Synfacts

Issue 01 · January 2007

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Issue
Synthesis of Natural Products and Potential Drugs
0001
Synthesis of the α-C-Glycoside Analogue of KRN7000

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0002
Synthesis of (-)-Deoxyharringtonine

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0003
Synthesis of (±)-β-Erythroidine FREE ACCESS

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0004
Synthesis of (±)-Magnofargesin

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0005
Synthesis of Valilactone

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0006
Synthesis of (+)-Intricarene

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0007
Synthesis of (-)-Rhazinilam

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0008
Synthesis of DOV21947

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0009
Synthesis of (+)-Gigantecin

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0010
Synthesis of Jimenezin

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0011
Synthesis of (-)-Swainsonine

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0012
Synthesis of cis-Solamin

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0013
Synthesis of (±)-Aspidophytine

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0014
Synthesis of Iejimalide B

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0015
Synthesis of (+)-Tetronolide

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Synthesis of Heterocycles
0017
Pd-Catalyzed Sequential C-N and C-C Coupling Route to 2-Vinylindoles

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0018
Diastereoselective Hydroamination Route to Hexahydroindoles

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0019
Pyrroles and Pyrazoles by a C-N Coupling-Hydroamination Sequence FREE ACCESS

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0020
Enantioselective Synthesis of Oxazolidinones

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0021
Synthesis of Benzothiazol-3-ones

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0022
Fluorous-Phase Synthesis of α-Methyleneγ-lactones

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0023
4-Difluoromethylene-1-Pyrrolines by Intramolecular Heck Cyclization

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0024
Pericyclic Ring Closure of Ketenimines to Quinolinones

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0025
An S_RN1 Route to 3-Substituted and Fused Isoquinolin-1-(2H)-ones

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0026
Gold-Catalyzed Synthesis of Pyrrole-Fused Heterocycles

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0027
Synthesis of 1,3-Oxathiolan-5-ones and Benzoxathian-4-ones

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0028
Chiral Benzothiopyrans by Organocatalysis

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0029
Metal-Free Synthesis of Indolines

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0030
2-Alkenylfurans via Feist-Benary and Wittig Reactions

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0031
Substituted Thiophenes via Intramolecular Thia-anti-Michael Addition

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Synthesis of Materials and Unnatural Products
0033
β-Glucopyranoside Cage Receptor

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0034
Tetrasulfonamide Macrocycles

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0035
Functionalization of Nanodiamond

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0036
Synthesis of TMS-Modified Polymethylenes

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0037
A Reusable Ring-Enlarging Catalyst

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0038
Preparation of Novel Tetrathia[7]helicenes

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0039
Stacked Conjugated Oligothiophenes

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0040
Porphyrin-Chlorin Dyads by 1,3-Dipolar Cycloaddition

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0041
Bent Radical Cation Dimers from Bicyclooctene-Substituted Terthiophenes

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0042
Fluorophore Formed in Ambient Light by two Ring Closures

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0043
New Fullerene Electronic Acceptors and Acids

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0044
Molecular Switches for Photorelease

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0045
Control of Helicity in a Metal Complex

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0046
Synthesis of a Hexafluorocyclopentene-Annelated Thiophene Monomer

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
0047
Asymmetric Silylboronation of Allenes

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0048
Au(I)-Catalyzed Diastereoselective Tandem Addition/Carbocyclization

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0049
Intermolecular Asymmetric Hydroamination

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0050
Catalytic Enantioselective Imino-Reformatsky Reaction

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0051
Enantioselective Radical Additions to Acyloxy Pyrones

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0052
Enantioselective Resolution of Ketone Nitroaldol Products

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0053
Palladium-Catalyzed Enantioselective Conjugate Reduction of Enones

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0054
New Ligands: Hydroxyoxazolinyl[2.2]paracyclophanes in Asymmetric Catalysis

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0055
Enantioselective Copper-Catalyzed Nitroaldol Reaction

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0056
Enantioselective Synthesis of β-Lactone Catalyzed by a Chiral Oxazaborolidine

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0057
Au(I)-Catalyzed Formal Hydroamination of Chiral Allenes to 3-Pyrrolines

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0058
Stereoselective Synthesis of N-Alkylaziridines from N-Chloroamines

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0059
Cu(I)-Catalyzed Stereoselective Formation of Tertiary Alkyl-Aryl Ethers

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0060
Role of the X Anion in the VO(salen) (X)-Mediated Cyanohydrin Synthesis

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0061
Chemodivergent Formation of Furanones and Piperidines

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0062
Ferrocenophane Diphosphine Ligands for Pd-Catalyzed Allylic Substitution

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0063
Regioselective Cuprate Additions to Tethered Allylic Phosphates

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0064
Rhodium-Catalyzed Intramolecular [4+2] Cycloaddition

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0065
[3+2] Annulation of N-Ts-α-Amino Aldehydes and 1,3-Bis(silyl)propenes

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0066
Asymmetric Palladium-Catalyzed [3+2] Cycloaddition

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0067
N,O,P-Ligand for Cu(II)-Catalyzed Enantioselective Conjugate Additions

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0068
Complementary Stereoselectivity in Pt-Catalyzed Silaboration of Alkenes

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0069
Chiral Quaternary Carbon Stereocenters via Diene-yne [2+2+2] Cycloaddition FREE ACCESS

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0070
Dynamic Kinetic Resolution of Benzoins by Lipase-Ru Catalysis

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0071
2,5-Disubstituted Furans via Diastereoselective Friedel-Crafts Reaction

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0072
Bifunctional Inverse Electron Demand Hetero-Diels-Alder Reactions

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0073
Cu-Catalyzed Asymmetric Synthesis of α,β-Unsaturated δ-Lactones

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0074
Achiral Additives for Enhancing the Stereoselectivity of Cycloadditions

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0075
Rh-Catalyzed Asymmetric Synthesis of 2-Substituted Pyrrolizidinones

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Metal-Mediated Synthesis
0077
Iron-Catalyzed Allylation of Ketones

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0078
Asymmetric Ni Phosphite Catalyzed Trialkylaluminum Addition to Aldehydes

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0079
Direct LiCl-Promoted Insertion of Zinc into Organic Iodides and Bromides FREE ACCESS

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0080
Direct Lewis Acid Promoted C-Allylation of Alcohols with Allylsilanes

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0081
Ru-Catalyzed Regiospecific Borylation of Methyl C-H Bonds

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0082
Lipase/Aluminum-Catalyzed Dynamic Kinetic Resolution of Alcohols

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0083
Reduction of Oxygen Functionalities to Alkanes with Alkylsilanes

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0084
Pd(II)-Catalyzed Addition of Boronic Acids to Nitriles

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0085
Ni-Catalyzed Intramolecular Enal-Alkyne [3+2] Reductive Cycloaddition

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0086
Stereoselective Preparation of Silyloxy-Alkenylcopper Species from Acylsilanes

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0087
AlMe₃-DABCO-Promoted Synthesis of Amides

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0088
Rh-Catalyzed Hydrogenation of Olefins with Zn Metal and Water

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0089
Cu-Catalyzed β-Boration of Michael Acceptors with Bis(pinacolato)diboron

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Organo- and Biocatalysis
0091
Nonenzymatic Kinetic Resolution of Indolines

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0092
Highly Enantioselective Synthesis of 1,4-Benzoxazinones and α-Amino Acids

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0093
First Organocatalytic Asymmetric Biginelli Reaction FREE ACCESS

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0094
Chiral Chromenes via Domino Oxa-Michael-Aldol Reaction

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0095
Enzymatic Kinetic Resolution of β-Hydroxy Ketones

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0096
Highly Enantioselective Organocatalytic Michael-Aldol Domino Reactions

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0097
Asymmetric Synthesis of Isoquinuclidines

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0098
Enantioselective Radical Addition of Alkyl Halides to Glyoxylate Oxime Ether

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0099
Phase-Transfer-Catalysis of Direct Mannich Reaction of Malonates with N-Carbamoylimines

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0100
Chiral N-Heterocyclic Carbene Catalyzed Oxodiene Diels-Alder Reactions

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0101
Aziridination of Chalcones Using Tertiary Amine Catalysts

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Polymer-Supported Synthesis
0103
CD-Monitored HTS of Chiral Catalysts FREE ACCESS

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0104
Solid-Phase Synthesis of β-Lactam Analogues

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0105
Allylic Azidation in Water

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0106
An Efficient Synthesis of Five-Membered N-Heterocycles

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0107
A Facile One-Pot Synthesis of Polymer-Supported 1,1′-Bi(2-naphthol)s

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0108
Enantioselective Hydrogenation Using a PEG-Supported Biphep-Ru Complex

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0109
Asymmetric Aldol Reaction in Water Using Dendrimer-Supported Proline

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0110
Poly(norbornene)-Supported N-Heterocyclic Carbenes

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0111
Safety Asymmetric π-Allylic C1-Substitution with Nitromethane in Water

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0112
Heteropolyacid-Functionalized Silica Catalyst for the Acylal Formation

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0113
Synthesis of Poly(ethylene glycol) Supported Benzazepines

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0114
α-Alkylation of Nitriles Promoted by Hydrotalcite-Supported Catalysts

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0115
Polymer-Supported m-Hydrobenzoin-Derived Chiral Auxiliary

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