Synfacts

Issue 02 · February 2006

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Synthesis of Natural Products and Potential Drugs
0095
Synthesis of (±)-Renieramycin G

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0096
Synthesis of (-)-CP55,940

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0097
Synthesis of (-)-Spirotryprostatin B

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0098
Synthesis of (+)-Lithospermic Acid

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0099
Synthesis of clastro-Lactacystin β-Lactone

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0100
Synthesis of (+)-Rollimembrin

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0101
Synthesis of Erythronolide

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0102
Synthesis of Psymberin/Irciniastatin A

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0103
Synthesis of Ningalin D

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0104
Synthesis of (S)-1-Amino-5-phosphonoindan-1-carboxylic Acid [(S)-APICA]

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0105
Synthesis of Aflatoxin B₂

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0106
Synthesis of Dictyodendrin B

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0107
Synthesis of Anisomycin

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0108
Synthesis of Spiro-oxindole MDM2 Inhibitors

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Synthesis of Heterocycles
0109
Chiral Pyrrolines via Asymmetric 1,3-Dipolar Cycloaddition Reactions

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0110
Synthesis of Carbazoles by Tandem C-H Activation and Buchwald-Hartwig Amination

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0111
A Concept for the Regioselective Synthesis of 1,2,3-Triazoles

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0112
Regioselective Synthesis of 4-Fluoroalkyl Isoquinolines

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0113
Indium(III)-Mediated Synthesis of Quinoline-4-carboxylic Acid Derivatives

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0114
Aromatizing Route to Benzo-, Benzofuranyl-, and N-Tosylindolenyl-isoindolines

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0115
Synthesis of Azabiaryls by a non-Cross-Coupling Method

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0116
A C-H Insertion Route to Fused Indoles

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0117
Convenient Synthesis of Isoxazoles

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0118
Synthesis of Endothiopeptides via Ugi Reaction and their Conversion to Thiazoles

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0119
Synthesis of Functionalized 2,3-Indoline-Fused Cyclobutanes

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0120
Multisubstituted Pyridines from 1,2,4-Triazines by Diels-Alder Chemistry

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0121
Oxazinones as Synthetic Intermediates for Enantiomerically Pure β-Amino Acids

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0122
Regioselective Lithiation of (S)-Nicotine

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Synthesis of Materials and Unnatural Products
0123
Biodiesel Made with a Sulfonated Solid Catalyst

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
0125
Ir-Catalyzed Asymmetric Ketimine Hydrogenation

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0126
All-Carbon Quaternary Stereogenic Centers via Cu-Catalyzed Conjugate Additions

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0127
Regioselective Hydrosilylation of Unsymmetrical Aryl Alkynes

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0128
Tandem Carbocupration/Oxygenation of Terminal Alkynes

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0129
[2,3]-Sigmatropic Rearrangement of Sulfur Ylides

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0130
Asymmetric Hydroformylation of [2.2.1]-Bicyclic Olefins

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0131
Cu-Catalyzed Enantioselective Aziridination of Chalcones

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0132
Biginelli Reaction Using a New Chiral Ytterbium Catalyst

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0133
Synthesis of β-Amino Ketones and β-Amino Alcohols

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0134
Trans- and cis-Selective Lewis Acid-Catalyzed Hydrogermylation of Alkynes

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0135
Intramolecular [4+2] Cycloaddition of Nitroalkenes

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0136
Synthesis of Chiral, All-Carbon Quaternary Centers via Allylic Alkylation

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0137
Ir(I)/Phosphoramidite-Catalyzed Asymmetric Allylic Amination

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0138
1,3-Dipolar Cycloaddition of Azomethine Ylides

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0139
Synthesis of Chiral Fluorous Oxazolidinone Auxiliaries

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0140
Enantiospecific Synthesis of Tetrahydrofurans via Cyclopropane Cycloaddition

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0141
Rhodium-Catalyzed 1,4-Addition of Arylzinc Reagents

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0142
Enantioselective Conjugate Addition of R₂Zn to α,β-Unsaturated Aldehydes and Ketones

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0143
One-Pot Conversion of Alkynyl Ketones into Saturated Chiral Alcohols

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0144
Al-Catalyzed Enantioselective Dialkylzinc Addition to α-Ketoesters

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0145
Yb(III)-Catalyzed Asymmetric Aldol-Tishchenko Reaction

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0146
Regioselective Heck Couplings of α,β-Unsaturated Tosylates and Mesylates

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Metal-Mediated Synthesis
0147
Kumada Coupling of Aryl and Vinyl Tosylates under Mild Conditions

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0148
Asymmetric Propargylation with Trimethylsilyl-9-borabicyclo[3.3.2]decanes

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0149
Pd-Catalyzed Hydrosilylative Coupling of Alkenes with Alkynes

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0150
Pd-P(t-Bu)₃-Catalyzed Cross-Coupling of Silanes with Aryl Halides

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0151
Silver-Catalyzed Asymmetric Allylation of Ketones with Allyl Silanes

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0152
Re-Catalyzed Hydrosilylation of Ketones with Et₃SiH

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0153
Chromium-Mediated Synthesis of Polycyclic Aromatic Compounds

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0154
Catalytic Asymmetric Allene Diboration/Allylation/Functionalization

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0155
Synthesis of Allylic Amines from Allylic Ethers and Zirconocene Imides

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0156
Cu-Catalyzed Stereoselective Reaction of Allylic Carbonates with Diboronate

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0157
Solvent-Free Asymmetric Alkylzinc Additions to Ketones

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0158
Asymmetric Conjugate Addition to α,β-Unsaturated Chiral Sulfinyl Imines

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0159
Surprisingly Efficient Catalytic Cr-Mediated Reactions

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Organo- and Biocatalysis
0161
Dynamic Kinetic Resolution of Primary Amines

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0162
Synthesis of 3,4-Dihydropyran-2-ones Catalyzed by Quaternary Ammonium Phenoxide

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0163
Mechanism of Phosphine-Catalyzed Cyclo-Oligomerization of Isocyanates

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0164
Brønsted Acid-Catalyzed Imine Amidation

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0165
Lipase-Catalyzed Michael Addition

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0166
A General Organocatalyst for the Asymmetric Direct α-Functionalization of Aldehydes

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0167
Hydrogenation Using Chemogenetically Optimized Chemzymes

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0168
A Highly Efficient Catalyst for the Enantioselective Direct Aldol Reaction

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0169
Organocatalytic Asymmetric Aza-Henry Reaction

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0170
DPP-IV Inhibitor by Proline-Catalyzed Mannich Reaction

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0171
Highly Regioselective Tandem Morita-Baylis-Hillman/Aldol Cyclization

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Polymer-Supported Synthesis
0173
Sintered Polyethylene Chips-Supported Pd, Rh and Ru Catalysts

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0174
Synthesis of 3-Amino-1,2,4-benzothiadiazine 1,1-Dioxides

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0175
A Traceless Solid-Phase Approach to Functionalized Tetramic Acids

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0176
PS-PEG-Supported Proline Catalysis for Aldol Reaction

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0177
Recycable Ligand-Free Mesoporous Pd Catalysts for Heck Reaction

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0178
Acidic and Basic Supported Reagents for One-Pot Synthesis of Benzo[b]thiophenes

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0179
Solid-Phase Synthesis of New Heterocyclic Azoniaspiro Ring Systems

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0180
A Highly Active and Reusable Heterogeneous Ruthenium Catalyst

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0181
Solid-Phase Synthesis of Pyrroloisoquinoline

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0182
Ceria/Vinylpyridine Polymer Nanocomposite-Catalyzed Biginelli Reaction

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0183
Solid-Phase Synthesis of Pyrazoledicarboxylic Acid Derivatives

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0184
Gram-Scale Synthesis of N-Aryl- and N-Aryl-N¢-methylpiperazines on PEG

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