Synfacts

Issue 11 · November 2008

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A104
SYNFORM ISSUE 2008/10 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
1125
Synthesis of QS-7-Api

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1126
Synthesis of ent-Abudinol B

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1127
Synthesis of (+)-Cortistatin A FREE ACCESS

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1128
Synthesis of (+)-Minfiensine

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1129
Synthesis of (-)-Pumiliotoxin C

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1130
Synthesis of Sanguiin H-5

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1131
Synthesis of Macbecin I

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1132
Formal Synthesis of (-)-Platensimycin

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1133
Synthesis of (+)-Nangustine

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1134
Synthesis of ()-Platencin

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1135
Synthesis of (+)-Cermizine D

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1136
Synthesis of ()-Axinellamines A and B

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1137
Synthesis of an Inhibitor of HCV Polymerase

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1138
Synthesis of (+)-Hirsutene

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1139
Synthesis of Bryostatin Analogues

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Synthesis of Heterocycles
1141
An Undemanding Synthesis of Thiazolo[4,5-d]pyridines

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1142
Three-Component Synthesis of Epoxides and Aziridines via Sulfur Ylides

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1143
Halogen Electrophile Induced Cyclization Route to Isoquinoline N-Oxides

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1144
3-Formylchromone to Quinoline Interconversion

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1145
Synthesis of 3-Chlorofurans and 5-Chlorofuropyrimidine Nucleosides FREE ACCESS

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1146
Ni-Catalyzed Conversion of 1,2,3-Benzo-triazin-4-ones into Isoquinolones

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1147
Pt-Catalyzed Cyclization of Propargylic Oxiranes to Substituted Furans

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1148
Intramolecular Aza-Wittig Route to 2-Aryl Indoles

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1149
Synthesis of 2,5-Dihydro-(1H)-pyrrol-2-ones from Pyruvate, Aldehydes and Anilines

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1150
AgNO₃-Catalyzed 5-endo-dig Cyclizations to Form Pyrazole N-Oxides and Pyrazoles

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1151
Cu-Catalyzed Huisgen Cycloaddition of Sulfonyl Azides ‘on Water∏

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1152
Synthesis of 4-Azidotetrahydropyrans via Prins Cyclization

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1153
Synthesis of Fluorinated Heterocycles via Prins Cyclization in Ionic Liquids

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1154
3-Amino-2(1H)-pyridinones from 1,3-Oxazolon-5-ones by a Multicomponent Reaction

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1155
One-Pot Synthesis of Tetrahydroquinolines by an Imino-Diels-Alder Reaction

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Synthesis of Materials and Unnatural Products
1157
Octacarboxy Spherosilicate

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1158
Large exTTF-Based Dendrimers

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1159
Stilbene/Cyclodextrin-Based Muscular Dimer

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1160
A Mild Access to Aryl Magnesium Reagents

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1161
Diels-Alder Synthesis of Trisbicyclo[2.2.1]heptabenzene FREE ACCESS

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1162
Fluorescence Indicator for Zn^²+/Hg^²+ Exchange

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1163
Efficient Five-Fold Ethynlylation of Corannulenes

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1164
Monodisperse Oligodiacetylenes

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1165
Ring-Opening Polymerization of Pyridinium Salts

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1166
High Sulfur-Content Polyimides

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1167
A Ratiometric Turn-on Cobalt Sensor

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1168
Cyclopenta[def]phenanthrene Polymers Go Green

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
1169
Desymmetrization of 1,3-Diols Using a Dinuclear Zinc Catalyst

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1170
Asymmetric Synthesis of Dienyl Alcohols

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1171
Catalytic Hydrodefluorination of Perfluorinated Compounds FREE ACCESS

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1172
Synthesis of Asymmetric Allenes with Chiral Copper Nucleophiles

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1173
Copper-Catalyzed 1,4-Reduction of α,β-Unsaturated Esters

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1174
Scandium-Catalyzed Hydroxymethylation of Silicone Enolates in Water

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1175
Iridium-Catalyzed Hydrogenation of 7,8-Dihydro-quinolin-5(6H)-ones

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1176
Acyclic Stereocontrol in Iridium-Catalyzed Hydrogenations

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1177
Copper-Catalyzed Addition of Diethylzinc to Boc-Protected Imines

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1178
Asymmetric Trapping of an Alcoholic Oxonium Ylide with Aldehydes

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1179
Synthesis of Terminal Epoxides via Dimethylsulfonium Methylide to Ketones

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1180
Mannich Reaction of β-Keto Phosphonate with a Dinuclear Ni Complex

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1181
Conjugate Additions Using a Water-Soluble Chiral Diene Ligand

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1182
Stereoselective Olefination Promoted by Rieke Manganese

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1183
Ligand-Controlled Palladium-Catalyzed Asymmetric Allylic Alkylations

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1184
Enantioselective Amination of Benzylic and Allylic C-H Bonds

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1185
Rhodium(I)-Triethylamine-Catalyzed 1,4-Addition of Enones

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1186
Pd-Catalyzed Asymmetric Synthesis of α-Hydroxy Ketones, Acids and Esters

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1187
Novel Tridentate Aminophenol Ligand for Alkylzinc Additions

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1188
Oxindole Synthesis by Palladium-Catalyzed Cyanoamidation

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1189
Titanium-Catalyzed Asymmetric Alkylation of Aldehydes Using Trialkylboranes

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1190
New Chiral Diene Ligands for Iridium-Catalyzed [3+2] Annulation

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1191
Enantioselective Desymmetrization via Ring Opening of Strained Alkenes

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1192
Ruthenium-Lithium Complex for the Cyanosilylation of Aldehydes

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1193
1,4-Addition of Alkyl and Aryl-Aluminums to Cyclic Enones

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1194
Copper-Catalyzed Cycloaddition of Bis-Sulfonyl Ethylene

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1195
Vanadium-Catalyzed Enantioselective Cyanoformylation of Aldehydes

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1196
Asymmetric Reformatsky Reaction with ortho-Substituted Diarylketones

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1197
Coupling of Acetylene and Aldehydes Applied to l-Hexoses Synthesis

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Metal-Mediated Synthesis
1199
Dehydrohalogenation of Alkyl Halides with Complementary Regioselectivity FREE ACCESS

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1200
Cu(II)-Mediated Cyclopropylation of Amides and Azoles

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1201
Efficient Sonogashira Coupling of Aryl Chlorides

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1202
Direct Pd-Catalyzed Acylation of Aryl Bromides with Aldehydes

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1203
Cu(I)-Promoted Synthesis of Chloromethyl Ketones from CCl₃-Carbinols

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1204
Oxidative Cyanation of Tertiary Amines

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1205
C-OH Bond Activation and Arylation of Tautomerizable Heterocycles

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1206
Water-Mediated Catalyst Preactivation for Efficient Pd-Catalyzed Aminations

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1207
Stereospecific α-Deprotonation of N-Protected Aziridines

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1208
Highly Selective Chelate-Controlled Heck-Miyaura Coupling Reaction

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1209
Dehydrogenative Cyclocondensation of Dialkylsilanes Providing Oxasilacyclopentenes

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1210
Stereospecific Synthesis of Allenes from Propargylic Alcohols

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1211
Cu-Mediated C-H Bond Arylation with Arylboronic Acids

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1212
Simple Conversion of Esters to Primary Amides Using Magnesium Nitride

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Organo- and Biocatalysis
1213
Synthesis of (R)-Pantolactone

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1214
α-Aminophosphonate-Catalyzed Michael Addition of Nitroalkanes to Enones

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1215
Catalytic Asymmetric Morita-Baylis-Hillman Reactions of Imines

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1216
Simple Carboxylic Acids as Cofactor in Asymmetric Protonation

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1217
Catalytic Asymmetric Synthesis of Aza-β-Lactams

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1218
Gold-Free Aldol-Type Additions of α-Isothiocyanato Imides to Aldehydes FREE ACCESS

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1219
A New Organocatalytic Domino Sequence

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1220
Quaternary α-Amino Acids and Derivatives

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1221
Asymmetric Synthesis of N,O-Aminals

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1222
Broad Scope Organocatalytic Aza-Michael Addition

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1223
Organocatalytic Mannich and Biginelli Reaction in Total Synthesis

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Polymer-Supported Synthesis
1225
Sonogashira Coupling with Pd/C

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1226
A New Solid-Phase Linker: Cu-Assisted Amide Bond Cleavage

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1227
Resin-Bound Pyrrolidine Catalysts for Enamine-Mediated Reactions FREE ACCESS

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1228
Microwave-Based Heck Reaction with Palladium Nanoparticles

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1229
Asymmetric Allylic Substitution in Water with a Polymeric Pd Catalyst FREE ACCESS

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1230
Asymmetric Hydrogenation of Ketones Using MSN-Supported Ruthenium Catalysts

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1231
Asymmetric Diels-Alder Reaction Using a Montmorillonite-Entrapped Organocatalyst

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1232
The Kharasch Reaction in Water with an Amphiphilic Polymeric Ru Catalyst

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1233
Solvent-Free Organic Transformations with Amberlite IRA900F

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1234
Reduction of Carbonyl Compounds with Supported Gold Catalysts

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1235
Hydrolytic Kinetic Resolution with Resin-Supported Co-(Salen) Catalysts

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1236
Polyisobutylene-Supported Pyridyl N-Oxide Catalyst for Allylation

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1237
Solid-Phase Synthesis of Benzodiazepine Derivatives

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1238
Preparation of Propargylamines via Multicomponent Reaction with Cu(I) Zeolites

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Addenda and Errata
1239
Rapidly Switching Photochromic Dyes

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