Synlett

Issue 03 · February 2005

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365
Rinner, Uwe; Hudlicky, Tomas: Synthesis of Amaryllidaceae Constituents - An Update

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388
Zezula, Josef; Hudlicky, Tomas: Recent Progress in the Synthesis of Morphine Alkaloids

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406
Miura, Katsukiyo; Wang, Di; Hosomi, Akira: Highly Regio- and Stereoselective Hydrostannylation of Propargyl Alcohols and Ethers Using Dibutylchlorostannane and Lithium Chloride

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411
Ernst, Tobias; Richert, Clemens: A Reactivity Test for HBTU-Activated Carboxylic Acids with Low Reactivity and Competitive Coupling of N-Methylpyrrole Derivatives

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417
Chin, Chin-Long; Tran, Duong Duc-Phi; Shia, Kak-Shan; Liu, Hsing-Jang: The Total Synthesis of Pygmaeocin C

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421
Wang, Bao-Yu; Huang, Jin-Wen; Liu, Le-Ping; Shi, Min: Highly Efficient and Stereoselective Construction of 1-Iodo- or 1-Phenylselenenyl-2-aryl-3-oxabicyclo[3.1.0]hexane from the Reaction of Arylmethylidenecyclopropylcarbinols with Iodine or Diphenyldiselenide

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425
Migianu, Evelyne; Guénin, Erwann; Lecouvey, Marc: New Efficient Synthesis of 1-Hydroxymethylene-1,1-Bisphosphonate Monomethyl Esters

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429
Le Roux, Rémi; Desroy, Nicolas; Phansavath, Phannarath; Genêt, Jean-Pierre: First Stereoselective Synthesis of the C(1)-C(13) Fragment of Dolabelides Using Ruthenium-SYNPHOS^®-Catalyzed Asymmetric Hydrogenation Reactions

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433
Tsujimoto, Takashi; Nishikawa, Toshio; Urabe, Daisuke; Isobe, Minoru: Synthesis of Functionalized Cyclopentane for Pactamycin, a Potent Antitumor Antibiotic

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437
Sun, Jiansong; Han, Xiuwen; Yu, Biao: First Total Synthesis of Caminoside A, an Antimicrobial Glycolipid from Sponge

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441
Gaillard, Stéphane; Papamicaël, Cyril; Marsais, Francis; Dupas, Georges; Levacher, Vincent: Preparation of 1,4-Dihydroquinolines Bearing a Chiral Sulfoxide Group: New Highly Enantioselective Recyclable NADH Mimics

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445
Gooßen, Lukas J.; Dezfuli, Mohammad K.: Practical Protocol for the Palladium-Catalyzed Synthesis of Arylphosphonates from Bromoarenes and Diethyl Phosphite

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449
Badetti, Elena; Moreno-Mañas, Marcial; Pleixats, Roser; Sebastián, Rosa M.; Serra, Anna; Soler, Roger; Vallribera, Adelina: Nucleophilic Aromatic Substitution on 4-Fluorophenylsulfonamides: Nitrogen, Oxygen, and Sulfur Nucleophiles

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453
Haase, Christian; Langer, Peter: Convenient Preparation of 5-Alkylidene-2,5-dihydropyrrol-2-ones by Ring-Transformations of γ-Alkylidenebutenolides: Formal Synthesis of Pukeleimide A

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457
Gupta, Arun Kumar; Kim, Ki Seong; Oh, Chang Ho: Pd-Catalyzed Addition of Organoboronic Acids to Alkynes at Room Temperature

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461
Bolm, Carsten; Saladin, Sandra; Claßen, Arno; Kasyan, Andrey; Veri, Elisabetta; Raabe, Gerhard: Enantiopure α-Silyl-Substituted α-Hydroxyacetic Acids Using O-H Insertion Methodology and Boron-Based Asymmetric Reductions

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465
Kreidler, Burkard; Baro, Angelika; Christoffers, Jens: A Poly(ethylene glycol) Supported Chiral Auxiliary for Asymmetric Michael Reactions

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469
Inoue, Seiichi; Wang, Ping; Nagao, Mami; Hoshino, Yujiro; Honda, Kiyoshi: One-Pot Stereoselective Synthesis of Pyrano[3,2-c]benzothiopyrans: A New Generation and [4+2] Cycloaddition of ortho-Thioquinonemethides

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473
Abbas, Muhammad; Neuhaus, Christiane; Krebs, Birte; Westermann, Bernhard: Catalytic Addition of Homoenolates to Imines - The Homo-Mannich Reaction

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477
Chevet, Caroline; Jackson, Toby; Santry, Barbara; Routledge, Anne: A Cleaner Approach to Solid-Supported Radical Chemistry: Application of Hypophosphite Salts to Intramolecular C-C Bond Formation on the Solid-Phase

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481
Dixon, Darren J.; Ley, Steven V.; Lohmann, Sophie; Sheppard, Tom D.: Synthesis of a Ceramide Sphingolipid as a Potential Sex Pheromone of the Hair Crab Erimacrus isenbeckii Using Butane-2,3-diacetal Desymmetrised Glycolic Acid Building Blocks

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485
Kuz’menok, Nina M.; Koval’chuk, Tatyana A.; Zvonok, Alexander M.: Synthesis of 5-Hydroxy- and 5-Amino-1-tosyl-5-phenyl-3-(2-arylvinyl)-4,5-dihydropyrazoles

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487
Tyrrell, Elizabeth; Al-Saardi, Ali; Millet, Julien: A Novel Silica-Supported Palladium Catalyst for a Copper-Free Sonogashira Coupling Reaction

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489
Somi Reddy, M.; Narender, M.; Rao, K. Rama: Regioselective Ring-Opening of Aziridines with Thiophenol in the Presence of β-Cyclodextrin in Water

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491
N’Zoutani, Marie-Ange; Lensen, Nathalie; Pancrazi, Ange; Ardisson, Janick: Total Synthesis of Rhizoxin D

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496
Vögtle, Markus M.; Marzinzik, Andreas L.: A Short and Efficient Protocol for the Solid-Phase Synthesis of Retro-Inverso Surrogates

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501
van Otterlo, Willem A. L.; Coyanis, E. Mabel; Panayides, Jenny-Lee; de Koning, Charles B.; Fernandes, Manuel A.: Tandem Catalysis: A Ring-Closing Metathesis Followed by Dehydrogenative Oxidation to Afford Substituted Indenones

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506
Surendra, K.; Krishnaveni, N. Srilakshmi; Rao, K. Rama: The Selective C-3 Opening of Aromatic 2,3-Epoxy Alcohols/Epoxides with Aromatic Amines Catalysed by β-Cyclodextrin in Water

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511
Stock, Christoph; Höfer, Frank; Bach, Thorsten: A Synthetic Approach to the Furanocembrane Carbon Skeleton by a Regioselective Bromine-Magnesium Exchange Reaction

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514
Ma, Shengming; He, Qiwen; Jin, Xin: Tunable 1,3-Lithium Shift of Propargylic/Allenylic Lithiums Formed by Conjugate Addition of 4-Aryl-3-butyn-1-enes with Organolithiums and the Subsequent Transmetalation/Pd(0)-Catalyzed Coupling Reaction with Aryl Halides

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517
Yoshino, Tomonori; Togo, Hideo: Facile Preparation of Polymer-Supported Methyl Sulfonate and its Recyclable Use for Methylation of Carboxylic Acids and Amines

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520
Gueyrard, David; Haddoub, Rose; Salem, Amine; Bacar, Nassib Said; Goekjian, Peter G.: Synthesis of Methylene Exoglycals Using a Modified Julia Olefination

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523
Saikia, Anil; Barthakur, Madan Gopal; Boruah, Romesh Chandra: Efficient Role of Mg-ZnCl₂ for Selective Reduction of α,β-Unsaturated Carbonyl Compounds in Aqueous Medium

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526
Wu, Zhimeng; Huang, Xian: Regioselective Hydrochalcogenation Reaction of 1,2-Allenyl Phosphine Oxides: A Novel Synthesis of b-Organochalcogenyl Allyl Phosphine Oxides

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529
Lightfoot, Andrew P.; Twiddle, Steven J. R.; Whiting, Andrew: 4,4,6-Trimethyl-2-vinyl-1,3,2-dioxaborinane: An Efficient and Selective 2-Carbon Building Block for Vinylboronate Suzuki-Miyaura Coupling Reactions

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532
Tron, Gian Cesare; Zhu, Jieping: A Three-Component Synthesis of (1,3-Oxazol-2-yl)-1,2-dihydro(iso)quinoline and its further Structural Diversifications

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535
Li, Bin Feng; Yuan, Ke; Dai, Li Xin; Hou, Xue Long: A Mild and Convenient Procedure for Desulfinylation of p-Toluenesulfinyl Amines

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538
Mathews, Christopher J.; Taylor, John; Tyte, Melloney J.; Worthington, Paul A.: Microwave Assisted Suzuki Reactions for the Preparation of the Antifungal 3-Aryl-5-methyl-2,5-dihydrofuran-2-ones

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541
Gogoi, Siddhartha: HOF·CH₃CN Complex FREE ACCESS

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543
Mishra, Jitendra Kumar: Oxaziridines FREE ACCESS

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