Synthesis
Synthesis
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Issue 07/2025
Du, Zhongjian; Ji, Chenlei; Wang, Xu; Zhang, Sijian; Wang, Zhenyu; You, Yang'en:
Nickel(II)-Catalyzed Cycloisomerization of 1,6-Dienes
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Issue 05/2025
Chaudhury, Subhabrata; Thennakoon, Dulanjali; Wetzel, Edward A.; Donaldson, William A.:
A Scalable, Chromatography-Free Synthesis of the Potent and Highly Selective ERβ Agonist EGX358
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Issue 04/2025
Yanase, Kana; Morimoto, Koji; Dohi, Toshifumi; Kita, Yasuyuki:
Practical Synthesis of
N
-Anilinylphenothiazines Using a Cyclic Hypervalent Iodine Coupling Reagent
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Issue 03/2025
Fett, Niels Thomas; Muratore, Michael E.; Gmaschitz, Gerhard; Treu, Matthias:
Palladium-Catalyzed α-Arylation of Cycloalkanones with Sterically Hindered Bromoazines under Neat Conditions
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Issue 01/2025
Kumar, Deepak; Satam, Nishikant; Namboothiri, Irishi N. N.:
Magnesium-Mediated Regioselective Additions of Bromoform to Quinone Methides and Aurone-Derived Azadienes
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Issue 23/2024
Rigby, Jake M.; Chantry, Andrew; Hemmings, Andrew M.; Richards, Christopher J.; Stephenson, G. Richard; Storr, Thomas E.:
An Improved Synthesis of 2,3-Diamino-5,6-dichloropyrazine: A Useful Heterocyclic Scaffold
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Issue 05/2024
de Souza, João H.; Vargas, Jorge A. M.; Burtoloso, Antonio C. B.:
An Improved Protocol for the Synthesis of Carbonyl Sulfoxonium Ylides
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Issue 02/2024
Espinoza-Hicks, José C.; Zaragoza-Galán, Gerardo; Camacho-Dávila, Alejandro A.:
A Practical Synthesis of Homoallylic Diene Halides: Versatile Synthons for the Preparation of the Taxane A-Ring System
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Issue 24/2023
Chacon-Teran, Miguel A.; Bhattacharjee, Shubhra; Bailoo, Jeremy D.; Deonarine, Amrika; Findlater, Michael:
Improved Syntheses of an Arseno-Fatty Acid (As-FA 362) and an Arseno-Hydrocarbon (As-HC 444)
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Issue 23/2023
Vorasin, Onanong; Phumjan, Tanawat; Saepua, Siriporn; Iwaniuk, Daniel; Kamchonwongpaisan, Sumalee; Yuthavong, Yongyuth; Thongpanchang, Chawanee; Srimongkolpithak, Nitipol:
Development of a Practical Synthetic Method for Clinical Candidate 3-(2-{3-[(2,4-Diamino-6-ethylpyrimidin-5-yl)oxy]propoxy} phenyl)propanoic acid (P218) and Its Hydroxylated Metabolites
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Issue 20/2023
Broudic, Nathan; Pacheco-Benichou, Alexandra; Fruit, Corinne; Besson, Thierry:
Synthesis of Trifunctional Thiazole-Fused Anthranilonitrile and Anthranilic Acid Derivatives
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Issue 17/2023
Saito, Katsuya; Sawazaki, Tomoya; Furusawa, Osamu; Kosugi, Teruo; Kimura, Yoshikazu; Kirihara, Masayuki:
Practical Synthesis of Pent-4-yn-1-ol and Pent-4-en-1-ol from Tetrahydrofurfuryl Halides
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Issue 16/2023
Liu, Zheng; Lu, Sheng-Mei; Zhao, Bao-Qian; Chen, Hao-Dong; Chen, Mu-Wang; Zhou, Yong-Gui:
An Improved Synthesis of Chiral 2,2′-Bipyridine Ligand C3-ACBP Without Column Chromatography
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Issue 14/2023
Weber, T. Moritz; Pietruszka, Jörg:
Synthesis of a Water-Soluble Tridentate (Dimethylamino)ethyl Cu(I)/Cu(II)-Ligand
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Issue 13/2023
Sugiishi, Tsuyuka; Motegi, Ryohei; Amii, Hideki:
Intramolecular Cyclization of
N
-Propargylic Amides without Transition-Metal Catalysis for Synthesis of Fluoroalkylated Oxazoles: Using Carboxylic Acid Anhydrides as the Fluoroalkyl Source
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Issue 23/2022
Hebert, Olivier; Dubouilh-Benard, Carole; Campos, Joana F.; Berteina-Raboin, Sabine; Fruit, Corinne; Besson, Thierry:
Monitoring of Catalyst-Free Microwave-Assisted MCR-Type Synthesis of 2-Amino-3-cyano-4
H
-chromene Derivatives Using Raman Spectrometry
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Issue 11/2022
Peshkov, Anatoly A.; Makhmet, Azat; Bakulina, Olga; Kanov, Evgeny; Gainetdinov, Raul; Peshkov, Vsevolod A.; Dar’in, Dmitry; Krasavin, Mikhail:
A General Approach to Spirocyclic Piperidines via Castagnoli–Cushman Chemistry
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Issue 10/2022
Hayward, John J.; Mader, Lavleen; Trant, John F.:
Giving Preparative Thin-Layer Chromatography Some Tender Loving Care
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Issue 07/2022
Müller, Harald; Bourcet, Léa:
[1,3]-Dithiolo-[4,5-
d
][1,3-dithiole]-2,5-dione
Open Access
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PDF (417 kb)
Issue 03/2022
Alterman, Joshua L.; Kraus, George A.:
A Convenient Procedure for Sonogashira Reactions Using Propyne
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Issue 02/2022
Janicki, Ignacy; Kiełbasiński, Piotr:
A Straightforward, Purification-Free Procedure for the Synthesis of Ando and Still–Gennari Type Phosphonates
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Issue 23/2021
Nizovtsev, Alexey V.; Bovin, Nicolai V.:
A Facile Synthesis of 2-Aminopropane-1,2,3-tricarboxylic Acid and Its Symmetrical Dimethyl Ester
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Issue 19/2021
Kadyrov, Renat; Tok, Oleg L.:
Convenient Synthesis of (
R
)-3-[(
tert
-Butoxycarbonyl)amino]piperidine and (
R
)-3-[(
tert
-Butoxycarbonyl)amino]azepane
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Issue 15/2021
Erb, William; Wen, Min; Roisnel, Thierry; Mongin, Florence:
Synthesis of Ferrocenesulfonyl Chloride: Key Intermediate toward Ferrocenesulfonamides
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Issue 04/2021
Lei, Peng; Li, Guangchen; Ling, Yun; An, Jie; Nolan, Steven P.; Szostak, Michal:
Protocol for Palladium/
N
-Heterocyclic Carbene-Catalyzed Suzuki–Miyaura Cross-Coupling of Amides by N–C(O) Activation
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Issue 24/2020
Moriguchi, Kento; Kono, Taro; Seko, Shinzo; Tanabe, Yoo:
Gram-Scale Robust Synthesis of 1-Chloro-2,3-dimethyl-4-phenylnaphthalene: A Promising Scaffold with Three Contiguous Reaction Positions
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Issue 23/2020
Bhilare, Shatrughn; Kori, Santosh; Shet, Harshita; Balaram, Gundapally; Mahendar, Koosam; Sanghvi, Yogesh S.; Kapdi, Anant R.:
Scale-Up of a Heck Alkenylation Reaction: Application to the Synthesis of an Amino-Modifier Nucleoside ‘Ruth Linker’
FREE ACCESS
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Issue 22/2020
Delpe Acharige, Anjana; Neri, Raul; Hodgson, James; Bossmann, Stefan H.:
A Catalyst-Free, Temperature-Driven One-Pot Synthesis of 1-Adamantylhydrazine Hydrochloride
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Issue 21/2020
Kadari, Lingaswamy; Roisnel, Thierry; Erb, William; Krishna, Palakodety Radha; Mongin, Florence:
Remote Deprotometalation-Iodolysis of
N
,
N
-Diisopropyl-2-trimethylsilylferrocenecarboxamide: A New Route Toward 1,1′-Disubstituted Ferrocenes
FREE ACCESS
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Issue 20/2020
Souquet, Florence; Drici, Wassila; Fayssal, Sandra Abi; Lazouni, Imane; Thueillon, Sébastien; Pérard-Viret, Joëlle:
N
-Acyliminium Ion Chemistry: Improving the Access to Unsaturated γ-Lactams and Their
N
-α-Methoxylated Derivatives: Application to an Expeditive Synthesis of (±)-Crispine A
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Issue 19/2020
Cavarischia, Claudia; Comely, Alex; Écija, Marta; Iacoangeli, Tommaso; Pastó, Mireia; Silvestri, Lavinia; Furlotti, Guido:
A Convenient, Scalable Process for the Preparation and Purification of Calcium Acamprosate
FREE ACCESS
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Issue 18/2020
Zisopoulou, Stavroula A.; Pafili, Anastasia E.; Gkizis, Petros; Andreou, Thanos; Koftis, Theoharis V.; Lithadioti, Alexandra; Neokosmidis, Efstratios; Gallos, John K.:
Environmentally Benign Large-Scale Synthesis of a Precursor to Vortioxetine
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Issue 17/2020
Steinebach, Christian; Voell, Sabine Anna; Vu, Lan Phuong; Bricelj, Aleša; Sosič, Izidor; Schnakenburg, Gregor; Gütschow, Michael:
A Facile Synthesis of Ligands for the von Hippel–Lindau E3 Ligase
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Issue 15/2020
Tom, Mai-Jan; Turnbull, Ben W. H.; Evans, P. Andrew:
A Concise and Modular Three-Step Synthesis of (
S
)-Verapamil using an Enantioselective Rhodium-Catalyzed Allylic Alkylation Reaction
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Issue 08/2020
Mulks, Florian F.; Heckershoff, Robin; Zimmer, Marc; Hashmi, A. Stephen K.:
Practical Preparation of Cyclopropenone 1,3-Propanediol Ketal
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Issue 06/2020
Morra, Barbora; Morra, Nicholas A.; MacDonald, Daniel G.; Pagenkopf, Brian L.:
Gram-Scale Synthesis of the Co(nmp)
2
Catalyst to Prepare
trans
-2,5-Disubstituted Tetrahydrofurans by the Aerobic Oxidative Cyclization of Pent-4-en-1-ols
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Issue 05/2020
Sherwood, Alexander M.; Meisenheimer, Poncho; Tarpley, Gary; Kargbo, Robert B.:
An Improved, Practical, and Scalable Five-Step Synthesis of Psilocybin
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Issue 23/2019
Zilate, Bouthayna; Fischer, Christian; Schneider, Lukas; Sparr, Christof:
Scalable Synthesis of Acridinium Catalysts for Photoredox Deuterations
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Issue 20/2019
Ashida, Yuya; Kondo, Shoichi; Arashiba, Kazuya; Kikuchi, Takamasa; Nakajima, Kazunari; Kakimoto, Seizo; Nishibayashi, Yoshiaki:
A Practical Synthesis of Ammonia from Nitrogen Gas, Samarium Diiodide and Water Catalyzed by a Molybdenum–PCP Pincer Complex
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Issue 17/2019
Erb, William; Roisnel, Thierry; Dorcet, Vincent:
Practical Chromatography-Free Synthesis of 2-Iodo-
N
,
N
-diisopropylferrocenecarboxamide and Further Transformations
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PDF (303 kb)
Issue 16/2019
Tao, Jason; Murphy, Graham K.:
A Practical, Large-Scale Synthesis of
p
-(Difluoroiodo)toluene (
p
-TolIF
2
)
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PDF (1591 kb)
Issue 15/2019
Torruellas, Carilyn; Hsu, Fu-Lian; Walz, Andrew J.:
Synthesis of
N
-Pyridyl Hydroxylamines via Copper-Catalyzed Cross-Coupling
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Issue 13/2019
Yin, Lingfeng; Mao, Yongjun; Liu, Yaowei; Bu, Lehao; Zhang, Long; Chen, Wenxin:
New Synthetic Route to Tucatinib
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PDF (153 kb)
Issue 12/2019
Rouzier, Florian; Sillé, Rosanne; Nourry, Arnaud; Tessier, Arnaud; Pipelier, Muriel; Guillarme, Stéphane:
Practical Gram-Scale Synthesis of Either α- or β-Anomer of
C
-Vinyl Glycosides
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PDF (290 kb)
Issue 07/2019
Nakura, Ryo; Inoue, Kazuki; Okano, Kentaro; Mori, Atsunori:
Practical Synthesis of Precursors of Cyclohexyne and 1,2-Cyclohexadiene
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Issue 04/2019
Morales-Chamorro, Maricela; Vázquez, Alfredo:
A Facile Synthesis of
N
-Boc-azocan-5-one
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PDF (178 kb)
Issue 02/2019
Shirinian, Valerii Z.; Lonshakov, Ilya A.; Zakharov, Alexey V.; Lvov, Andrey G.; Krayushkin, Mikhail M.:
Practical Deoxygenation of Oxazole
N
-Oxides by PCl
3
/Collidine
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PDF (193 kb)
Issue 23/2018
Baidilov, Daler; Makarova, Mariia; Rycek, Lukas; Hudlicky, Tomas:
Preparation of Rearranged Allylic Isocyanates from the Reaction of Allylic Alcohols with 1-Cyano-4-dimethylaminopyridinium Bromide
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Issue 17/2018
Olmos, Andrea; Pereira, Ana; Belderrain, Tomás R.; Pérez, Pedro J.:
Multigram Synthesis of Thallium Trispyrazolylborate Compounds
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Fearraigh, Martin P. Ó; Matlock, Johnathan V.; Illa, Ona; McGarrigle, Eoghan M.; Aggarwal, Varinder K.:
Synthesis of Isothiocineole and Application in Multigram-Scale Sulfur Ylide Mediated Asymmetric Epoxidation and Aziridination
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Issue 09/2018
Khan, Imran; Luo, Zhi-Bin; Valeru, Anil; Xu, Yin; Liu, Bin; Sangepu, Bhavanarushi; Xie, Ji-Min:
Dihydroxylation of Olefins with Potassium Permanganate Catalyzed by Imidazolium Salt
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Issue 08/2018
Jiang, Xingguo; Ma, Shengming:
Studies on Iron-Catalyzed Aerobic Oxidation of Benzylic Alcohols to Carboxylic Acids
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PDF (528 kb)
Issue 05/2018
Matoba, Kazutaka; Eizawa, Aya; Nishimura, Shunsuke; Arashiba, Kazuya; Nakajima, Kazunari; Nishibayashi, Yoshiaki:
Practical Synthesis of a PCP-Type Pincer Ligand and Its Metal Complexes
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Issue 04/2018
Plevová, Kristína; Mudráková, Brigita; Šebesta, Radovan:
A Practical Three-Step Synthesis of Vinylferrocene
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Issue 02/2018
Buonomo, Joseph A.; Eiden, Carter G.; Aldrich, Courtney C.:
Scalable Synthesis of Hydrido-Disiloxanes from Silanes: A One-Pot Preparation of 1,3-Diphenyldisiloxane from Phenylsilane
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Issue 24/2017
Hamper, Bruce C.; Sullivan, Brendan T.; Rath, Nigam P.; Spilling, Christopher D.:
A Practical Gram-Scale Synthesis of Acrylohydroxamic Acid
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Issue 18/2017
Weiberth, Franz J.; Bourque, Andre J.; Elenbaas, Steven; Hanna, Reda; Powers, Matthew R.; Siegel, Craig S.; Zhao, Jin:
Scalable Syntheses of Chirally Pure Mono-protected and Orthogonally Di-protected
cis
-3,4-Diaminotetrahydrofurans
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PDF (166 kb)
Issue 14/2017
Kotthaus, Andreas F.; Ballaschk, Frederic; Stakaj, Vjoni; Mohr, Fabian; Kirsch, Stefan F.:
Synthesis and Resolution of a Chiral Diamine: 2,2′-(Propane-2,2-diyl)dipyrrolidine
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PDF (337 kb)
Issue 13/2017
Denmark, Scott E.; Chi, Hyung Min:
Synthesis of 2-Alkenyl-Tethered Anilines
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PDF (309 kb)
Issue 11/2017
van der Haas, Richard N. S.; Dekker, Jeroen A.; Hassfeld, Jorma; Hager, Anastasia; Fey, Peter; Rubenbauer, Philipp; Damen, Eric:
Synthesis and Properties of 2-Oxa-6-azaspiro[3.3]heptane Sulfonate Salts
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Issue 09/2017
De Angelis, Sonia; Celestini, Paolo; Rebuzzini, Gabriele; Degennaro, Leonardo; Luisi, Renzo:
A Practical
11
B NMR Evaluation of BH
3
Titer in Commercial Solutions
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PDF (660 kb)
Issue 03/2017
Blades, Kevin; Glossop, Steven C.:
A Three-Step Protocol towards
N
-8-(2,2-Dimethoxyethyl)-2-methylsulfanylpyrido[2,3-
d
]pyrimidin-7-one
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PDF (142 kb)
Issue 21/2016
Luo, Zhi-bin; Zhao, Chen; Xie, Jimin; Lu, Hong-fei:
An Efficient and Practical Method for Olefin Dihydroxylation
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PDF (187 kb)
Issue 20/2016
Godeau, Julien; Martinet, Anthony; Levacher, Vincent; Fruit, Corinne; Besson, Thierry:
Efficient Microwave-Assisted Synthesis of Methyl 4- or 5-Nitroanthranilate
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PDF (1073 kb)
Issue 18/2016
Zhu, Cheng-Liang; Lu, Deng-Fu; Sears, Jeffrey D.; Jia, Zhen-Xin; Xu, Hao:
Practical Synthetic Procedures for the Iron-Catalyzed Intermolecular Olefin Aminohydroxylation Using Functionalized Hydroxylamines
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PDF (266 kb)
Issue 14/2016
Hill, Matthew D.:
A Multicomponent Approach to Highly Substituted 1
H
-Pyrazolo[3,4-
b
]pyridines
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PDF (192 kb)
Issue 13/2016
Castillo-Rangel, Norma; Pérez-Díaz, José Oscar H.; Vázquez, Alfredo:
An Expeditious Synthesis of 8-Methoxy-1-tetralone
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PDF (994 kb)
Issue 11/2016
Kerkovius, Jeff K.; Menard, Frederic:
A Practical Synthesis of 6,8-Difluoro-7-hydroxycoumarin Derivatives for Fluorescence Applications
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PDF (205 kb)
Issue 09/2016
Mao, Yongjun; Zhu, Chunping; Zhu, Guoqing; Wang, Han; Ren, Xinfeng:
Kilogram Synthesis of Crebinostat
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PDF (150 kb)
Issue 08/2016
Herrera, Alberto; Linden, Anthony; Heinemann, Frank W.; Brachvogel, René-Chris; von Delius, Max; Dorta, Romano:
Optimized Syntheses of Optically Pure P-Alkene Ligands: Crystal Structures of a Pair of P-Stereogenic Diastereomers
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PDF (400 kb)
Issue 07/2016
Balakrishna, Bugga; Vidal-Ferran, Anton:
A Practical Synthesis of Rhodium Precatalysts for Enantioselective Hydrogenative Transformations
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PDF (177 kb)
Issue 02/2016
Correia, Henrique D.; Cicolani, Renato S.; Moral, Raphael F.; Demets, Grégoire J. F.:
Easy Synthesis of
trans
-4,5-Dihydroxy-2-imidazolidinone and 2,4-Dimethylglycoluril
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PDF (147 kb)
Issue 01/2016
Varjosaari, Sami E.; Suating, Paolo; Adler, Marc J.:
One-Pot Synthesis of
O
-Aryl Carbamates
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PDF (170 kb)
Issue 24/2015
Beaudoin, Daniel; Rominger, Frank; Mastalerz, Michael:
Efficient, Scalable Syntheses of Important Intermediates in Tribenzotriquinacene Chemistry
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PDF (740 kb)
Issue 23/2015
Roy, Sudeshna; Sutivisedsak, Nongnuch; Hamper, Bruce C.; Lyss, Alexander M.; Spilling, Christopher D.:
A Practical and Scalable Synthesis of (
S
)- and (
R
)-1-(Dimethoxyphosphoryl)allyl Methyl Carbonates
Full Text
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PDF (173 kb)
Issue 20/2015
Mao, Yongjun; Zhu, Chunping; Kong, Ziyang; Wang, Jiao; Zhu, Guoqing; Ren, Xinfeng:
New Synthetic Process for Bosutinib
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PDF (183 kb)
Issue 18/2015
Zhang, Ziyang; Kitamura, Yoshiaki; Myers, Andrew G.:
An Efficient Directed Claisen Reaction Allows for Rapid Construction of 5,6-Disubstituted 1,3-Dioxin-4-ones
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Issue 17/2015
Lei, Xiangyang; Jalla, Anusha; Abou Shama, Mhd A.; Stafford, Jamie M.; Cao, Billy:
Chromatography-Free and Eco-Friendly Synthesis of Aryl Tosylates and Mesylates
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PDF (201 kb)
Issue 15/2015
Le Marquer, Nicolas; Laurent, Mathieu Yves; Martel, Arnaud:
A Practical and Cost-Effective Method for the Synthesis of Bicyclo[2.2.2]octane-1,4-dicarboxylic Acid
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PDF (689 kb)
Issue 14/2015
Marelli, Enrico; Fernández Salas, José A.; Nolan, Steven P.:
Synthesis of an Intermediate of Nafoxidine via Nickel-Catalyzed Ketone Arylation
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PDF (193 kb)
Issue 13/2015
Chmurski, Kazimierz; Stepniak, Pawel; Jurczak, Janusz:
Improved Synthesis of C2 and C6 Monoderivatives of α- and β-Cyclodextrin via the Click Chemistry Approach
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PDF (183 kb)
Issue 11/2015
Aitken, R. Alan; Meehan, Anna; Power, Lynn A.:
Synthesis of (
R
)-Lactic Acid and (2
R
,5
R
)-2-
tert
-Butyl-5-methyl-1,3-dioxolan-4-one
Full Text
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PDF (685 kb)
Issue 10/2015
Mao, Yongjun; Jiang, Luobin; Chen, Tianyun; He, Haijun; Liu, Gang; Wang, Han:
A New and Practical Synthesis of Vortioxetine Hydrobromide
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PDF (140 kb)
Issue 09/2015
Kurata, Kaoruko; Inoue, Kumiko; Nishimura, Kazuhiko; Hoshiya, Naoyuki; Kawai, Nobuyuki; Uenishi, Junichi:
Synthesis of Optically Pure (
R
)- and (
S
)-Tetrahydroisoquinoline-1- and -3-Carboxylic Acids
Full Text
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PDF (197 kb)
Issue 08/2015
Molnár, Katalin; Takács, László; Kádár, Mihály; Kardos, Zsuzsanna; Faigl, Ferenc:
A Practical Route for the Preparation of Bis(2,2,2-trifluoroethyl) 2-Oxoalkylphosphonates
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Issue 07/2015
Castelló, Luis M.; Nájera, Carmen; Sansano, José M.; Larrañaga, Olatz; de Cózar, Abel; Cossío, Fernando P.:
Enantioselective Synthesis of
exo
-4-Nitroprolinates from Nitroalkenes and Azomethine Ylides Catalyzed by Chiral Phosphoramidite·Silver(I) or Copper(II) Complexes
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PDF (248 kb)
Issue 03/2015
Tummatorn, Jumreang; Thongsornkleeb, Charnsak; Ruchirawat, Somsak; Thongaram, Phanida; Kaewmee, Benyapa:
Convenient and Direct Azidation of
sec
-Benzyl Alcohols by Trimethylsilyl Azide with Bismuth(III) Triflate Catalyst
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PDF (212 kb)
Issue 01/2015
Daniels, David S. B.; Smith, Siobhan R.; Lebl, Tomas; Shapland, Peter; Smith, Andrew D.:
A Scalable, Chromatography-Free Synthesis of Benzotetramisole
FREE ACCESS
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PDF (218 kb)
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