Synfacts

Issue 07 · July 2024

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A103
Zanda, Matteo: SYNFORM ISSUE 2024/07 FREE ACCESS

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Synthesis of Natural Products
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0671
Total Synthesis of (±)-Keramaphidin B and (±)-Ingenamine

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0672
Formal Total Synthesis of (±)-Arborisidine

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0673
Total Synthesis of (±)-Rhynchine E FREE ACCESS

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0674
Total Synthesis of Nominal Melognine

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0675
Total Synthesis of (+)-Randainin D

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0676
Total Synthesis of (±)-Pepluacetal

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0677
Total Synthesis of (+)-Saxitoxin FREE ACCESS

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Synthesis of Heterocycles
z0679
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0679
Asymmetric Hydrogenation of Heteroaromatics Using Brønsted and Lewis Acid Substrate Activation

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0680
Copper Catalysis for the Formation of Quaternary Carbon Containing Azepino[4,5-b]indoles

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0681
Synthesis of Versatile Pyridinimine Precursors to Access N-Heterocyclic Scaffolds

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0682
Base-Promoted Direct C–H Hydroxylation of N-Heteroarenes

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0683
‘Flash-Flow’ Generation and Exploitation of 3-Oxetanyllithium as a Reactive Nucleophile

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0684
Diaziridinones as an Amine Source for the Synthesis of Fused Indoles

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0685
Flow Synthesis of Functionalized 1,2,4-Triazolo[1,5-a]pyridines

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0686
Desmethyl SuFEx-IT as a Novel, Stable FSO₂ Donor for SuFEx Click Chemistry

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0687
Ylide-le Bit of Cycloaddition and Ylide-le Bit of Ring Expansion: Divergent Reactivity of Pyrazolium Ylides

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0688
One-Pot Synthesis of 1,2-Diamines

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0689
Direct Aryl/Aliphatic Amide Formation through Ring Opening of Non-Activated Aziridines

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0690
Synthesis and Reactivity of Housanes and Azahousanes in the Formation of 2-Azanorbornanes

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Synthesis of Materials and Unnatural Products
z0691
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0691
Polyethylene with Laddered Long-Chain Branching FREE ACCESS

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0692
Ligand-Tuned Open- and Closed-Shell Diborepins

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0693
Molecular Cages of Dibenzocyclooctatetraene

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0694
A Room-Temperature-Stable, Antiaromatic Cyclopentadienyl Cation

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0695
Cyclic Diaryl λ³-Bromanes for Regiodivergent Alkynylation

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0696
A Recyclable Polyolefin

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0697
Solventless Depolymerization of Nylon-6

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0698
Synthesis of carbo-Stilbenes

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0699
Tetra- and Dianionic [18]Annulenes

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0700
Radical and Cation Reactivity in One Ring

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0701
Cyanoketene Anion and Its Reactivity

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0702
Torsional Tension-Driven Polymerization

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Metals in Synthesis
z0703
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0703
Dyotropic Rearrangement of Tertiary Alcohols for the Synthesis of Fluorinated Tetrasubstituted Carbons FREE ACCESS

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0704
Copper-Catalyzed Enantioconvergent C(sp³)–N Cross-Coupling of Aryl Amines and α-Bromo Amides

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0705
Iridium-Photocatalyzed Hydrodecyanation of Alkyl Isonitriles with NHC–Borane FREE ACCESS

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0706
Nickel-Catalyzed Divergent Synthesis of Bisboronic Esters

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0707
Photoinduced Decarboxylative Aminoalkylation of Vinyl Cyclic Carbonates to Access Stereodefined Olefins

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0708
Alkene Dialkylation with Alkyl Halides and Hypervalent Iodine Reagents by Dual Photoredox/Nickel Catalysis

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0709
Two-Step Synthesis of 3-Amido-benzo[b]silines via Formal Silyformylation of Ynamides and Friedel-Crafts–Cyclization

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0710
Cobalt-Catalyzed Regiodivergent and Asymmetric Reductive Coupling of 1,3-Dienes with Aldehydes

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0711
Enantioselective Coupling of Aldehydes with C=O and C=N Bonds via Photoredox-Coupled Cobalt Catalysis

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0712
Synthesis of Chiral Naphthalene Isosteres via Copper-Catalyzed Hydroboration

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0713
Photocatalytic Aminoalkylation of Alkenes via a Brook Rearrangement Provides Access to γ-Amino Alcohols

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0714
Directed C–H Alkylation of Heterobiaryls via Iridium Catalysis

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0715
Enantioconvergent C(sp³)–C(sp) Cross-Electrophile Coupling Enabled by Halogen Atom Transfer

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0716
Manganese(I)-Catalyzed C(sp³)–H Bond Functionalization of 8-Methylquinolines

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0717
Nickel-Catalyzed Reductive Methylation of Secondary Mesylates with Methyl Tosylate

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0718
Synthesis of Polysubstituted Vinylsilanes via anti-Selective Carbosilylation of Alkynes

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0719
Asymmetric α-Alkylation of β-Ketocarbonyls by Photoredox-Iron-Chiral Primary Amine Triple Catalysis

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0720
Ru/Photocatalyzed Decarboxylative Coupling of α-Fluoroacrylic Acids with Difluoroalkyl Bromides

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0721
Photo-Induced Copper-Catalyzed C–H Arylation of 1,3-Azoles

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0722
Enantioselective Palladium-Catalyzed Synthesis of Polyarenes

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0723
Rhodium-Catalyzed Synthesis of Phenanthrenes from Biarylboronic Acids and Sulfoxonium or Iodonium Ylides

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0724
Nickel-Catalyzed Asymmetric Hydroalkylation of Alkenyl Fluorides

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0725
Direct Allylic C–H Amination of Alkenes with Amines to Branched Allylic Amines under Dual Catalysis

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0726
Turning Alkyl Iodides into Acyl Fluorides by Photoinduced Copper-Catalyzed Fluorocarbonylation

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0727
Pd(II)-Promoted Addition of Organometallic Reagents to Olefins: Pd-Catalyzed C–C Bond-Forming Reactions FREE ACCESS

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0728
2,5-Hydrofunctionalization of Allene-Ynes

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Polymer-Supported Synthesis
z0729
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0729
Amination of Aryl Chlorides via Benzynes Catalyzed by Sodium Alkoxide Clusters FREE ACCESS

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0730
Synthesis of Thioxoimidazolidinones Bearing 4-Indolyl/Indenyl Substituents in Water

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0731
Continuous-Flow Asymmetric Hydrogenation Using a Silica-PS-Supported Homochiral Iridium Catalyst

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0732
Dehydrogenation of α-Cyclohexene-Substituted Nitriles to Benzyl Cyanides

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0733
C–H Annulation of Benzoic Acids and Alkynes Using Rh (III) Complex Immobilized onto COF-316

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0734
Controlled Hydrogenation of Nitroarenes to Bisaryldiazene Oxides with Single Atomic Co on Nb₂O₅

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0735
Chemoselective Carbene Insertion of N−H Bond Using a Single-Atom Rhodium Catalyst

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0736
An Anthraquinone-Based COF: A Direct Hydrogen-Atom Transfer Photocatalyst for C–N/C–C Couplings

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0737
Sulfur-Tolerant Reductive Amination by Ruthenium Phosphide Nanoparticles Supported on Carbon

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0738
Borylation of Aryl Halides Using a Nickel-Based MOF

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Organo- and Biocatalysis
z0739
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0739
Photocatalysis Enables the Hydroamidation of Alkenes Using Sulfonyl Azides and Hantzsch Esters FREE ACCESS

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0740
Photocatalyst Enables the Phosphonylation of Unactivated C(sp³)–H Bonds

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0741
Brønsted Acid Catalyzes Intramolecular Allylic Substitution Reaction of Allylic Alcohols

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0742
Organocatalytic Asymmetric Construction of Vicinal Stereocenters via α-Alkylation

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0743
Decarboxylative Sulfhydrylation of Carboxylic Acids Enabled by Multimodal Acridine Photocatalysis

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0744
N-Heterocyclic Carbenes Catalyze the Formation of Fused 6-5-5 Tricyclic Natural-Product Frameworks

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0745
Enantioselective Access to β,β-Difluorinated Carbocycles

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0746
Stereodivergent Radical Cyclizations Enabled by Directed Evolution of Fatty Acid Photodecarboxylases

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0747
Hydrodeamination through in situ Generation of Diazonium Species by ortho-Naphthoquinone Catalysis

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0748
Organocatalytic Stereodivergent Intramolecular Synthesis of Spiroaminals

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0749
Asymmetric Photoredox Catalytic de Mayo Reaction

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Innovative Drug Discovery and Development
z0751
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0751
Using Artificial Intelligence to Identify TRAF2- and NCK-Interacting Kinase as a Target for Fibrosis FREE ACCESS

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0752
Late-Stage Aromatic-Ring Reduction within Drug Molecules

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0753
Mastering Cell Penetration: Wash-Free Fluorogenic Probes for Membrane Damage FREE ACCESS

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0754
An 8 Step Total Synthesis of Tabernanthine and Ibogaline

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0755
Late-Stage Diversification of Phenol Containing Compounds via para- to meta-Isomerization

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0756
Ligand-Controlled Divergent Coupling with Cobalt Catalysis

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0757
A Copper Metallaphotoredox-Catalyzed Dehydroxylative Radical Approach to N-Glycosylation

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0758
Synthesis of Ferulic Acid Derivatives Uncovers Potential Candidate for Alzheimer’s Disease Management

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0759
TNG908, a Clinical Candidate for PRMT5 Inhibition Exploiting Synthetic Lethality with MTAP

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0760
LXRβ-Selective Tricyclic Agonist Developed with New [4σ+4π] and [4σ+4π–1] Cycloaddition Strategy

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0761
Discovery of a Potent and Long-Acting Seretonin 5-HT₂ Receptor Agonist

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0762
Substrate-Induced Regioselectivity in Intermolecular [2+2+2] Cyclotrimerizations

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0763
Mechanistic Studies and Reaction Calorimetry Enable Safe Scale-up of a Reduction with NaBH₄ and TFA

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0764
Ester Synthesis from Methyl Ketones

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0765
A Classic Route to the Synthesis of Tamiflu^® FREE ACCESS

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Peptide Chemistry
z0767
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0767
Utilizing Proline Surrogates in the Synthesis of ‘Difficult’ Peptides FREE ACCESS

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0768
Photoredox-Catalyzed C–H Decyanative Pyridination of N-Arylated Glycine Derivatives with Cyanopyridines

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0769
Photoredox-Catalyzed C–H Alkylation of N-Arylated Glycine Derivatives

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0770
Synergistic Pd/Cu Catalysis for the Synthesis of Unnatural Quaternary Amino Acids

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0771
Deoxyfluorinated Amidation of Carboxylic Acids Using Pyridinesulfonyl Fluoride

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0772
The Peptide Backbone-Targeted Installation of (4H)-Imidazolone cis-Amide Bioisosteres Synthetic Strategy

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0773
Deprotection of Fmoc Group Using Catalytic Amounts of DMAP under Solvent-Free Conditions

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0774
[2,3]-Sigmatropic Rearrangement for the Synthesis of Unnatural α,α-Disubstituted α-Amino Acid Derivatives

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0775
Dual Metal-Catalyzed Electrocatalytic Synthesis of Unnatural Amino Acids

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0776
AlCl₃- and HFIP-Mediated Selective Deprotection of the N-Cbz Group

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0777
Ir-Catalyzed Synthesis of β-Substituted α-Amino Acids Using Alkene and Glycine Derivatives

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0778
Distal Amino Acids Formation by Amidation of Cyclic Ketones

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0779
Efficient Method for the Synthesis of N-Methylated Peptides FREE ACCESS

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0780
Synthesis of Amino Acids with Axially Chiral Diaryl Ethers Units

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Flow Chemistry
z0781
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0781
Oxidative Asymmetric Catalysis via Microfluidic Flow Electrochemistry

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0782
Scalable Synthesis of Glycerol Carbonate Using Serially Connected Mesofluidic-Plate Reactors

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