Synlett

Issue 05 · March 2025

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431
Guo, Haoxin; Rajca, Andrzej: Chiral π-Conjugated Double Helical Aminyl Diradical with the Triplet Ground State

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438
Li, Pengfei; Qiu, Youai: Reductive Electrophilic Cross-Coupling for Constructing C(sp³)–C(sp³) Bonds

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445
Singha, Tushar; Hari, Durga Prasad: Visible-Light-Mediated Strain-Release Radical Spirocyclizations: Access to Functionalized Spirocyclobutanes

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452
Zeng, Jun; Li, Yajie; Li, Feiyan; Zhou, Sisi: Comparison of the Activity for Theaflavin Production by a Recombinant Polyphenol Oxidase and a Commercial Enzyme

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459
Keesara, Srinivasa Reddy; Bolla, Ratnasekhar; Bharathkumar, Hanumantharayappa; Andugulapati, Sai Balaji; Gundekari, Sreedhar; Varkolu, Mohan: Synthesis, Characterization, and Biological Applications of Tetramethylpiperidinyl Triazolopyridazine Derivatives

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464
Zhong, Jianming; Li, Shuangshuang; Wang, Zhaoxin; Zhou, Wang: 1,2-Diaroyl Benzofurans: Synthesis and Photochromic Properties

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468
Odagi, Minami; Shimizu, Yuta; Sugimoto, Kota; Mori, Io; Xu, Ban; Tan, Choon Hong; Nagasawa, Kazuo: Enantioselective Oxidative Homocoupling of 2-Oxindoles with a Chiral Bisguanidinium Hypoiodite Catalyst

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474
Yang, Bo; Wang, Xin; Chai, Yao; Xu, Wen-Bo; Tian, Ya-Ling; Ma, Yong-Jun; Alduma, Anwar I.; Cao, Xin-Rui; Wang, Xi-Cun; Chen, Dong-Ping; Quan, Zheng-Jun: Direct Synthesis of N-Substituted Phosphinecarboxamides from [TBA][P(SiCl₃)₂] and Isonitriles

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480
Li, Zheyao; Ju, Lei; Bao, Ruipeng; Lin, Xinbo; Wang, Teng; Yu, Xinhong: N-Heterocyclic Carbene Catalyzed Reassembly of Dibenzyl Ethers: Facile Access to α-Hydroxy Ketones

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484
Huang, Hong-Li; Li, Shan; Lv, Yong-Zheng; Shi, Ya-Qian; Liu, Chang-Bo; Peng, Zhongzhong; Gao, Fei: Efficient Metal-Free Synthesis of Heterotriarylmethanes by 1,4-Addition of Benzofuran Azadienes

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488
Sahu, Satya Narayan; Shaw, Ranjay; Althagafi, Ismail; Pratap, Ramendra: Transition-Metal-Free Approach for the Synthesis of N-Arylated Piperidones and their Ketals from Ketene Dithioacetals

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496
Bremerich, Maximilian: Access to 1,3- and 1,5-Disubstituted 1,2,4-Triazoles by Condensation of Acyl Hydrazides with Formamidinium Acetate

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504
Menna, Tim J.; Kerr, Michael A.: Synthesis of the (±)-trans-Whiskey and Cognac Lactones via a Donor–Acceptor Cyclopropane Hemimalonate

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508
Novikov, Alexander S.; Malkov, Georgiy V.; Akkuratov, Alexander V.: Selection of Conditions for the Synthesis of Methacrylate Monomers Based on Adamantane

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512
Fraser, Tommy; Harbour, Zakiel; Voyer, Normand; Cardinal, Sébastien: Chemo- and Regioselective Demethylation of 2-Bromo-α-resorcylic Acid Derivatives Using Alkylthiolate Salts

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517
Wan, Jie; Xiao, Guozhi: One-Pot Assembly of Octasaccharide Motif from Cranberry Arabinoxyloglucan Oligosaccharides

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522
Sathe, Balaji Dashrath; Meenakshi, Meenakshi; Murti, Yogesh; Mane, Madhav Shivaji; Pandey, Sarvesh Kumar; Mahajan, Shriya; Rawat, Pramod; Kandhari, Harsimrat; Goel, Kapil Kumar; Dwivedi, Ashish Ranjan; Rathod, S. V.: Development of New N-{4-[(7-Chloro-5-methylpyrrolo[2,1-f] [1,2,4]triazin-4-yl)oxy]-3-fluorophenyl}benzenesulfonamide Analogues: Exploring Anticancer Potential through MerTK Inhibition

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531
You, Hui; Liu, Daming; Pan, Mengni; Shen, Yue; Li, Yang; Li, Wanfang: Base-Promoted Reaction between N-Acyl Benzotriazoles and p-Toluenesulfonylmethyl Isocyanide (TosMIC): A Facile Synthesis of 4,5-Disubstituted Oxazoles

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536
Masal, Dattatraya P.; Reddy, D. Srinivasa: Gram-Scale Synthesis of (±)-Tylophorine

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541
Bai, Song; Liu, Lin; Wu, Rong; Tang, Shouyin; Wan, Suran; Wang, Fang; Wei, Xian; Chen, Lijun; Xu, Shunyi; Li, Miao: Synthesis and Biological Evaluation of Novel Coumarin Derivatives Bearing a Sulfonamide Moiety as Antiviral and Antibacterial Agent

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546
Sano, Shigeki; Yamada, Shoki; Ihara, Takahito; Seki, Kazumasa; Kitaike, Syuji; Nakao, Michiyasu: Synthesis of Methyl 2-[Bis(benzylthio)phosphoryl]acetate as a Novel Horner–Wadsworth–Emmons-Type Reagent and Its Application to the Diastereodivergent Synthesis of (E)- and (Z)-α,β-Unsaturated Esters Open Access

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551
Fujita, Hikaru; Kato, Toshiyuki; Betsuyaku, Tatsuki; Kunishima, Munetaka: Development of a Purely Isolable (Dimorpholino)triazine-Based Reagent for the Epoxidation of Alkenes

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556
Rupanawar, Bapurao D.; Bansode, Ajay H.; Suryavanshi, Gurunath: Hypervalent-Iodine-Mediated Base-Free Oxidative Olefination of Benzylic Amines to Access α,β-Unsaturated Ketones

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561
Takahashi, Hikaru; Shibata, Takashi; Naito, Daisuke; Murakami, Ryo; Inagaki, Fuyuhiko: Synthesis of Chiral L₂/Z-Type Ligands Featuring a Bisoxazoline Framework and Their Application to Palladium-Catalyzed Asymmetric Allylic Alkylation

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566
Dai, Hao-Tian; Huang, Xu-Lun; Cheng, Yuan-Zheng; You, Shu-Li: Nickel-Catalyzed Radical Hydroalkylative Dearomatization of Indoles with Alkyl Bromides

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571
Cheney, Hunter B. D.; Zevitz, Elise S.; Herbrechtsmeier, Madeline G.; Dhimitruka, Ilirian: Microwave-Assisted Synthesis of Fluorescent 8-Aryl-7-deazaguanines

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576
Hansen, Jonathan Kirschner Solberg; Nielsen, Mogens Brøndsted: Synthesis of Bifluorenylidene- and Cycloocta[1,2,3-jk:6,5,4-j′k′]difluorene-Extended Tetrathiafulvalenes: Novel Multi-Redox Systems

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