Synfacts

Ausgabe 05 · Mai 2024

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Synform
A071
SYNFORM ISSUE 2024/05 FREIER ZUGRIFF

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Synthesis of Natural Products
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0447
Total Synthesis of (–)-Hunterine A FREIER ZUGRIFF

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0448
Syntheses of (–)-Nidulalin A and (–)-Nidulaxanthone A

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0449
Total Synthesis of Securamine D

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0450
Synthesis of (+)-Principinol B

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0451
Total Synthesis of (–)-Psammaplysin A

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0452
Total Synthesis of (+)-Penicibilaenes A and B

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0453
Synthesis of (±)-Gelsemine FREIER ZUGRIFF

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Synthesis of Heterocycles
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0455
Spiro-Substituted Dioxetane-Based Chemical Probes with Enhanced Detection and Sensitivity Limits FREIER ZUGRIFF

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0456
Palladium-Mediated Diastereoselective Functionalization of Cyrene

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0457
Mild Nitrogen-to-Carbon Transmutation of Azaarene N-Oxides

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PDF (81 kb)
0458
Using Metallaphotoredox Towards the Synthesis of Aryl Nitriles and α-Aryl Nitriles

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0459
Access to and Physicochemical Analysis of Fluorinated Saturated Bicyclic Amine Building Blocks

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PDF (84 kb)
0460
Synthesis of Quinolones from Propargylic Chlorides and Amines

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PDF (70 kb)
0461
Electrochemical Formal C–H/C–H Regioselective Coupling of Heteroarenes

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0462
Copper-Catalyzed Synthesis of N-Heterocyclic Bicycles

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0463
Skeletal Editing of Pyridines to Afford 1,2-Diazepines

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0464
Electrochemical Cross-Dehydrogenative of Amides and Heteroarenes

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0465
Tether-Controlled Regiochemical Access to Complex Polyheterocyclic Molecular Architectures

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Synthesis of Materials and Unnatural Products
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0467
First Stable σ⁰π² Carbene FREIER ZUGRIFF

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0468
BN-Heterocycles from N-Heterocycle Editing

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0469
Stabilizing Acenes with Macrocycle Shielding

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PDF (144 kb)
0470
Biaryl Ligation Promoted by Catalyst-based π–π Stacking

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PDF (93 kb)
0471
Unsymmetric Macrocycle from Post-Modification of Dynamic Covalent Synthesis

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0472
Metalla-dehydro[11]annulenes from [10+1] Reactions

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0473
Azahomocorannulene Cation and Radical

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0474
Convertible Polyphenylene Covalent Organic Frameworks

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PDF (86 kb)
0475
Single-Crystal Ladder Polymer with Double Dynamic Covalent Linkers

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0476
Heptagon-embedded Highly Curved Diaza[7]helicenes

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0477
Acid-Triggered RAFT Polymerization

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0478
Spirobifluorenes from Biaryls and Fluorenones

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Metals in Synthesis
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0479
Hydrohalogenation of Alkenes Using Collidine·HX Salts under Dual Cobalt and Photoredox Catalysis FREIER ZUGRIFF

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0480
Hydrofluorination of Alkenes Using Et₃N·HF under Dual Cobalt and Photoredox Catalysis FREIER ZUGRIFF

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0481
Stereoselective Cu-Catalyzed Hydroborylation and Hydrosilylation of Spirocyclopropenes

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0482
Making Allylamines by 1,4-Aminoarylation of Butadienes under Photoinduced Palladium Catalysis

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0483
Cross-Electrophile Coupling Enabled by Visible-Light Palladium Catalysis FREIER ZUGRIFF

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0484
Copper-Catalyzed Crystallization-Induced Deracemization of Atropisomeric BINOL Derivatives

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0485
Cobalt-Catalyzed Hydrogenation and Deuteration of Bicyclic Olefins

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0486
Copper-Catalyzed Cross-Coupling of Benzyl Halides with (Me₄N)SCF₃

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0487
Asymmetric Synthesis of α-Aryl Amides Using Nickel/Photoredox Catalysis

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0488
C(sp³)–H Borylation of Alkanes and Silanes under Photoelectrochemically Driven Iron Catalysis

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0489
Dialkylation of Alkenes with Aliphatic Alcohols and Alkyl Halides by Dual Nickel and Photoredox Catalysis

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0490
Visible Light/Cu-Catalyzed Four-Component Alkene Azidosulfonylation Using DABSO and Arylthianthrenium Salts

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0491
Cobalt-Catalyzed Hydrosilylation of 1,6-Diynes via an Oxidative Cyclization

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0492
Iridium-Catalyzed Asymmetric Silylation of Propargylic C(sp³)–H Bonds

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0493
Asymmetric Synthesis of 1,3-Cyclohexadienes Enabled by Pd/Chiral Phosphoric Acid Cooperative Catalysis

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0494
Azidation and Etherification of Remote C(sp²)–C(sp³) Bonds of Amines Involving 1,4-Aryl Migration

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0495
Access to Axially Chiral N‑Arylindoles via Palladium-Catalyzed Atroposelective Larock Indole Synthesis

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0496
Access to Highly Functionalized Cyclohexanes via a Silver-Catalyzed Double Desymmetrization

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0497
Asymmetric α-C(sp³)–H Allylic Alkylation of Primary Alkylamines by Merging Iridium and Ketone Catalysis

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0498
Ni-Catalyzed Electroreductive Decarboxylative Cross-Coupling of Redox-Active Esters and Oxime Esters

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0499
Synthesis of N-Aryl Sulfonamides Enabled by Visible-Light Nickel Catalysis

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0500
Synthesis of C(sp³)-Rich Carbonyl-Containing Scaffolds via Ni-Catalyzed Deaminative Alkyl-Alkyl Cross-Coupling

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0501
Merging Decatungstate-Photocatalyzed Carbonylation of Alkanes and Asymmetric Brønsted Acid Catalysis

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0502
Deoxygenative Coupling of Carbonyl Compounds with Alkynes under Molybdenum Catalysis

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0503
Pd-Catalyzed Synthesis of Hydropyrrole-Containing Spirocycles via Domino Isonitrile Insertion/Heck Reactions

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0504
Asymmetric Photocycloaddition of 2-Acetonaphthones

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0505
Cobalt-Mediated Intramolecular Cyclization of Bis-homoallylic Alcohols under Aerobic Conditions FREIER ZUGRIFF

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Polymer-Supported Synthesis
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0507
Oxidative Homo-Coupling of Benzyamines Using Multi-Motif Molecule-Based COFs

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0508
Oxidation, Halogenation and Diels–Alder Reaction Promoted by a Covalent Triazine Framework

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0509
Asymmetric α-Arylation of Aldehydes with Aminophenol by 2D Chiral COF FREIER ZUGRIFF

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0510
N-Alkylation of Primary Amides with Alcohols Catalyzed by Cobalt Nanoparticles

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0511
Low-Valent Platinum Single-Atom Catalyst for Hydrosilylation of Alkenes

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0512
Selective Hydrogenation of Benzofurans Catalyzed by Pd–Ru Bimetallic Nanoparticles

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0513
Hydrogenation of Chlorobenzenes and Nitrobenzenes Using Au–Pd Bimetallic NPs Supported on COF

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0514
Quinoline-Linked COF for the Photocatalytic Oxidative Decarboxylation and Homo-Coupling Reactions

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0515
C–O, C–S, and C–P Coupling of Aryl Halides by a Ni(II)-Incorporated Covalent Organic Framework

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0516
Photoreduction of Nitrogroups via a Self-Assembled TiO₂-TEOA-Nitroarenes Complex

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0517
Trisindole Synthesis through a Graphene Oxide-Catalyzed Carbene-Transfer Reaction

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Organo- and Biocatalysis
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0519
Organocatalytic Nucleophilic Desymmetrization of P(V) Precursors FREIER ZUGRIFF

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PDF (137 kb)
0520
Flavin-Photocatalytic Sulfide α-C–H Functionalization Using Arylsulfonyl Multiple-Bond Reagents

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0521
Diazaphospholene Hydrides Catalyze Enantioselective Reductive Eschenmoser–Claisen Rearrangements

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0522
Organocatalytic Photoinduced Diastereoselective 1,2-Sulfonylsulfination of Alkenes

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0523
Regiodivergent Radical Termination for Intermolecular Biocatalytic C–C Bond Formation

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0524
Stereoselective Synthesis of α-Aminonitriles, Catalyzed by Hydrogen-Bonding Donors

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0525
Enzymatic Cleavage of Silicon–Carbon Bonds in Siloxanes

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PDF (176 kb)
0526
Mesoionic N-Heterocyclic Olefin Catalyzes Formylation of Thiols via CO₂ Trapping

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0527
Enantioselective Control Over α-Iminonitriles with a Novel Bifunctional Superbase-Thiourea Organocatalyst

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Innovative Drug Discovery and Development
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0529
A Convergent and Short Synthesis of Sorbicillactone A FREIER ZUGRIFF

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0530
Brain Biodistribution in Non-Human Primates of [¹¹C]BIIB104, an AMPA Receptor PAM

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0531
CVN766, the Selective Orexin-1-Receptor Antagonist Progressed to Clinical Investigations

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PDF (80 kb)
0532
One-Pot, Palladium-Free Access to 1° and 2° Amines

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0533
Access to Buchwald–Hartwig Products by ‘NH’ Insertion of Suzuki–Miyaura Aryl Partners

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0534
Arenophile Cycloaddition-Mediated Dearomative Pyridine Oxidation

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0535
Converting ¹⁴N-Pyridines to ¹⁵N-Pyridines through Zincke Imine Intermediates

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PDF (72 kb)
0536
From Racemic Mixtures to Enantioenriched Molecules: Suzuki–Miyaura Arylation of Acyclic Allylic Systems

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0537
Accelerated Photochemical Reactions at Oil-Water Interface Exploiting Melting Point Depression

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0538
Carbene-Catalyzed Alkylation of Indoles

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0539
A Mild Sulfation Strategy for Alcohols

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PDF (70 kb)
0540
Organo-Click Reaction Enables Access to Antimalarial Derivatives of Artemisinin

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0541
Parallel Synthesis of PROTACs via Photochemical C(sp²)–C(sp³) Cross-Coupling

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0542
An Asymmetric Synthesis of Sulfoximines, Sulfonimidamides and Sulfonimidoyl Fluorides

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0543
Schwartz’s Regent as a Chemo- and Diastereoselective Reductant of Sulfinyl Ketimines to Yield Chiral Amines

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0544
Total Synthesis and SAR Studies of the Neurotrophic Sesquiterpenoid Jiadifenin FREIER ZUGRIFF

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Peptide Chemistry
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0545
Dehydrative Peptide Coupling Promoted by HBF₄/MS 5Å FREIER ZUGRIFF

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0546
Synthesis of Functionalized Amino Acids from Cysteine Pentafluoropyridine

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0547
Chiral Ru-Li Combined Catalysts for Asymmetric Cyanation of α-Ketimino Ester Derivatives

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PDF (90 kb)
0548
Unprotected Cyclic Peptide Methylene Dithioacetals Synthesis by Rhodium Catalysis

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0549
Synthesis of α,α-Dialkyl Amino Acid Ethyl Esters Using Asymmetric Phase-Transfer Alkylation

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PDF (84 kb)
0550
Copper-Catalyzed C(sp³)–H Alkylation of Glycine Derivatives

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0551
Activation of N-Ts Amide C–N Bonds by N-Heterocyclic Carbene-Squaramide Bifunctional Catalyst

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PDF (79 kb)
0552
One-Pot Protocol to Access Spirocyclic Unnatural β-Amino Acids via C–H Activation/C–C Cleavage

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PDF (92 kb)
0553
Synthesis of β-Tertiary Amino Acids Analogues via Cobalt-Catalyzed Stereoselective Radical Addition

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PDF (89 kb)
0554
Copper-Catalyzed [3+2] Cycloaddition for the Site-Specific Modification of Peptides

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PDF (95 kb)
0555
Photoredox and Nickel-Catalyzed Glycosylation of Amino Acids and Peptides

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PDF (67 kb)
0556
Synthesis of Optically Active Amino Amides

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PDF (84 kb)
0557
Racemization-Free Synthesis of N-Formyl Amino Acid Esters FREIER ZUGRIFF

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Flow Chemistry
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0559
Synthesis of Pentafluorosulfanylpyrazoles in Flow

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