Synfacts
Issue 06 · June 2011
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Synform
A46
SYNFORM
ISSUE 2011/06
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Synthesis of Natural Products and Potential Drugs
z577
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0577
Synthesis of NS9544 Acetate
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0578
Synthesis of an hNK-1 Receptor Antagonist
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0579
Synthesis of the Biaryl Core of Anacetrapib
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0580
Synthesis of Kempene-2
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0581
Synthesis of
ent
-Seragakinone A
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0582
Synthesis of (±)-Stemoamide
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0583
Synthesis of a CXCR3 Antagonist
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0584
Synthesis of EBC-23
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0585
Synthesis of Efavirenz
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0586
Synthesis of AMG 837
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0587
n
-Nitric Oxide Synthase Inhibitor
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0588
Synthesis of Variecolortides A and B
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0589
Synthesis of ABT-341
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0590
Enantioselective Synthesis of (+)-Salvileucalin B
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0591
Syntheses of Guanacastepenes N and O
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Synthesis of Heterocycles
z593
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0593
Rhodium-Catalyzed Synthesis of Isoquinolines from Oximines and Alkynes
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0594
Transition-Metal-Free S
N
Ar-Type Synthesis of Chromones
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0595
Synthesis of 1,3-Thiazoles from Nitrostyrenes and Aromatic Thioamides
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0596
Palladium-Catalyzed C-H Activation/C-N Coupling Route to 1-Aryl-1
H
-benzotriazoles
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0597
Gold-Catalyzed Hydroamination-Hydroarylation Route to Fused Indoles
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0598
Tetrahydropyranoquinolinone via a Knoevenagel Reaction
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0599
Synthesis of Quinazolinones by Combined Ullmann Coupling-Oxidative C-H Amidation
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0600
One-Pot Synthesis of Indoles and N-Fused Indoles from Nitriles
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0601
Nickel-Catalyzed Dehydrogenative [4+2]-Cycloaddition Route to Dihydropyridones
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0602
A Catalyst-Free MCR Approach to 1,5-Benzodiazepines
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0603
A Boronic Acid Catalyzed Route to Imidazoles. Synthesis of LFA-1 Antagonists
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0604
Phenanthridine Synthesis via a Pd-Catalyzed Direct Arylation/N-Arylation Sequence
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0605
Zinc(II)-Catalyzed Synthesis of Poly-functionalized Pyrroles
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0606
Mn(III)-Catalyzed Synthesis of Pyrroles from Vinyl Azides and β-Keto Acids
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0607
Synthesis of Furans via Indium-Catalyzed Rearrangement of Acetylenic Epoxides
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Synthesis of Materials and Unnatural Products
z609
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0609
Greener 1,1-Difluoroallenes
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0610
Bulky, Solid…but still Topochemical!
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0611
Porphyrin-Annulene Hybrid
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0612
Polyaromatic Furans from Diynyl-1,6-diols
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0613
A Concise Route to Functionalized Truxenes
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0614
Cyanated Pentacene and Naphthacene as Air-Stable Acene Derivatives
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0615
9-H-9-Borafluorene: Hydroboration and Oligomerization
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0616
A New Twist to [2.2]Paracyclophanes
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0617
The Tale (Tail) of Hemifluorinated Surfactants
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0618
Through-Space in a Boat
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0619
Red-Shifted Porphyrins
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0620
A More Efficient Access to Tetraaza-pentacenes
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0621
Octupolar HBC Chromophores
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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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0623
Catalytic
Z
-Selective Olefin Cross-Metathesis
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0624
Synthesis of 2,3-Disubstituted Indolines by Asymmetric Hydrogenation
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0625
Construction of Quaternary Stereogenic Centers from Tertiary Boronic Esters
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0626
Catalytic Asymmetric Allylation of Unsaturated Methylidene Ketones
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0627
Ruthenium-Catalyzed Asymmetric [2+2] Cycloaddition of Ynamides with Enones
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0628
P*,P*-Bidentate Diamidophosphite Ligands in Palladium-Catalyzed Reactions
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0629
[3+2] Cycloaddition of Azomethine Ylides and Cyclopropylidene Acetates
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0630
Gold-Catalyzed Stereoselective Synthesis of Azetidin-3-ones
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0631
Palladium-Catalyzed Enyne Cyclization towards Complex Cyclopentanes
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0632
Catalytic Asymmetric Addition of Alkyl Enol Ethers to 1,2-Dicarbonyls
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0633
Ligand-Controlled Highly Regioselective and Asymmetric Hydrogenation of Quinoxalines
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0634
Vinylogous Mannich Reactions of Fluorinated Aldimines and Siloxyfurans
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0635
Diastereo- and Enantioselective Synthesis of Pyrrolidines
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0636
Synthesis of Chiral γ-Butyrolactones by a Domino Aldol-Cyclization Reaction
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0637
Nickel-Catalyzed Cycloaddition between Phthalic Anhydrides and Allenes
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0638
Rh(II)-Catalyzed Stereoselective Cross-Coupling of Diazo Compounds
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0639
Asymmetric Synthesis of γ-Butenolides via Sequential Metal-Catalyzed Reactions
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0640
Au(I)-Catalyzed Asymmetric Cycloadditions and Mannich Reactions of Azlactones
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0641
Asymmetric Addition of Boronic Acids to
N
-Benzylnicotinate Salts
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0642
Copper-Catalyzed Asymmetric Conjugate Addition of Grignard Reagents
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0643
Copper-Catalyzed Asymmetric Friedel-Crafts Reaction of Indoles
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0644
Ring Opening of Oxabicyclic Alkenes Catalyzed by Multinuclear Complexes
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0645
Novel Chiral Diene Ligand for Rhodium-Catalyzed Asymmetric 1,4-Addition
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0646
Asymmetric Propargylation of Imines
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0647
Combined Rh/Au Catalysis to Form 2,5-Dihydrofurans
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0648
Synthesis of γ-Quaternary Acylcyclopentenes via a Ring-Contraction Strategy
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0649
Enantio- and Diastereoselective Aldol Reaction of Thioamides
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0650
Asymmetric Palladium-Catalyzed Allylic Alkylation of Indoles
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0651
Rapid Access to Stereochemically Defined Heterocyclic Scaffolds
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0652
Highly Diastereoselective Iron-Mediated C(sp
²
)-C(sp
³
) Cross-Couplings
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Metal-Mediated Synthesis
z653
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0653
Ni-Catalyzed Alkyne Cycloaddition to Give Boronic Esters
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0654
Synthesis of Tertiary and Quaternary Allyl- and Crotylsilanes
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0655
Synthesis of Polysubstituted Indoles via Three-Component Reaction
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0656
Three-Component Cascade Reaction towards Substituted Tetrazoles
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0657
C-H Alkylation of Heteroarenes with Alkyl- and Alkoxymethyltrifluoroborates
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0658
Cu-Catalyzed Benzylic C-H Oxidation Using Imines as Directing Groups
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0659
Cyclobutenone Synthesis from 2,3-Allenoates and Organozincs
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0660
A Stereoselective Approach to Tetrasubstituted Silyl Enol Ethers
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0661
Cu-Catalyzed Highly Enantioselective 1,4-Addition of Grignard Reagents
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0662
Ni-Catalyzed Negishi Cross-Coupling of Secondary Alkylzinc Halides
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0663
Base-Mediated Biaryl Formation via Benzyne Intermediates
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0664
Pd-Catalyzed Coupling of Tetrafluoroethylene with Arylzinc Compounds
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0665
Titanium-Mediated Diastereo- and Enantioselective Dimerization of Enals
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0666
Synthesis and Cross-Coupling of Sulfonamidomethyltrifluoroborates
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0667
anti
-Carbozincation of Diethyl Acetylenedicarboxylate
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Organo- and Biocatalysis
z669
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0669
Trienamines in Organocatalysis
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0670
Metal-Free Aerobic Oxidation of Alcohols
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0671
How to Oxidize Methane with a P450 Enzyme
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0672
Highly Efficient Hydrogen-Bond Catalysis with (Thio)Phosphorodiamides
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0673
Reduction of Quinoxalines: A Convergent Disproportionation Reaction
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0674
Catalytic Asymmetric Aminoallylation of Aldehydes
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0675
Kinetic Resolution of Allylic Amines via a Dual-Catalysis Approach
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0676
Coupled Lewis Base and Phase-Transfer Catalysis for Imine Trifluoromethylation
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0677
Z
-Selective 1,4-Addition of 5
H
-Oxazol-4-ones with Alkynyl Carbonyl Compounds
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0678
Activation of C(sp
³
)-H Bond via 1,5-Hydride Transfer-Cyclization
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0679
Biocatalytic, Decarboxylative Addition of Malonates to Imines, a ”Rodionovase"
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0680
Asymmetric Vinylogous Michael Addition of Furanones to Nitroolefines
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0681
Catalytic Asymmetric Chlorocyclization of Unsaturated Amides to Heterocycles
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Polymer-Supported Synthesis
z683
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0683
Hydrogenation with Iron Nanoparticles Supported on CDG
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0684
Suzuki-Miyaura Coupling with Pd(OAc)
2
Supported on an Ionic Copolymer
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0685
Crotylation and Homopropargylation by Flow Technology
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0686
CuFe
2
O
4
Nanoparticles for N-Arylation of Heterocycles
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0687
Immobilized DMAP Derivatives Rivaling Homogeneous DMAP
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0688
Recyclable Polystyrene-Supported (Dichloroiodo)benzene
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0689
Synthesis of
N
,
N
-Bicyclic Pyrazolidinones Using Cu(OH)
x
/Al
2
O
3
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0690
Reduction of Nitroarenes and Alkenes with Rh-Fe
3
O
4
Nanocrystals
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0691
Suzuki-Miyaura Coupling with Sulfur-Modified Gold-Supported Palladium
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0692
Solid-Phase Synthesis of Polyamidoamines
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0693
Ring-Closing Metathesis for the Preparation of Cyclic Peptoids
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0694
Deoxygenation of Epoxides to Alkenes with H
2
Using Au/HT
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