Synfacts

Issue 06 · June 2006

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Synthesis of Natural Products and Potential Drugs
0531
Synthesis of Palominol and Dolabellatrienone

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0532
Synthesis of an NO-Releasing Prodrug of Rofecoxib

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0533
Synthesis of CJ-15,161 via Cu-Catalyzed N-Arylation

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0534
Synthesis of (±)-Gelsemine

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0535
Synthesis of (±)-Physostigmine

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0536
Synthesis of UCS1025A

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0537
Synthesis of (-)-N-Acetylcolchinol

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0538
Synthesis of (±)-Bipinnatin J

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0539
Synthesis of (±)-Bipinnatin J

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0540
Synthesis of Spiruchostatin A

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0541
Synthesis of Ecteinascidin 743

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0542
Synthesis of (-)-7-Demethylpiericidin A₁

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0543
Synthesis of Tarchonanthuslactone

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0544
Synthesis of Sceptrin and Ageliferin

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0545
Synthesis of Lamellarin L

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Synthesis of Heterocycles
0547
Gold-Catalyzed Pictet-Spengler Reactions

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0548
Palladium(II)-Catalyzed Cyclization of 3-(3′-Alkenyl)indoles to Carbazoles

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0549
Dearomatization Route to Cyclohexadienone Spirolactams

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0550
Synthesis of a Fused β-Lactone via Pyridine-Assisted [2+2] Cycloaddition

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0551
Asymmetric Alkynylation of Isoquinoline Iminium Salts

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0552
Pictet-Spengler Synthesis of Thiazolo- and Pyrazolo-quinolines

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0553
Synthesis of Indazole Derivatives Involving Aryl Nitrene Species

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0554
One-Pot Synthesis of Imidazophenanthridinium Salts

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0555
Metal-Mediated Heterocyclic Annulation to Indolopyrrolidines

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0556
Palladium-Catalyzed C-N Bond Coupling Reactions. Aminopyrimidine Synthesis

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0557
Pd(II)-Catalyzed Synthesis of Tetrahydrocarbazoles and 3-Substituted Indoles

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0558
Synthesis of Perhydroindolines by Ring-Opening/Ring-Closing Metathesis

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0559
Three-Component Diastereoselective Synthesis of Imidazooxazines

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0560
Rhodium-Catalyzed N-Allylation of Thymine

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0561
Synthesis of 3,4,5-Trisubstituted Pyridines from Baylis-Hillman Adducts

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Synthesis of Materials and Unnatural Products
0563
Efficient Synthesis of Helicenes

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0564
Fluorescent Dyes Highly Aligned in Nematic Liquid Crystals

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0565
Ultramicroporous Polymers for Hydrogen Storage by Design

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0566
A Chiral 1,8-Anthrylene-Ethynylene Tetramer

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0567
Fullerobutenes

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0568
Phenacenes from Diels-Alder Trapping of Photogenerated o-Xylylenols

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0569
Dendrimer Carbodiimides Mediated Lactamization

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0570
Suzuki-Miyaura Cross-Coupling Providingcis-Poly(arylenevinylene)s

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0571
A One-Pot Synthesis and Functionalization of Polyynes

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0572
Poly(p-fluoranthene vinylene)

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0573
A Fused Selenocycle as a Stable Organic Semiconductor

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0574
Liquid-Crystalline Electronic Polymers for Transistors

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
0575
Synthesis of Chiral Allylic Phosphine Oxides

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0576
Asymmetric Friedel-Crafts Addition of Indoles to N-Sulfonyl Aldimines

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0577
Stereoselective Nucleophilic Monofluoromethylation of Sulfinylimines

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0578
New Efficient Chiral Pentamethylferrocene Phosphinooxazoline Ligands

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0579
Asymmetric Allylation of Aldehydes Using a Chiral Cr(III) Complex

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0580
Chiral Enones via Asymmetric Allylic Oxidation

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0581
Convergent Asymmetric Alkylation from meso and dl Carbonates

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0582
Catalytic Enantioselective Hydrogenation of Quinolines and Isoquinolines

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0583
Improved Ru Catalyst for Enantioselective Hydrogenation of Ketones

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0584
Pd(II)-Catalyzed Enantioselective Synthesis of Indolines

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0585
Catalytic Asymmetric Synthesis of cis-Vicinal Diamine Derivatives

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0586
Rhodium-Catalyzed Imine-Directed C-H Bond Functionalization

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0587
Synthesis of Propargylamines via a Three-Component Coupling Reaction

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0588
A New Lipase/Vanadium Combination for DKR of Allyl Alcohols

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0589
Resolution of 2-Aminocyclohexanol Derivatives and Applications

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Metal-Mediated Synthesis
0591
Efficient Aldol Addition of Simple Thioesters

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0592
Diastereoselective Synthesis of Chiral 3-Aryl-1-alkynes from Bromoallenes

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0593
Catalytic Asymmetric Addition of Dimethylzinc to α-Keto Esters

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0594
Cross-Coupling of Organoindium Reagents with Propargylic Esters

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0595
Enantioselective Pd-Catalyzed Arylation ofN-Boc-Pyrrolidine

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0596
Creation of Chiral Quaternary Stereocenters via a Multicomponent Reaction

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0597
Synthesis and Reactions of Stannylated Allylic Alcohols

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0598
Conjugate Addition of Alkyl Iodides to Alkenenitriles in Water

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0599
Radical Phosphination of Organic Halides and Thioates

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0600
Pd-Catalyzed Addition of Arylboronic Acids to Alkynes Using O₂ as an Oxidant

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0601
Three-Component Synthesis of Benzhydrylamines from Arylzinc Halides

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0602
Metallation-Addition Reactions of Enantiopure Aromatic Sulfoxides

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0603
Cu-Catalyzed Carbometallation of Propargylic Alcohols by Grignard Reagents

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Organo- and Biocatalysis
0605
Trichlorination of l-Leucin by Fe(II) Halogenases

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0606
Biocatalyzed α-Hydroxylation of Phenyl-acetic Acid Derivatives and Buspirone

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0607
Biocatalytic Deuterium- and Hydrogen-Transfer using Over-Expressed ADH-‘A’

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0608
Hydroacylation of Activated Ketones Catalyzed by N-Heterocyclic Carbenes

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0609
Enantioselective Michael Addition of
N-Heterocycles to Nitroolefins

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0610
Epoxycyclohexanones via Organocatalytic Asymmetric Domino Reactions

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0611
Asymmetric Michael Reaction Catalyzed by Chiral Ionic Liquids

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0612
Organocatalytic Asymmetric Mannich Reaction of Malonates with Imines

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0613
Asymmetric Strecker Reaction Catalyzed by a Brønsted Acid

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0614
PmHNL-Catalyzed Synthesis of Aliphatic(R)-Cyanohydrins

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0615
Enamine Catalysis for the Direct Asymmetric Hydroxyamination

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0616
Direct Nucleophilic Acylation of Nitroalkenes

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Polymer-Supported Synthesis
0617
Heck Reaction Using a New N-Heterocyclic Carbene Palladium Complex on Silica

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0618
Release of the Product from the Polymer Support under Neutral Conditions

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0619
Development of Supported Salen Catalysts

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0620
Solid-Phase Synthesis of Oligo[(1,4-phenyleneethynylene)-alt-(2,5-thiopheneethynylene)]s

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0621
A New Strategy Towards the Efficient Solid-Phase Synthesis of Cyclopeptides

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0622
A Continuous-Flow Process for Natural Product Synthesis

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0623
A Semicarbazide Resin for the Synthesis of Peptide Ketones

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0624
Solid-Phase Synthesis of 2-Alkyl-4,6-diamino- and 2,4,6-Triaminopyrimidines

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0625
Polymer-Incarcerated (PI) Pd-Catalyzed Semi-Hydrogenation of Alkynes

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0626
α-Alkylation of Ketones with Alcohols Using a Polymer-Nano-Pd Catalyst

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0627
Polymer-Supported Synthesis of Pyridines via [2+2+2] Cycloaddition

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0628
Staudinger Ligation Using Solid-Supported Phosphinethiol

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0629
Expanding the Utility of One-Pot Multistep Reaction Networks

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0630
Debenzylation of Aryl Benzyl Ethers by Using Solid-Supported Acids

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0631
Synthesis of Peptide-^αThiophenylesters for Native Chemical Ligation

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0632
Solid-Phase Synthesis of Coumarins via ipso Substitution Reaction

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