Synlett

Issue 04 · March 2004

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577
Inoue, Masayuki; Hirama, Masahiro: Total Synthesis of Ciguatoxin CTX3C, a Causative Toxin of Ciguatera Seafood Poisoning

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596
Spada, Gian Piero; Gottarelli, Giovanni: The Disclosure of the Stepwise Supramolecular Organization of Guanosine Derivatives: Serendipity or Programmed Design?

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603
Baba, Takayuki; Takai, Shigeyuki; Sawada, Naotaka; Isobe, Minoru: Stereoselective Synthesis of the Fully Functionalized HIJ-ring Framework of Ciguatoxin

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609
Adachi, Masaatsu; Tanaka, Hiroshi; Takahashi, Takashi: An Effective Sialylation Method Using N-Troc- and N-Fmoc-protected β-Thiophenyl Sialosides and Application to the One-pot Two-step Synthesis of 2,6-Sialyl-T Antigen

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615
Yasui, Yoshizumi; Koga, Yukiko; Suzuki, Keisuke; Matsumoto, Takashi: A Novel Approach to Erythrinan Alkaloids by Utilizing Substituted Biphenyl as Building Block

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619
Yasui, Yoshizumi; Suzuki, Keisuke; Matsumoto, Takashi: Transmission of Axial Chirality to Spiro Center Chirality, Enabling Enantiospecific Access to Erythrinan Alkaloids

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623
Kazmaier, Uli; Pohlman, Matthias: Regioselective Palladium-Catalyzed Allylic Alkylations via anti/syn-π-Allyl Intermediates

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627
Chakraborti, Asit K.; Gulhane, Rajesh: Zirconium(IV) Chloride as a New, Highly Efficient, and Reusable Catalyst for Acetylation of Phenols, Thiols, Amines, and Alcohols under Solvent-Free Conditions

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631
Vasudevan, Anil; Verzal, Mary K.: Neutral, Metal-free Hydration of Alkynes Using Microwave Irradiation in Superheated Water

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635
Tajbakhsh, Mahmood; Hosseinzadeh, Rahman; Lasemi, Zahra: Selective Iodination of Alcohols with NaI/Amberlyst 15 in Acetonitrile

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639
Muthusamy, Sengodagounder; Gunanathan, Chidambaram; Nethaji, Munirathinam: Stereoselective Epoxide Generation with Cyclic Rhodium Carbenoids: A New Access to Spiro-indolooxiranes

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643
Bakó, Péter; Bakó, Tibor; Mészáros, Attila; Keglevich, György; Szöllősy, Áron; Bodor, Sándor; Makó, Attila; Tőke, László: Phase Transfer Catalysed Asymmetric Epoxidation of Chalcones Using Chiral Crown Ethers Derived from d-Glucose and d-Mannose

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647
Balakumar, Vijayakrishnan; Aravind, Appu; Baskaran, Sundarababu: A Highly Regio- and Chemoselective Reductive Cleavage of Benzylidene Acetals with EtAlCl₂-Et₃SiH

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651
Suzuki, Masaki; Tomooka, Katsuhiko: Anionic Ring-Contraction Reaction of Cyclic Acetal System: Stereoselective Approach to Multi-Functionalized Oxetanes

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655
Kressierer, Christoph J.; Müller, Thomas J. J.: A Novel One-Pot Cycloisomerization-Wittig Sequence with Yne-Allyl Alcohols

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659
Ganguly, Nemai C.; Datta, Mrityunjoy: Ecofriendly Solid-State Oxidative Deprotection of 1,3-Dithianes and 1,3-Dithiolanes Using Ammonium Persulfate on Wet Montmorillonite K-10 Clay Support under Microwave Irradiation

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663
Lin, Mei-Jung; Sun, Chung-Ming: Focused Microwave-Assisted Parallel Synthesis of bis-Benzimidazoles

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667
Buschmann, Nicole; Wakamatsu, Hideaki; Blechert, Siegfried: An Easily Assembled Highly Active Ruthenium Initiator for Olefin Metathesis

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671
Kranke, Birgit; Hebrault, Dominique; Schultz-Kukula, Martin; Kunz, Horst: Arabinosylamine in Asymmetric Syntheses of Chiral Piperidine Alkaloids

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675
MacCoss, Rachel N.; Henry, Dara J.; Brain, Christopher T.; Ley, Steven V.: Catalytic Polymer-Supported Potassium Thiophenolate in Methanol as a Method for the Removal of Ester, Amide, and Thioacetate Protecting Groups

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679
Crackett, Peter; Demont, Emmanuel; Eatherton, Andrew; Frampton, Christopher S.; Gilbert, Jenny; Kahn, Irfan; Redshaw, Sally; Watson, William: HIV Protease Inhibitor Part 1: Use of Evans’ Oxazolidinone in Intermolecular Diels-Alder Reaction en route to 3,4-Substituted Cyclohexanones

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684
Demont, Emmanuel; Eatherton, Andrew; Frampton, Christopher S.; Kahn, Irfan; Redshaw, Sally: HIV Protease Inhibitors Part 2: [3+2] Cycloaddition, Isomerization; and Ring Expansion en route to 4,5-Substituted Cyclohexenones

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688
Behnke, Dirk; Taube, Roswitha; Illgen, Katrin; Nerdinger, Sven; Herdtweck, Eberhardt: Substituted 2-(Cyanomethyl-amino)-acetamides by a Novel Three-Component Reaction

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693
Koch, Guido; Loiseleur, Olivier; Altmann, Karl-Heinz: Total Synthesis of 26-Fluoro-epothilone B

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698
Štefane, Bogdan; Polanc, Slovenko: A New Regio- and Chemoselective Approach to β-Keto Amides and β-Enamino Carboxamides via 1,3,2-Dioxaborinanes

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703
Nishiwaki, Nagatoshi; Matsushima, Kazuo; Chatani, Miki; Tamura, Mina; Ariga, Masahiro: New Reactivity of Nitropyrimidinone: Ring Transformation and N-C Transfer Reactions

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708
Di Bari, Lorenzo; Guillarme, Stéphane; Hermitage, Stephen; Howard, Judith A. K.; Jay, David A.; Pescitelli, Gennaro; Whiting, Andrew; Yufit, Dmitrii S.: Lewis Acid-catalysed Aza-Diels-Alder versus Mannich Reactions of N-Diethyl Phosphoryl Imino Dienophiles with Oxygenated Dienes and Application of a Chiral Lewis Acid

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711
Guillarme, Stéphane; Whiting, Andrew: Unexpected Temperature, Time and Solvent Effects in the Catalytic Asymmetric aza-Diels-Alder Reaction of an Ethyl Glyoxylate-derived N-Aryl Imine with Danishefsky’s Diene Catalysed by a BINOL-Zinc Complex

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714
Panda, Gautam; Rao, N. Venugopal: A Short Synthetic Approach to Chiral Serine Azido Derivatives

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717
Mąkosza, Mieczysław; Judka, Marek: New Synthesis of Substituted Cyclopentanes via Reactions of γ-Chloro-carbanions with Electron-deficient Alkenes

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720
Bazán-Tejeda, Belén; Georgy, Marie; Campagne, Jean-Marc: Stereoselective Syntheses of the C1-C5, C7-C15 and C17-C24 Fragments of (+)-Discodermolide Using a Catalytic and Asymmetric Vinylogous Mukaiyama Reaction

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723
El Ashry, El Sayed H.; Ramadan, El Sayed; Hamid, Hamida M. Abdel; Hagar, Mohamed: Microwave Irradiation for Accelerating each Step for the Synthesis of 1,2,4-Triazino[5,6-b]indole-3-thiolsand their Derivatives from Isatin and 5-Chloroisatin

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726
Weigelt, Sven; Sewald, Norbert: Synthesis of ²H-Labelled α-Azidoisobutyryl Chloride (D₆-Azib-Cl) as ²H₆-Aib Equivalent Building Block in Peptide Synthesis

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729
De Paolis, Michaël; Chen, Xiaochuan; Zhu, Jieping: A Short Enantioselective Synthesis of Protected l-3-Hydroxy-4-methoxy-5-methyl Phenylalanine and its Corresponding Aldehyde - A Common Subunit of Ecteinascidin-743, Safracin and Congeners

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732
Takikawa, Hiroshi; Ishihara, Kazuaki; Saito, Susumu; Yamamoto, Hisashi: Asymmetric Vinylogous Direct Aldol Reaction Using Aluminum Tris[2,6-bis(4-alkylphenyl)phenoxide]

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735
Glaser, Thorsten; Liratzis, Ioannis: A Streamlined Synthesis for 2,7-Diformyl-1,8-naphthalenediol

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738
Bressette, Andrew R.; Glover IV, Louis C.: A Convenient One-Pot PCC Oxidation-Wittig Reaction of Alcohols

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741
Guo, Minjie; Li, Dao; Sun, Yanhui; Zhang, Zhaoguo: Selective Reduction of the Carbonyl Group in β,γ-Unsaturated α-Ketoesters by Transfer Hydrogenation with Ru-TsDPEN

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744
Sridhar, Perali Ramu: Chemistry of Tetrathiomolybdate and Tetraselenotungstate: Applications in Carbohydrate and Peptide Chemistry FREE ACCESS

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746
Jorapur, Yogesh R.: 1-Butyl-3-methylimidazolium Tetrafluoroborate as a Green Reaction Medium FREE ACCESS

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748
Sorg, A.; Siegel, K.; Brückner, R.: A Novel Access to γ-Alkylidenebutenolides: Sequential Stille Couplings of Dibromomethylenebutenolides FREE ACCESS

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