Synthesis

Issue 03 · 1988

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159
Schmidt, Ulrich; Lieberknecht, Albrecht; Wild, Jochen: Didehydroamino Acids (DDAA) and Didehydropeptides (DDP)

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173
Pettig, Dagmar; Schöllkopf, Ulrich: Asymmetric Synthesis via Heterocyclic Intermediates; XXXVII¹ Asymmetric Synthesis of Dimethyl (R)-2-Amino-(E)-hept-4-enedioates by the Bislactim Ether Method

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175
Miyoshi, Noritaka; Hatayama, Yoshio; Ryu, Ilhyong; Kambe, Nobuaki; Murai, Toshiaki; Murai, Shinji; Sonoda, Noboru: Ring Opening of Tetrahydrofurans with Phenyl Trimethylsilyl Selenide Catalyzed by Moist Zinc Iodide

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178
Katayama, Sadamu; Fukuda, Kinue; Watanabe, Toshio; Yamauchi, Masashige: Synthesis of 1,3-Dicarbonyl Compounds by the Oxidation of 3-Hydroxycarbonyl Compounds with Corey-Kim Reagent

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184
Feringa, Ben L.; Jansen, Johan F. G. A.: A New Synthesis of Imines via Grignard- and Cuprate Additions to N-Trimethylsilylformamides

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186
Yuan, Chengye; Li, Shusen; Cheng, Zhiyi: Studies on Organophosphorus Compounds XXVI. New Aspects on the Synthetic Study of Some Cyclic Esters of Alkylphosphonic Acids

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189
Burger, Klaus; Geith, Klaus; Hübl, Dieter: Über eine neue Methode zur positionsselektiven Einführung von Trifluormethyl-Gruppen in Heteroaromaten, Teil ¹. Synthese von trifluormethyl-substituierten 1,3-Azolen (Oxazole, Thiazole, Imidazole)

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194
Burger, Klaus; Hübl, Dieter; Geith, Klaus: Über eine neue Methode zur positionsselektiven Einführung von Trifluormethyl-Gruppen in Heteroaromaten, Teil 2.¹ Nucleophile Substitution an 5-fluor-4-trifluormethyl-substituierten 1,3-Azolen

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199
Burger, Klaus; Geith, Klaus; Hübl, Dieter: Über eine neue Methode zur positionsselektiven Einführung von Trifluormethyl-Gruppen in Heteroaromaten, Teil 3.¹ Lineare und angulare Verknüpfung von Ringsystemen sowie Herstellung anellierter trifluormethyl-substituierter Fünfring-Heterocyclen.

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203
Alberola, A.; Antolín, L. F.; Cuadrado, P.; González, A. M.; Laguna, M. A.; Pulido, F. J.: The Reactions of 3-Unsubstituted Isoxazolium Salts with 1,2-Dinucleophiles. Synthesis of 4-Functionalized 3-Aminoisoxazoles and 3-Aminopyrazoles

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208
Kamitori, Yasuhiro; Hojo, Masaru; Masuda, Ryöich; Fujitani, Toshihiko; Ohara, Seiji; Yokoyama, Tetsuya: A Convenient Synthesis of 5-Aryl-6-trifluoromethyl-3,6-dihydro-2H-1,3,4-oxadiazines. A Silica Gel Catalyzed Novel Cyclization Reaction

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210
Ahlbrecht, Hubertus; Ibe, Marcellinus: Die Addition von 1-Lithio-1-(phenylthio)alkanen an 2-(N-Methylanilino)acrylnitril: Ein einfacher Weg zu 3-(Phenylthio)ketonen und 2-Enonen

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215
Katritzky, Alan R.; Vazquez de Miguel, Luis M.; Rewcastle, Gordon W.: Specific Synthesis of 1-Substituted Phenothiazines Using Carbon Dioxide Protection of the NH Group During Lithiation

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communication
218
Effenberger, Franz; Niesert, Claus-Peter; Kühlwein, Jürgen; Ziegler, Thomas: Aminosäuren, Teil 11¹. Eine einfache Synthese von N-Carboxy-α,β-didehydro-α-aminosäure-anhydriden (4-Alkyliden-2,5-oxazolidindionen)

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219
Giese, Bernd; Rupaner, Robert: A Convenient Synthesis of exo-Brevicomin via a Radical C-C Bond Forming Reaction

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221
Tolstikov, A. G.; Khakhalina, N. V.; Spirikhin, L. V.: Benzyl Esters of D- and L-Arabinals as Chiral Synthons in Organic Synthesis

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223
Szeja, Wiesław: A Convenient Synthesis of α-D-Glucopyranosides

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224
Szeja, Wiesław; Bogusiak, Jadwiga: Synthesis of S-Glycosyl N,N-Diethyldithiocarbamates from Protected, Reducing Monosaccharides Under Phase-Transfer Conditions

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226
Luk, Kin-Chun; Wei, Chung-Chen: Preparation of Derivtives of (R)-1,2,4-Butanetriol from L-Ascorbic Acid

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228
Aoyama, Toyohiko; Shioiri, Takayuki: New Methods and Reagents in Organic Synthesis; 73.¹ Trimethylsilyldiazomethane: A Convenient Reagent for the Conversion of Aliphatic Aldehydes to the Homologous Methyl Ketones

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229
Ashwell, Mark A.; Jackson, Richard F. W.: A New Method for the Preparation of α-Nitroacetophenones

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231
Ballini, Roberto; Petrini, Marino; Marcantoni, Enrico; Rosini, Goffredo: Utilization of Basic Alumina in a One-Pot Synthesis of 1,4-Diketones, 1,4,7-Triketones, and Dihydrojasmone by Conjugate Addition of Nitroalkanes to Enones

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233
Thurkauf, Andrew; Jacobson, Arthur E.; Riee, Kenner C.: An Improved Procedure for the Preparation of Acetals from Diaryl Ketones

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234
Barluenga, José; Fernández-Simón, José L.; Concellón, José M.; Yus, Miguel: Highly Stereoselective Synthesis of Vinylsilanes from Carbonyl Compounds

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236
Suzuki, Hitomi; Aihara, Mie; Yamamoto, Hidetoshi; Takamoto, Yuuko; Ogawa, Takuji: Copper(I) Iodide-Assisted Halogen Exchange at Vinylic Positions. Conversion of Vinyl, Vinylene, and Vinylidene Bromides to the Corresponding Iodo Analogs

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238
Takahashi, Hiroshi; Tsubuki, Takeshi; Higashiyama, Kimio: A New Method for the Synthesis of α-Substituted Phenethylamines via Titanium Amide Complexes

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240
Son, Jong-Keun; Ramalingam, Kondareddiar; Woodard, Ronald W.: A Facile Synthesis of (+)-L-Discadenine and its Deuterio Derivatives

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242
Hosmane, Ramachandra S.; Lim, Benjamin B.: A Novel Method for the Synthesis of 9-Benzyl-6-(2-methylhydrazino)purine and 1-Methyl-4-(2-methylhydrazino)-1H-pyrazolo[3,4-d]pyrimidine

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244
Chimirri, Alba; Grasso, Silvana; Monforte, Pietro; Romeo, Giovanni; Zappalà, Maria: A Simple, One-Pot Synthesis of Novel 1H, 3H-Thiazolo-[3,4-a]benzimidazoles

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246
Latif, Nazih; Asaad, Fahmy M.; Grant, Nabil: A Simple, One-Step Synthesis of 3,4-Dihydro-4-phenacyl-2H-1,3-benzoxazin-2-ones

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248
Datta, A.; Ila, H.; Junjappa, H.: Reformatsky Reaction on Aroylketene S,N-Acetals: A Facile Route to 4-Amino-6-aryl-2H-pyran-2-ones

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250
Bengtsson, Marie; Liljefors, Tommy: DMPU: An Alternative to HMPT in Moth Sex Pheromone Synthesis

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252
Brownbridge, Peter; Jowett, Ian C.: 'One-Pot' Synthesis of Sulphinic Esters from Disulphides

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255
Mangeney, P.; Tejero, T.; Alexakis, A.; Grosjean, F.; Normant, J.: Titanium Induced Coupling of Imines to Symmetrical Vicinal (R*,R*)-Diamines

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257
Mizuno, Takumi; Nishiguchi, Ikuzo; Hirashima, Tsuneaki; Ogawa, Akiya; Kambe, Nobuaki; Sonoda, Noboru: Facile Synthesis of 4-Hydroxycoumarins by Sulfur-Assisted Carbonylation of 2′-Hydroxyacetophenones with Carbon Monoxide

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259
Houssin, Raymond; Bernier, Jean-Luc; Hénichart, Jean-Pierre: A Convenient and General Method for the Preparation of tert-Butoxycarbonylaminoalkanenitriles and Their Conversion to Mono-tert-butoxycarbonylalkanediamines

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261
Lwata, Chuzo; Watanabe, Mayumi; Okamoto, Shigeha; Fujimoto, Michitaro; Sakae, Masatoshi; Katsurada, Masanori; Imanishi, Takeshi: 5-Substituted 6-Amino-2,3-dihydroimidazo[2,1-b]thiazoles and 2-Amino-5,6-dihydrothiazolo[3,2-b]-1,2,4-triazole

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