Synlett

Issue 06 · June 1999

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657
Brückner, Reinhard; Suffert, Jean: The Bis(enol triflate) Route to Dienediyne Models of the Biradical Forming and DNA-Cleaving Natural Product Neocarzinostatin Chromophore

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680
Butenschön, Holger: π Complexes with Annellated Cyclobutene Rings: Bicyclo[3.2.0]heptadienyl Anion and Benzocyclobutene as Ligands for Transition Metals

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letter
692
Ishiwata, Akihiro; Sakamoto, Satoshi; Noda, Takeshi; Hirama, Masahiro: Synthetic Study of Pinnatoxin A: Intramolecular Diels-Alder Approach to the AG-ring

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695
Nitta, Aiko; Ishiwata, Akihiro; Noda, Takeshi; Hirama, Masahiro: Synthetic Study of Pinnatoxin A: Intramolecular Alkylation Approach to the G-ring

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697
Taillefumier, Claude; Lakhrissi, Mohammed; Chapleur, Yves: Two Novel Strategies for the Construction of the Core Acetal of the Zaragozic Acids

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701
Ernholt, Bettina V.; Thomsen, Ib B.; Jensen, Kenneth B.; Bols, Mikael: Synthesis of (+)-Azafagomine from D-xylose

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705
Takeda, Kei; Tanaka, Tadashi: Formation of Four- to Six-Membered Carbocycles by Tandem Brook Rearrangement-Intramolecular Michael Reaction

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709
Ramasamy, Kanda S.; Averett, Devron: O-(Benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium Tetrafluoroborate (TBTU): A New Reagent for the Cleavage of Tetrahydropyranyl, Silyl and 4,4′-Dimethoxytrityl Ethers

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713
Barrero, Alejandro F.; Alvarez-Manzaneda, E. J.; Alvarez-Manzaneda, R.; Chahboun, Rachid; Meneses, R.; Aparicio B, Marta: Ring A Functionalization of Terpenoids by the Unusual Baeyer-Villiger Rearrangement of Aliphatic Aldehydes

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717
Yang, Jun; Li, Chao-Jun: Indium-Trichloride Mediated Synthesis of 4,4-Dichlorotetrahydropyrans

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719
Enders, Dieter; Klein, Daniela: A Novel Enantioselective Synthesis of α-Azido Ketones

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721
Zhong, Ping; Huang, Xian; Xiong, Zhi-Xing: A Stereoselective Synthetic Route to (E)-2-Arylvinylphosphonates

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723
Usami, Yoshihide; Numata, Atsushi: Total Syntheses of Trichodenones A-C

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725
Lamarre, Caroline; Stella, Lucien: First Synthesis of 2,4-Bis(trifluoroacetyl)-6-dimethylaminopentafulvene by a Sequence of Reactions Involving DMF, Trifluoroacetic Anhydride, and Cyclopentadiene

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727
Agami, Claude; Cheramy, Sandrine; Dechoux, Luc; Kadouri-Puchot, Catherine: A New Chiral Auxiliary Derived from (2S)-Phenylglycinol: an Access to Enantiomerically Pure β-Amino Acids

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729
Ooi, Takashi; Tayama, Eiji; Yamada, Masao; Maruoka, Keiji: Efficient Synthesis of Aromatic sec-Amides from Esters: Synthetic Utility of Bislithium Amides

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731
Kitamura, Tsugio; Wasai, Kanako; Todaka, Mitsuru; Fujiwara, Yuzo: Synthesis and Reactions of a Hypervalent Iodine-Benzyne Precursor Possessing an Ester Group

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733
Terao, Keiji; Kunishima, Munetaka; Tani, Shohei: Organoselenium-Induced Cyclization of 2-Alkenylthiazolines to Functionalized γ-Lactams

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735
Li, Chao-Jun; Chen, Dong-Li: Eight-Membered Thiocycloether via Indium-Mediated Ring Enlargement

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737
Kuribayashi, Takeshi; Gohya, Sayako; Mizuno, Yumiko; Shimojima, Masayuki; Ito, Kazuhiro; Satoh, Susumu: Bis C-Glycosylated Diphenylmethanes for Stable Glycoepitope Mimetics

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741
Enders, Dieter; Müller, Stephan F.; Raabe, Gerhard: Asymmetric Synthesis of α-Substituted β-Amino Sulfones by aza-Michael Addition / α-Alkylation

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744
Hodgson, David M.; Foley, Anne M.; Lovell, Peter J.: Alkene Chemoselectivity in Ring-Closing Metathesis: A Formal Synthesis of (-)-Periplanone-B

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747
Enders, Dieter; Otten, Thomas: α-Silyl Controlled Asymmetric Michael Additions of Acyclic and Cyclic Ketones to Nitroalkenes

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750
Schmittel, Michael; Ammon, Horst: Preparation of a Rigid Macrocycle with Two Exotopic Phenanthroline Binding Sites

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753
Yu, Biao; Yu, Hai; Hui, Yongzheng; Han, Xiuwen: Trichloroacetimidate as an Efficient Protective Group for Alcohols

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756
Funabiki, Kazumasa; Nakamura, Hiroko; Matsui, Masaki; Shibata, Katsuyoshi: One-pot Preparation of 2,6-Disubstituted 4-(Trifluoromethyl)pyrimidines via the Tandem Cyclization, Dehydration, and Oxidation Reaction of α,β-Unsaturated Trifluoromethyl Ketones Using POCl₃-Pyridine-Silica Gel and MnO₂ Systems

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759
Bódai, Viktória; Novák, Lajos; Poppe, László: Synthesis and Lipase-Catalyzed Enantiotope Selective Acetylation of 2-Benzoyloxy-1,3-propanediol

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762
Bedjeguelal, Karim; Bolitt, Véronique; Sinou, Denis: Intramolecular Heck Cyclisation-β-Alkoxy Elimination in Carbohydrate Chemistry. A Simple Route to Enantiopure Annelated Dioxatricyclic Compounds

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765
Torrens, Antoni; Castrillo, JoséA.; Claparols, Alex; Redondo, Jordi: Enantioselective Synthesis of (R)- and (S)-Cizolirtine; Application of Oxazaborolidine-Catalyzed Asymmetric Borane Reduction to Azolyl Phenyl Ketones

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768
Sugihara, Takumichi; Okada, Yoshinari; Yamaguchi, Masahiko; Nishizawa, Mugio: A Novel Carbonylative Decomplexation of Alkyne-Dicobalt Hexacarbonyls: Hydrocarbamoylation of Alkynes

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771
Sugihara, Takumichi; Yamada, Mamiko; Yamaguchi, Masahiko; Nishizawa, Mugio: The Intra- and Intermolecular Pauson-Khand Reaction Promoted by Alkyl Methyl Sulfides

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774
Tanaka, Hideo; Tokumaru, Yoshihisa; Torii, Sigeru: Synthesis of 3-Alkenyl-Δ³-cephems via Sequential Reductive 1,2-Elimination/Addition/Cyclization in an Alkenyltin/Copper(I) Chloride/bpy System

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777
Curini, Massimo; Epifano, Francesco; Marcotullio, Maria Carla; Rosati, Ornelio: Oxone®: A Convenient Reagent for the Oxidation of Acetals

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780
Matsushima, Tomohiro; Zheng, Bao-Zhong; Maeda, Hiroshi; Nakajima, Noriyuki; Uenishi, Jun-ichi; Yonemitsu, Osamu: Synthetic Studies of Tedanolide. 4. Stereoselective and Efficient Synthesis of the C13-C23 Part

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783
Miura, Keishi; Katsuki, Tsutomu: Dynamic Control of Ligand Conformation: Asymmetric Epoxidation Using Achiral (Salen)manganese(III) Complex

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786
Damour, D.; Pulicani, J.-P.; Vuilhorgne, M.; Mignani, S.: cis- and trans-3-(3-Indolyl)proline Derivatives as Conformationally Restricted Analogues of Tryptophan

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789
Martins, Marcos A. P.; Bastos, Giovani P.; Sinhorin, Adilson P.; Flores, Alex F. C.; Bonacorso, Helio G.; Zanatta, Nilo: Regiochemistry of the Reaction of 2-Acylcyclohexanones with Trimethyl Orthoformate: A Convenient One-Pot Method to Obtain 7,7-Dimethoxy Alkanoate Methyl Esters

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792
Coutrot, Philippe; Grison, Claude; Tabyaoui, Mohamed; Tabyaoui, Badia; Dumarçay, Stéphane: Towards a Synthesis of Glucidic Phosphoenol Pyruvic Acid Derivatives

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795
Genski, Thorsten; Macdonald, Gregor; Wei, Xudong; Lewis, Norman; Taylor, Richard J. K.: Epoxidation of Electron Deficient Alkenes Using tert-Butyl Hydroperoxide and 1,5,7-Triazabicyclo[4.4.0]dec-5-ene and its Derivatives

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798
Castro, Francisco J. Freire; Vila, Manuel M.; Jenkins, Paul R.; Sharma, Madan L.; Tustin, Gary; Fawcett, John; Russell, David R.: The Addition of Diallylzinc to 5-Substituted 4,5-Dihydroisoxazoles

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801
Vanelle, Patrice; Benakli, Kamel; Giraud, Luc; Crozet, Michel P.: Synthesis of Tetrasubstituted Ethylenic Compounds from a gem-Trichloroimidazole Derivative by Electron Transfer Reactions

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804
Namyslo, Jan Christoph; Kaufmann, Dieter E.: Asymmetric Synthesis of Both Enantiomers of N-Protected Epibatidine via Reductive Heck-Type Hetarylation

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807
Ollivier, Cyril; Chuard, Rachel; Renaud, Philippe: TEMPO-Induced Generation of Alkyl Radicals from B-Alkylcatecholboranes

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810
Yeh, Chih-Ming; Sun, Chung-Ming: Rapid Parallel Synthesis of Benzimidazoles

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813
Toshima, Kazunobu; Kasumi, Ken-ichi; Matsumura, Shuichi: Novel Stereocontrolled Glycosidations of 2-Deoxyglucopyranosyl Fluoride Using a Heterogeneous Solid Acid, Sulfated Zirconia (SO₄/ZrO₂)

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816
Chen, Chien-Tien; Hon, Sang-Wen; Weng, Shiue-Shien: Oxovanadium(IV) Complex-mediated Catalysis in Mukaiyama-type Aldol Additions

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819
Roberts, Christopher D.; Schütz, Rolf; Leumann, Christian J.: The Synthesis of a Thymine Containing E-Olefinic Peptide Nucleic Acid (OPA) Monomer

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822
Baccolini, Graziano; Boga, Carla: New Feature of Friedel-Crafts Phosphonation of Anisoles: Unexpected In Situ Methylphosphorylation Reaction

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new tools in synthesis
825
Jäschke, Andres; Frauendorf, Christian; Hausch, Felix: In Vitro Selected Oligonucleotides as Tools in Organic Chemistry FREE ACCESS

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synlett spotlight
834
Sommermann, Thomas: Ceric(IV) Ammonium Nitrate FREE ACCESS

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