Synlett

Issue 11 · November 1999

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1681
Coxon, James M.; Froese, Robert D. J.; Ganguly, Bishwajit; Marchand, Alan P.; Morokuma, Keiji: On the Origins of Diastereofacial Selectivity in Diels-Alder Cycloadditions

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1704
Lo Sterzo, Claudio: The Wonder of Palladium Catalysis: From Carbon-Carbon to Metal-Carbon Bond Formation. An Opportunity of Getting Astonishment from Reality

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letter
1723
Bertram, Anna; Hannam, Jeffery S.; Jolliffe, Katrina A.; González-López de Turiso, Felix; Pattenden, Gerald: The Synthesis of Novel Thiazole Containing Cyclic Peptides via Cyclooligomerisation Reactions

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1727
Cardillo, Giuliana; Gentilucci, Luca; Tolomelli, Alessandra; Tomasini, Claudia: A Practical Method for the Synthesis of β-Amino α-Hydroxy Acids. Synthesis of Enantiomerically Pure Hydroxyaspartic Acid and Isoserine

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1731
Mosimann, Hervé; Vogel, Pierre: Polyhydroxylated Perhydro-1H-benz[e]indenyl Derivatives with Two Angular 3a,5a-Carbaldehyde Moieties

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1735
Bandini, Elisa; Martelli, Giorgio; Spunta, Giuseppe; Bongini, Alessandro; Panunzio, Mauro: Synthesis of Perhydrooxazinones from 2-Aza-3-Trimethylsilyloxy-1,3-Butadiene. A General Route to 3,3-Disubstituted-β-Hydroxy Acids

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1739
Degl'Innocenti, Alessandro; Capperucci, Antonella; Scafato, Patrizia; Mecca, Tommaso; Reginato, Gianna; Mordini, Alessandro: The First Synthesis of α,β-Acetylenic Thioketones and Thioaldehydes

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1743
Chauhan, Kamlesh K.; Frost, Christopher G.; Love, Ian; Waite, David: Indium Triflate: An Efficient Catalyst For Acylation Reactions

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1745
Sabitha, Gowravaram; Abraham, Sunny; Subba Reddy, B. V.; Yadav, J. S.: Microwave Assisted Selective Cleavage of Sulfonates and Sulfonamides in Dry Media

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1747
Heber, Dieter; Stoyanov, Edmont V.: The Microwave Assisted Nucleophilic Substitution of 4-Hydroxy-6-methyl-2(1H)-pyridones

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1749
Ng, Po Ling; Lambert, John N.: Synthesis of Macrocyclic Inclusion Complexes Using Olefin Metathesis

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1751
Doi, Takayuki; Hijikuro, Ichiro; Takahashi, Takashi: A Novel Strategy for the Automated Synthesis of Bis-amides of 1,2-Diamines

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1754
Nakashima, Hiromi; Sato, Masayuki; Taniguchi, Takahiko; Ogasawara, Kunio: Lipase-mediated Resolution of cis-4-Cumyloxy-2-cyclopenten-1-ol and its Utilization for Enantioconvergent Preparation of (-)-Oxabicyclo[3.3.0]-oct-6-en-3-one

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1757
Ohi, Hidenori; Inoue, Susumu; Iwabuchi, Yoshiharu; Irie, Hiroshi; Hatakeyama, Susumi: Efficient Route to Functionalized Eight-Membered Lactones Based on Intramolecular Silicon-Directed Acylative Ring-Opening Reactions of 3-(Tetrahydro-2-furyl)propanoic Acid Derivatives

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1760
Fujita, Ken-ichi; Watanabe, Katsuhiro; Oishi, Akihiro; Ikeda, Yoshikazu; Taguchi, Yoichi: Preparation of Polymer-Supported Selenocyanates and their Application to Solid-Phase Oxyselenenylation-Deselenylation

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1763
Chaudhari, Sachin S.; Akamanchi, Krishnacharya G.: Thionyl Chloride-Benzotriazole in Methylene Chloride: A Convenient Solution for Conversion of Alcohols and Carboxylic Acids Expeditiously into Alkyl Chlorides and Acid Chlorides by Simple Titration

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1766
Sugimoto, Isamu; Shuto, Satoshi; Matsuda, Akira: Kinetics of a Novel 1,2-Rearrangement Reaction of β-Silyl Radicals. The Ring-expansion of (3-Oxa-2-silacyclopentyl)methyl Radical into 4-Oxa-3-silacyclohexyl Radical Is Irreversible

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1769
Takai, Kazuhiko; Hikasa, Shintaro; Ichiguchi, Tetsuya; Sumino, Naoki: One-Pot Transformation of RCHO to (E)-RCH=CHSiMe₃ Using CHI₃, Mn, Me₃SiCl, and a Catalytic Amount of CrCl₂

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1772
Shimizu, Masaki; Ishizaki, Shuji; Nakagawa, Hisashi; Hiyama, Tamejiro: Synthesis of Polysilacage Compounds Containing a Trisilane Bridge

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1775
Anada, Masahiro; Mita, Orie; Watanabe, Hiroko; Kitagaki, Shinji; Hashimoto, Shunichi: Catalytic Enantioselective Synthesis of the Phosphodiesterase Type IV Inhibitor (R)-(-)-Rolipram via Intramolecular C-H Insertion Process

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1778
Pon, Richard T.; Yu, Shuyuan: Efficient and Rapid Coupling of Nucleosides to Amino Derivatized Solid-Phase Supports

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1781
Bhattacharyya, Sukanta; Neidigh, Kurt A.; Avery, Mitchell A.; Williamson, John S.: Selective Monoalkylation of Ammonia: A High Throughput Synthesis of Primary Amines

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1784
Chen, Xiaoyuan; Chen, Xiaoyuan; Ji, Min; Fisher, Darrell R.; Wai, Chien M.: Monofunctionalization of Calix[4]arene Tetracarboxylic Acid at the Upper Rim with Isothiocyanate Group: First Bifunctional Chelating Agent for Alpha-Emitter Ac-225

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1790
Ishiyama, Tatsuo; Momota, Seiji; Miyaura, Norio: Platinum(0)-Catalyzed Diboration of Methylenecyclopropanes with Bis(pinacolato)diboron: A Selective Route to 2,4-Bis(boryl)-1-butenes

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1793
Uchida, Tatsuya; Irie, Ryo; Katsuki, Tsutomu: Highly cis- and Enantioface-Selective Cyclopropanation Using (R,R)-Ru-Salen Complex: Solubility Dependent Enantioface Selection

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1796
Kato, Toru; Hayakawa, Yoshihiro: A Facile Method for the Oxidation of Nucleoside H-Phosphonates to Phosphates with Bis(trimethylsilyl) Peroxide

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1799
Itoh, Takashi; Matsuya, Yûji; Enomoto, Yasuko; Nagata, Kazuhiro; Miyazaki, Michiko; Ohsawa, Akio: A Novel Synthesis of Chiral 1-Allyl-1,2,3,4-tetrahydro-β-carboline Employing Allyltributyltin and Chiral Acyl Chlorides

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1802
Knerr, Laurent; Schmidt, Richard R.: Application of a Ring Closing Metathesis Based Linker to the Solid Phase Synthesis of Oligosaccharides

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1805
Fritz-Langhals, Elke: Synthesis of Optically Active (2-Fluoroacyl)benzenes

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1808
Wolbers, P.; Hoffmann, H. M. R.; Sasse, F.: Structure-Activity Investigations of Analogues of the C15-C26 Phorboxazoles Segment

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1811
Alexakis, Alexandre; Benhaïm, Cyril; Fournioux, Xavier; van den Heuvel, Alexandra; Levêque, Jean-Marc; March, Sebastien; Rosset, Stephane: Catalytic Asymmetric Conjugate Addition on Macrocyclic and Acyclic Enones. Synthesis of R-(-)-Muscone

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1814
Hilgraf, Robert; Pfaltz, Andreas: Chiral Bis(N-tosylamino)phosphine- and TADDOL-Phosphite-Oxazolines as Ligands in Asymmetric Catalysis

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1817
Pfau, Roland; Kunz, Horst: Selectively Deprotectable Carbohydrates Based on Regioselective Enzymatic Reactions

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1820
Avolio, Salvatore; Malan, Christophe; Marek, Ilan; Knochel, Paul: Preparation and Reactions of Functionalized Magnesium Carbenoids

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1823
Hiersemann, Martin: The Pd(II)-Catalyzed and the Thermal Claisen Rearrangement of 2-Alkoxycarbonyl-Substituted Allyl Vinyl Ethers

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1826
Löffler, Frank; Hagen, Martin; Lüning, Ulrich: Concave Reagents 32: syn- and anti-Selective Cyclopropanation of Alkenes with Diazoacetates Catalyzed by Copper (i) Complexes of Concave 1,10-Phenanthrolines

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1829
Jolimaître, Pascale; André-Barres, Christiane; Malet-Martino, Myriam; Martino, Robert; Rico-Lattes, Isabelle: A New Method for the Synthesis of 5-Fluorouracil Prodrugs

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1832
Dupau, P.; Le Gendre, P.; Bruneau, C.; Dixneuf, P. H.: Optically Active Amine Derivatives: Ruthenium-Catalyzed Enantioselective Hydrogenation of Enamides

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1835
Gras, Jean-Louis; Bonfanti, Jean-François: New Synthetic Strategies Toward Pure Two-Component Triglycerides

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1838
Agami, Claude; Cheramy, Sandrine; Dechoux, Luc: Stereoselective α-Alkylation of New Chiral Auxiliaries: An Access to Enantiomerically Pure α- and α,β-Substituted β-Amino Acids

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1841
Deagostino, Annamaria; Balma Tivola, Paolo; Prandi, Cristina; Venturello, Paolo: A Short and Efficient New Synthesis of γ-Halo-Substituted α,β-Unsaturated Acetals and Carbonyl Compounds

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synlett spotlight
1844
Vollmer, Heidi R.: (4-Tolylsulfonyl)hydrazones FREE ACCESS

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