Polyaminoborane Depolymerization

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0353
How Does 5+7 Compare to 6+6

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0354
Desymmetrized Chiral Calix[4]arenes

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0355
Aromatic Ring Expansions by Iminosilylene

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0356
o-Nitrobenzyl Ether-Enabled Polymer Photo-Degradation

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Metals in Synthesis
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0357
ortho Difunctionalization of Arenes by Iron/Titanium Synergistic Interaction FREIER ZUGRIFF

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0358
Enantioselective Molybdenum-Catalyzed Cyclopropanation via Carbonyl Activation

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0359
Ni-Catalyzed Formation of Two Vicinal Enantioenriched C(sp³) Centers Stemming from Two Starting Materials FREIER ZUGRIFF

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0360
Enantioselective Rhodium-Catalyzed Synthesis of Cyclobutene Derivatives Using Boronic Acids

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0361
Enantioselective Copper-Catalyzed Inverse-Electron-Demand Diels–Alder Using Phenyl Vinyl Selenide

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0362
Catalytic Asymmetric Conjugate Addition of 1,4-Dienes to β-Substituted Alkenyl Azaarenes

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0363
Nickel-Catalyzed Acylzincation of Ynamides with Alkylzinc Reagents Under CO Atmosphere

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0364
Photoinduced Decarboxylative C–C and C–N Couplings of Carboxylic Acids under Dual Iron/Copper Catalysis

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0365
Synthesis of Oxaspirolactones via Palladium-Catalyzed Hydrocarbonylation of Alcohol-Tethered Styrenes

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0366
Enantioselective Cobalt-Catalyzed Double Hydrogenation for Chiral Z-Allylamide Syntheses

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0367
Iron-Catalyzed and Electrochemical Dehydrogenative Synthesis of Monofluorinated Oxindoles

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0368
Copper-Catalyzed Benzo[d][1,3,2]dithiazole-1-oxide Synthesis via Cross-Coupling with Elemental Sulfur

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0369
Copper-Catalyzed Addition of Terminal Alkynes across Dialkyl Azodicarboxylates

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0370
Syntheses of Difluorocarbonyl Oxindoles and Isoquinoline-1,3-diones via Radical Nickel Catalysis

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0371
Asymmetric α-Acylation of N-Heterocycles with Carboxylic Acids by Dual Nickel/Photoredox Catalysis

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0372
Nickel-Catalyzed Regiodivergent Cross-Electrophile Coupling of Alkyl Bromides Steered by the Ligand

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0373
Photocatalytic C(sp²)−H Fluoromethoxylation of Arenes

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0374
Silver-Catalyzed Synthesis of Spirocycles via an Enamine–Iminium Umpolung Step

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0375
Gold-Catalyzed Synthesis of Alkynylated Pyrrolidines from N,O-Acetals via Cyclic Iminium Ion Intermediates

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0376
Synthesis of Pyrrolines via Ni-Catalyzed Iminoarylation of Alkene-Tethered Oxime Esters

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0377
Enantioconvergent Cross-Electrophile Coupling of Two Alkyl Halides to Access Chiral α-Alkylboronic Esters

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0378
Stereoconvergent 1,3-Rearrangement of (Homo)Allylic Alcohols Using Crabtree’s Catalyst

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0379
Nickel-Catalyzed Enantioselective C(sp)–P Cross-Coupling of Secondary Phosphines with Bromoalkynes

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0380
Highly Linear- or Branched-Selective Ni-Catalyzed Mizoroki–Heck Reaction of 1,3-Dienes

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0381
Intercepted Kinugasa Reaction with Ir Catalysis: Asymmetric Synthesis of Allylated β-Lactams

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0382
Desymmetrization of 1,3-Diols by Copper(I)-Catalyzed S–O Cross-Coupling with Aryl Sulfonyl Chlorides

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Polymer-Supported Synthesis
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0383
Semi-Hydrogenation of Alkynes and Suzuki Coupling with a Polyurethane Foam-Supported Pd Catalyst FREIER ZUGRIFF

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0384
C3-Formylation of Indoles with Methanol by g-C₃N₄/rGO/BiVO₄ Heterojunction Photocatalyst

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0385
MOF-Supported Chiral Frustrated Lewis Pair for Asymmetric Hydrogenation

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0386
Photocatalytic Dehydrative Etherification of Alcohols by an Unsupported Nanoporous Gold Catalyst

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0387
Aerobic Oxidative Annulation of N-Arylpyrrolidines Catalyzed by Pt/C

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0388
Synthesis of Amino Phenazines through the Oxidative Cyclization of Anilines with o-Phenylenediamines

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0389
1,4-Arylation of α,β-Unsaturated Ketones with Arylboronic Acids Using NHC–Coordinated Rh on Ceria

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0390
Heterogeneous Photocatalytic Multicomponent Reaction for the Synthesis of Imidazolidines

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0391
Hydrogenation of Nitroarenes Catalyzed by a COF-Based Photocatalyst

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0392
Oxidative Coupling of Carbon Monoxide with Amines by Gold Nanoparticles Supported on ZnO

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0393
Synthesis of α‑Haloketones from Vinylarenes Catalyzed by Cu-Modified Graphitic Carbon Nitride

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0394
Asymmetric Allylic Amination Using PS-Supported Phosphoramidite Ligands–Ir Complex

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Organo- and Biocatalysis
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0395
Formal Electronically Mismatched Radical Additions

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0396
Carbene Transferases as Catalysts for Chemodivergent Activation of C(sp²)–H and C(sp³)–H Bonds

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0397
Enantioselective Synthesis of Tertiary Nitroalkanes Enabled by Enzyme Catalysis FREIER ZUGRIFF

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0398
Aminocatalytic Enantio-, Diastereo- and Periselective [4+4] Cycloaddition

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0399
Hydrogen-Bond-Donor Catalyst Permits Asymmetric Transformation of Sulfonyl Cyanides toward Sulfinates

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0400
Photocatalytic Cyclopropanation of Unactivated Olefins with α-Bromomalonates and α-Bromo-β-Keto Esters

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0401
Borenium-Catalyzed Hydrogenative Cleavage of Unactivated C(Aryl)–C(Alkyl) Bonds

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0402
Conformation-Switching DNA Photocatalyst for Radical Polymerization

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0403
Asymmetric Enolexo-Aldol Condensations of Siladials via Enamine Catalysis

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0404
Identification of a Pericyclase that Catalyzes the Formation of cis-Decalins

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Innovative Drug Discovery and Development
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0405
Bioorthogonal “Click-and-Release” of Iminosydnones to Give Water-Stable Isocyanates FREIER ZUGRIFF

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0406
Total Synthesis of Iridoid Oligomers Enlightens Efficacy of Folk Medicine

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0407
Process Understanding Enables Control of Hydrogen Fluoride Formation in a Nitroarene Reduction FREIER ZUGRIFF

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0408
Hydrolysis-Resistant Ester for Probe Development

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0409
Design and Synthesis of BCL6 BTB Inhibitor OICR12694

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0410
MK-8189: A Potent and Selective PDE10A Inhibitor for the Treatment of Schizophrenia

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0411
Photo-Decarboxylative Coupling of α-Amino Acids and Enones Enables Efficient Synthesis of a Drug Scaffold

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0412
A Scalable Asymmetric Total Synthesis of (–)-Emetine

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0413
Efficient Synthesis of DNA Interstrand Cross-Links

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0414
Stepwise, Controllable Electrochemical Reduction of Trifluoromethylarenes

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0415
Macrocyclization and Scaffold Hopping Improves Selectivity and ADME Properties of HPK1 Inhibitors

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0416
Synthesis of Anesthetic Ketamine FREIER ZUGRIFF

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Peptide Chemistry
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0417
Rh(III)-Catalyzed Synthesis of Unnatural Peptides FREIER ZUGRIFF

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0418
Coupling of Amino Acid Terminal Alkyne with in situ Iminium Ion to Access N^ε‑Substituted Lysine Mimetics

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0419
Visible-Light-Mediated Continuous-Flow Technology for the Synthesis of α-(N-Hydroxy)amino Amides

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0420
Modification of Diamino Acid-Containing Hydrospirophosphoranes

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0421
Acetoxylation of Tyrosine-Containing Peptides Using a Palladium Catalyst

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0422
Palladium-Catalyzed C–H Alkenylation to Form Maleimide-Braced Peptides

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0423
Organocatalyzed Enantioselective N–H Insertion

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0424
Synthesis of N-Formyl Amino Acid Esters FREIER ZUGRIFF

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Flow Chemistry
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0425
Segmented Continuous Flow Allows for Convenient Synthesis of Phenyl Glucosazone

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Erratum
0426
Erratum: 2-Amino-3,3-difluoro-2,3-dihydrofurans from Difluorocarbenes and Enaminones

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